CN104663956B - Safflower seabuckthorn freeze-dried instant tea powder - Google Patents
Safflower seabuckthorn freeze-dried instant tea powder Download PDFInfo
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- CN104663956B CN104663956B CN201510054854.2A CN201510054854A CN104663956B CN 104663956 B CN104663956 B CN 104663956B CN 201510054854 A CN201510054854 A CN 201510054854A CN 104663956 B CN104663956 B CN 104663956B
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Abstract
The invention discloses a kind of preparation method of safflower seabuckthorn freeze-dried instant tea powder, its drip irrigation device is：The present invention processes disintegrating slag as raw material using safflower suede, sea-buckthorn, does active ingredient in extraction media safflower extracting using water, and it is refined by purifying, concentrating；Active ingredient in sea-buckthorn branches and leaves disintegrating slag is extracted using ultrasonic assistant complex enzyme (cellulase, pectase) extraction method, and concentrating and impurity removing is carried out to it；Processing is dried using vacuum-freezing process, finally carried out using superfine communication technique exquisite into instant tea powder.The present invention is utilized to the disintegrating slags of safflower leftover pieces and Leaves of Hippophae L, avoids the wasting of resources, and the safflower seabuckthorn freeze-dried instant tea powder after ultramicro grinding is refined, delicate mouthfeel, strong and brisk in taste；Possess safflower, the nutritive value of sea-buckthorn.
Description
Technical field
The present invention relates to a kind of instant tea powder, more particularly to a kind of safflower seabuckthorn freeze-dried instant tea powder.
Background technology
The dry tubular flower of safflower category feverfew, history are loaded in《Kaibao Bencao》, " blood transports lockjaw after main product, extravesated blood in abdomen
Not to the utmost, angina, fail before being carrying out, and wine boils clothes, also blood under middle disease due to noxious agents produced by various parasites ".It has coronary artery, hypotensive, resist oxygen lack, promoting blood circulationization
A variety of pharmacological effects such as the stasis of blood, anti-inflammatory and antalgic.
Contain a variety of biochemical compositions (flavonoids, fats, several amino acids, organic acid, unsaturation in sea-buckthorn branches and leaves
Aliphatic acid) and abundant vitamin etc., there is good effect to human body immune function, antioxygenic property etc..
But many leftover pieces can be left after safflower is processed, sea-buckthorn branches and leaves make the disintegrating slag left after sea-buckthorn tea,
All also there is multi-purpose nutriment in the leftover pieces of safflower and the disintegrating slag of sea-buckthorn branches and leaves, if directly discarded resulted in wave
Take, so being badly in need of a kind of product can be utilized, avoid wasting.
The content of the invention
The technical problem to be solved in the present invention is to overcome the defects of existing, there is provided a kind of safflower seabuckthorn freeze-dried instant tea powder.
A kind of safflower seabuckthorn freeze-dried instant tea powder, it is characterised in that including the composition and sand extracted out of safflower leftover pieces
The composition extracted in the disintegrating slag of spine branch leaf, its manufacturing process comprise the following steps：
(1) first safflower leftover pieces and the disintegrating slag of sea-buckthorn branches and leaves are cleaned and dried；
(2) extraction media is done using active ingredient in reflux extraction safflower using water；Its step is as follows：
By the leftover bits and pieces in safflower process, crushed after drying process, cross 40-80 mesh sieves, it is front and rear to press solid-to-liquid ratio
Example 1：15-18 add water, temperature be 70-80 DEG C at a temperature of extract 1-2 hours, it is front and rear twice, merge leaching liquor, 500 mesh
Filtration treatment, stand an evening, extract supernatant, cross D101 macroporous absorbent resins, regulation flow velocity 3B column volume/when；After upper prop terminates,
Carry out rushing post removal of impurities with 3B cylinders water accumulating volume；Eluted using gradient method, alcohol gradient be 30%-35%, 80%,
95%；Eluent is collected, eluent spirituosity concentration is 70-75%, stands 48 hours, extracts supernatant, concentration is recovered under reduced pressure
Temperature is 50-65 DEG C, and concentration amount is stored under refrigeration at 1/2,4 DEG C of original volume, and it is safflower clear cream to extract supernatant；
(3) it is as follows using the active ingredient in ultrasonic assistant multiplex-enzyme extraction method extraction sea-buckthorn branches and leaves disintegrating slag, its step：
Leftover bits and pieces during sea-buckthorn tea is processed, cleaning-drying processing is carried out, 40-80 mesh sieves are crossed after crushing, are pressed
Ratio 1：15 add water, add 1-2% cellulase, pectase complex enzyme hydrolysis system 1.5-2：1, pH to 4.5-5.0 is adjusted,
50 DEG C of temperature digest 60-80min under ultrasonic power 500-600W power, and rise temperature is stopped to after boiling destroy the enzyme treatment 10min
Only heat, extract 1 hour, stirring once, releases filtrate per 20min；1 is pressed in residue：10 ratios add water, are 80 DEG C in temperature
Under, temperature extraction takes 1h, releases filtrate；Merging filtrate, stood for 1 evening, release precipitation, 500 are filtered now, and filtrate is handed over cation
Change resin and anion exchange resin carries out desalting processing, liquid is flowed through in collection, carries out ultrafiltration, is concentrated under reduced pressure under 60-70 degrees Celsius
To 30%-40% containing dry, 0-4 DEG C of refrigeration of concentrate, it is hippophae rhamnoides to extract supernatant；
(4) active ingredient extracted in the active ingredient and sea-buckthorn branches and leaves disintegrating slag extracted safflower leftover pieces is according to 4：6
Ratio is mixed, homogeneous；
(5) take supernatant to be freeze-dried through staticly settling the material mixed, ultramicro grinding carried out to dried object,
It is crushed to 10 μm or so of particle；
(6) packed.
Compared with prior art, the beneficial effects of the invention are as follows：Safflower is effectively combined with the nutritive value of sea-buckthorn,
Prepared using pure natural extraction process, embody green, the theory of health, using discarded leftover bits and pieces as raw material, embodied
18 it is big since thrifty, resource make full use of, the call of environmental protection, keep up with the trend of the times.Safflower seabuckthorn produced by the present invention freezes
Instant tea powder can take after mixing it with water in the hot water, tea powder particle≤10 μm after ultramicro grinding, solubility >=98%, and it is immune to possess regulation
Systemic-function, beneficial sleep, antifatigue, anti-aging, prevention cardiovascular and cerebrovascular disease, norcholesterol, the healthcare function of hypotensive.
Embodiment
The following examples, the embodiment of the present invention is described in further detail.Following examples are used to say
The bright present invention, but it is not limited to the scope of the present invention.
Embodiment one：Accurately, unambiguously
(1) by the leftover bits and pieces in safflower process, crushed after drying process, cross 50 mesh sieves, it is front and rear to press solid-to-liquid ratio
Example 1：18、1：15 (g/g) add water, and 1h is extracted at a temperature of temperature is 80 DEG C, it is front and rear twice, merge leaching liquor, 500 mesh mistakes
Filter is handled, and is stood an evening, is extracted supernatant,
(2) supernatant is crossed into D101 large pore resin absorption columns, regulation flow velocity 3B column volumes/h；After upper prop terminates, with 3B
Cylinder water accumulating volume carries out rushing post removal of impurities；Eluted using alcohol gradient method；Eluent is collected, eluent spirituosity concentration is
75%, 48 hours are stood, extracts supernatant
(3) concentration being recovered under reduced pressure in 60 DEG C of gained elution supernatant, concentration amount is the 1/2 of original volume,
(4) stored under refrigeration at 0-4 DEG C, it is standby to extract supernatant.
(5) leftover bits and pieces during sea-buckthorn tea is processed, cleaning-drying processing is carried out, 40-80 mesh sieves is crossed after crushing,
In proportion 1：15 add water, add 1% cellulase, pectase complex enzyme hydrolysis system (1.5：1), regulation pH to 4.5,50 DEG C
Temperature digests 60min under ultrasonic power 500W power.
(6) temperature is raised to boiling destroy the enzyme treatment 10min, after, stop heating, extract 1h, stirring once, is put per 20min
Go out filtrate；1 is pressed in residue：10 ratios add water, and in the case where temperature is 80 DEG C, temperature extraction takes 1h, releases filtrate；Merging filtrate, it is quiet
Put for 1 evening.
(7) precipitation is released, 500 are filtered now, and filtrate is taken off with cationic ion-exchange resin and anion exchange resin
Liquid is flowed through in salt treatment, collection, carries out ultrafiltration (0.45 micron, 0.2Mpa), and 60 DEG C are concentrated under reduced pressure into containing soluble solid 37%,
4 DEG C of refrigerations of concentrate, it is hippophae rhamnoides to extract supernatant.
(8) 1 is pressed：2 ratios mix step (4), (7) gained clear liquid, add 8% beta-schardinger dextrin, homogenization, carry out cold
It is lyophilized dry.
(9) gained dry product carries out ultramicro grinding, makes its particle≤10 μm.
(10) aseptic packaging.
Embodiment two,
(1) by the leftover bits and pieces in safflower process, crushed after drying process, cross 80 mesh sieves, it is front and rear to press solid-to-liquid ratio
Example 1：15 (g/g) add water, 1.5h are extracted at a temperature of temperature is 70 DEG C, front and rear to merge leaching liquor twice, 500 mesh filter
Processing, an evening is stood, extracts supernatant,
(2) supernatant is crossed into D101 large pore resin absorption columns, regulation flow velocity 3B column volumes/h；After upper prop terminates, with 3B
Cylinder water accumulating volume carries out rushing post removal of impurities；Eluted using alcohol gradient method, collect eluent, eluent spirituosity concentration is
70%, 48 hours are stood, extracts supernatant.
(3) concentration being recovered under reduced pressure in 60 DEG C of gained elution supernatant, concentration amount is the 1/2 of original volume,
(4) stored under refrigeration at 0-4 DEG C, it is standby to extract supernatant.
(5) leftover bits and pieces during sea-buckthorn tea is processed, cleaning-drying processing is carried out, 480 mesh sieves is crossed after crushing, are pressed
Ratio 1：15 add water, add 2% cellulase, pectase complex enzyme hydrolysis system (2：1) pH to 4.5,50 DEG C of temperature, are adjusted
80min is digested under ultrasonic power 550W power
(6) temperature is raised to boiling destroy the enzyme treatment 10min, after, stop heating, extract 1h, stirring once, is put per 20min
Go out filtrate；1 is pressed in residue：15 ratios add water, and in the case where temperature is 80 DEG C, temperature extraction takes 1h, releases filtrate；Merging filtrate, it is quiet
Put for 1 evening.
(7) precipitation is released, 500 are filtered now, and filtrate is taken off with cationic ion-exchange resin and anion exchange resin
Liquid is flowed through in salt treatment, collection, carries out ultrafiltration (0.45 micron, 0.2Mpa), 60 DEG C are concentrated under reduced pressure into containing soluble solid 30%
Left and right, 4 DEG C of refrigerations of concentrate, it is hippophae rhamnoides to extract supernatant.
(8) 2 are pressed：3 ratios mix step (4), (7) gained clear liquid, add 8% beta-schardinger dextrin, homogenization, carry out cold
It is lyophilized dry.
(9) gained dry product carries out ultramicro grinding, makes its particle≤10 μm.
(10) sterilizing, aseptic packaging.
Finally it should be noted that：The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention,
Although the present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, it still may be used
To be modified to the technical scheme described in foregoing embodiments, or equivalent substitution is carried out to which part technical characteristic.
Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in the present invention's
Within protection domain.
Claims (1)
1. a kind of safflower seabuckthorn freeze-dried instant tea powder, it is characterised in that including the composition extracted out of safflower leftover pieces and sea-buckthorn
The composition extracted in the disintegrating slag of branches and leaves, its manufacturing process comprise the following steps：
(1) first safflower leftover pieces and the disintegrating slag of sea-buckthorn branches and leaves are cleaned and dried；
(2) extraction media is done using active ingredient in reflux extraction safflower using water；Its step is as follows：
By the leftover bits and pieces in safflower process, crushed after drying process, cross 40-80 mesh sieves, it is front and rear in solid-liquid ratio 1：
15-18 adds water, 1-2 hours is extracted at a temperature of temperature is 70-80 DEG C, front and rear to merge leaching liquor twice, 500 mesh filter
Processing, stand an evening, extract supernatant, cross D101 macroporous absorbent resins, regulation flow velocity 3B column volume/when；After upper prop terminates, use
3B cylinders water accumulating volume carries out rushing post removal of impurities；Eluted using gradient method, alcohol gradient is 30%-35%, 80%, 95%；Receive
Collect eluent, eluent spirituosity concentration is 70-75%, stands 48 hours, extracts supernatant, thickening temperature, which is recovered under reduced pressure, is
50-65 DEG C, concentration amount is stored under refrigeration at 1/2,4 DEG C of original volume, and it is safflower clear cream to extract supernatant；
(3) it is as follows using the active ingredient in ultrasonic assistant multiplex-enzyme extraction method extraction sea-buckthorn branches and leaves disintegrating slag, its step：
Leftover bits and pieces during sea-buckthorn tea is processed, cleaning-drying processing is carried out, 40-80 mesh sieves are crossed after crushing, in proportion
1：15 add water, add 1-2% cellulase, pectase complex enzyme hydrolysis system 1.5-2：1, adjust pH to 4.5-5.0,50 DEG C
Temperature digests 60-80min under ultrasonic power 500-600W power, and rise temperature stops adding to after boiling destroy the enzyme treatment 10min
Heat, extract 1 hour, per 20min, stirring once, releases filtrate；1 is pressed in residue：10 ratios add water, in the case where temperature is 80 DEG C,
Temperature extraction takes 1h, releases filtrate；Merging filtrate, stood for 1 evening, release precipitation, 500 filter now, by filtrate cation exchange
Resin and anion exchange resin carry out desalting processing, and liquid is flowed through in collection, carry out ultrafiltration, are concentrated under reduced pressure under 60-70 degrees Celsius
30%-40% containing dry, 0-4 DEG C of refrigeration of concentrate, it is hippophae rhamnoides to extract supernatant；
(4) active ingredient extracted in the active ingredient and sea-buckthorn branches and leaves disintegrating slag extracted safflower leftover pieces is according to 4：6 ratio
Mixed, homogeneous；
(5) material mixed is taken supernatant to be freeze-dried, carries out ultramicro grinding to dried object, crush through staticly settling
To 10 μm of particle；
(6) packed.
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| CN104996645A (en) * | 2015-08-30 | 2015-10-28 | 余芳 | Processing method of schisandra chinensis tea essence |
| CN108244295A (en) * | 2018-03-23 | 2018-07-06 | 青海康普生物科技股份有限公司 | A kind of preparation method of sea-buckthorn Fu tea |
| CN108902405A (en) * | 2018-06-26 | 2018-11-30 | 新疆超越歆生物科技有限公司 | The manufacture craft of lycium ruthenicum sea-buckthorn freeze-dried instant powder |
| CN109480017A (en) * | 2018-12-17 | 2019-03-19 | 邵阳学院 | A kind of Ramulus et Folium Mussaendae Pubescentis extract and the preparation method and application thereof |
| CN115005300A (en) * | 2022-05-17 | 2022-09-06 | 铜仁市印江青耕茶叶有限公司 | Internal heat-reducing scented tea and preparation method thereof |
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|---|---|---|---|---|
| CN101238842A (en) * | 2007-02-05 | 2008-08-13 | 高原圣果沙棘制品有限公司 | Sea-buckthorn instant tea and preparation thereof |
| CN103271187A (en) * | 2013-05-21 | 2013-09-04 | 宁波优美肽生物科技有限公司 | Enzyme immobilization method for preparing tea concentrated juice or instant tea powder |
| CN104189031A (en) * | 2014-09-04 | 2014-12-10 | 南京标科生物科技有限公司 | Method for extracting total flavones of hippophae rhamnoides from hippophae rhamnoides leaves |
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2015
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Patent Citations (3)
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| CN101238842A (en) * | 2007-02-05 | 2008-08-13 | 高原圣果沙棘制品有限公司 | Sea-buckthorn instant tea and preparation thereof |
| CN103271187A (en) * | 2013-05-21 | 2013-09-04 | 宁波优美肽生物科技有限公司 | Enzyme immobilization method for preparing tea concentrated juice or instant tea powder |
| CN104189031A (en) * | 2014-09-04 | 2014-12-10 | 南京标科生物科技有限公司 | Method for extracting total flavones of hippophae rhamnoides from hippophae rhamnoides leaves |
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| 中压制备与大孔树脂联用快速分离羟基红花黄色素A;武永刚等;《湖北农业科学》;20120430;第51卷(第7期);第1441-1443页 * |
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