CN104649471B - A kind of fracturing outlet liquid processes recycling flow process - Google Patents

A kind of fracturing outlet liquid processes recycling flow process Download PDF

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Publication number
CN104649471B
CN104649471B CN201410845813.0A CN201410845813A CN104649471B CN 104649471 B CN104649471 B CN 104649471B CN 201410845813 A CN201410845813 A CN 201410845813A CN 104649471 B CN104649471 B CN 104649471B
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liquid
fracturing outlet
outlet liquid
fracturing
discharge opeing
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CN104649471A (en
Inventor
徐迎新
杨博丽
袁伟文
张冕
李启新
席仲琛
谢涛
韩静静
任荣利
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China National Petroleum Corp
CNPC Chuanqing Drilling Engineering Co Ltd
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CNPC Chuanqing Drilling Engineering Co Ltd
Changqing Downhole Operation Co of CNPC Chuanqing Drilling Engineering Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/24Treatment of water, waste water, or sewage by flotation
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2301/00General aspects of water treatment
    • C02F2301/08Multistage treatments, e.g. repetition of the same process step under different conditions

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  • Life Sciences & Earth Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Cyclones (AREA)

Abstract

The present invention provides a kind of fracturing outlet liquid to process recycling flow process, discharge opeing is returned from what well head open flow went out, sequentially pass through high pressure cyclone desanding device, reducing pressure by regulating flow manifold, low voltage three-phase segregation apparatus and fine filtration device, fracturing outlet liquid storage tank, reconfigure fracturing fluid through detection interpolation water conditioner and leave in fracturing fluid storage tank, isolated gas after high pressure cyclone desanding device collected by gas transmission line, the Selid propping agent that container collection goes out collected through low voltage three-phase segregation apparatus sub-argument by proppant, the present invention saves water blanket, shorten construction period, monolayer shortens about 1 day engineering time, next lamination that can be used for very moment well splits, and take up an area and little need not storage reaction pond etc., recycling water resource, reduce environmental pollution.

Description

A kind of fracturing outlet liquid processes recycling flow process
Technical field
The present invention relates to a kind of fracturing outlet liquid and process recycling flow process, belong to the water treatment field of oil-gas field development.
Background technology
Cluster well transformation the most both at home and abroad all has been enter into the large-scale development stage, from initial " two sisters " on Oil/gas Well Cluster well is to " 14 sisters " cluster well, and from clump formula straight well (inclined shaft) to cluster horizontal well, cluster well quantity increases year by year, transformation Scale increases the most year by year.Further, since large quantities of hypotonic Oil in Super-low Permeability Reservoirs enter scale development stage, fractured horizontal well and volume pressure Split the agent technology being increasingly becoming oil-gas field development, but along with the expansion of transformation scale, the quantity returning discharge opeing after pressure is also anxious Increase severely big.According to statistics, the Changqing oilfields fracturing outlet liquid amount of nearly 3 years is about 72.64,128.39,1,800,000 tons.
Processing mode currently for fracturing fluid recovery (backflow) liquid has two kinds, a kind of be take with water-tank lorry be transported to specify useless Water station carries out concentrating purified treatment, then re-injection or discharge;Another kind is the collection using at the construction field (site) and digging blowdown hole paving antiseepage film Middle process, does not only take up substantial amounts of soil, and the pollution to environment can not thoroughly solve.
Summary of the invention
In order to overcome fracturing outlet liquid cannot the technical barrier of online recycling recycling, pollute environment and relatively costly, with It is the longest that past fracturing outlet liquid processes technique, and processing equipment and storage tank take up an area big problem, and the present invention provides a kind of pressure break Return discharge opeing and process recycling flow process.
A kind of fracturing outlet liquid process recycling flow process be carry out fracturing outlet liquid separating, filter after, then reconfigure The fracturing fluid of Cheng Xin, it is achieved the process recycling of fracturing outlet liquid.Flow can be processed reach pressure with online treatment fracturing outlet liquid Split the traffic requirement of open flow discharge opeing, quickly process (the lowest 60m for the treatment of capacity3/ h), next lamination that can be used for very moment well splits, and accounts for Ground is little, it is not necessary to storage reaction pond etc., reuses water resource, reduces environmental pollution.
The technical solution used in the present invention is:
A kind of fracturing outlet liquid processes recycling flow process, specifically comprises the following steps that
1) after natural gas well pressing crack construction terminates, the fracturing outlet liquid that well head open flow goes out through high pressure cyclone depassing unit, Gas in fracturing outlet liquid is separated to gas transmission line, liquid and Selid propping agent mixed liquor are separated;
2) by step 1) through separation after mixed liquor through low voltage three-phase segregation apparatus, by the gas in mixed liquor, liquid Body and Selid propping agent separate, and gas separates to gas transmission line, and Selid propping agent collects container collection by proppant;
3) by step 2) in isolated liquid send into fine filtration device, through coarse filtration and finly filtration, reduce the row of returning The content of float in liquid so that it is content is not higher than 200mg/L;
4) by step 3) through fine filtration device process after fracturing outlet liquid be sent to fracturing outlet liquid holding vessel In, through detector detection pH value and liquid viscosity, when pH value > 5 time, add pH adjusting agent so that pH value≤5, liquid PH value be adjusted to pH value≤5 after, by inject adding set to return discharge opeing holding vessel supplement weight ratio be 3 ‰ add water quality adjust Joint agent, and inject thickening agent so that it is viscosity increases to more than 30mPa s;
5) it is sent in fracturing fluid holding vessel store by the mixing liquid obtained through step 4).
In described step 1) through high pressure cyclone depassing unit process after liquid and Selid propping agent mixed liquor through celebrating a festival Stream blood pressure lowering manifold blood pressure lowering, is re-fed into after being controlled within 2MPa by the pressure of mixed liquor in low voltage three-phase segregation apparatus.
First the fracturing outlet liquid that described well head open flow goes out branch can also be stored into and return in discharge opeing temporary storage tank, is then fed into To low voltage three-phase segregation apparatus.
Described Selid propping agent is quartz sand or haydite.
The invention have the benefit that
(1) this cover system can realize online treatment and the recycling of fracturing outlet liquid, and treating capacity is not less than 60m3/h, Oil/gas Well open flow discharge opeing requirement can be met.
(2) return discharge opeing recovery system and there is execute-in-place simply, return discharge opeing organic efficiency high, the advantage of reusable edible.
(3) return discharge opeing recovery and processing system and can reduce fracturing fluid discharging of waste liquid, save water blanket, by the row of returning of 65-85% Rate, recovery return discharge opeing for the dosing water constructed again, shorten construction period, monolayer shortens about 1 day engineering time.
It is described in detail below with reference to accompanying drawing.
Accompanying drawing explanation
Fig. 1 one fracturing outlet liquid processes recycling flow process.
In figure, reference: 1, well head;2, high pressure cyclone depassing unit;3, reducing pressure by regulating flow manifold;4, low voltage three-phase separates Device;5, fine filtration device;6, fracturing outlet liquid holding vessel;7, fracturing fluid holding vessel;8, discharge opeing temporary storage tank is returned;9, appendix Line;10, container collected by proppant;11, adding set is injected;12, detector.
Detailed description of the invention
Embodiment 1:
In order to overcome fracturing outlet liquid cannot the technical barrier of online recycling recycling, pollute environment and relatively costly, with It is the longest that past fracturing outlet liquid processes technique, and processing equipment and storage tank take up an area big problem, and the present invention provides a kind of pressure break Returning discharge opeing and process recycling flow process, the present invention can realize online treatment and the recycling of fracturing outlet liquid, and treating capacity is the lowest In 60m3/ h, can meet Oil/gas Well open flow discharge opeing requirement.Return discharge opeing recovery system and there is execute-in-place simply, return discharge opeing and reclaim effect Rate is higher than 98%, the advantage of reusable edible.Return discharge opeing recovery and processing system and can reduce fracturing fluid discharging of waste liquid, save pressure break and use Water, shortens construction period, and monolayer shortens about 1 day engineering time.
Device in the present invention is to carry out installing connection by following, and high pressure cyclone depassing unit 2 is by pipeline and well head 1 Connecting, the gas outlet, top of high pressure cyclone depassing unit 2 connects gas gathering pipeline 9, high pressure cyclone depassing unit 2 bottom Outlet is connected with reducing pressure by regulating flow manifold 3, and reducing pressure by regulating flow manifold 3 lower part outlet is connected with low voltage three-phase segregation apparatus 4;Low voltage three-phase The outlet connection of segregation apparatus 4 one end has proppant to collect container 10, low voltage three-phase segregation apparatus 4 upper outlet and gas gathering and transportation Pipeline 9 is connected, and lower part outlet is connected with fine filtration device 5, and described fine filtration device 5 lower part outlet stores up with fracturing outlet liquid Deposit the connection of tank 6 upper entrance;Porch, fracturing outlet liquid holding vessel 6 one end connects has the injection injecting fracturing fluid additive to add Device 11, fracturing outlet liquid holding vessel 6 other end is additionally provided with the detector 12 that detection is analyzed, described fracturing outlet liquid holding vessel 6 lower part outlets connect fracturing fluid holding vessel 7.
A kind of fracturing outlet liquid processes recycling flow process, specifically comprises the following steps that
1), after natural gas well pressing crack construction terminates, the fracturing outlet liquid that well head 1 open flow goes out is through high pressure cyclone depassing unit 2, the gas in fracturing outlet liquid is separated to gas transmission line 9, liquid and Selid propping agent mixed liquor are separated;
2) by step 1) through separation after mixed liquor through low voltage three-phase segregation apparatus 4, by the gas in mixed liquor, liquid Body and Selid propping agent separate, and gas separates to gas transmission line 9, and Selid propping agent is collected container 10 by proppant and received Collection;
3) by step 2) in isolated liquid send into fine filtration device 5, through coarse filtration and finly filtration, reduce the row of returning The content of float in liquid so that it is content is not higher than 200mg/L;
4) fracturing outlet liquid after fine filtration device 5 processes in step 3) is sent to fracturing outlet liquid holding vessel In 6, detect pH value and viscosity through detector 12, when pH value > 5 time, add pH adjusting agent so that pH value≤5, the pH of liquid After value is adjusted to pH value≤5, it is that 3 ‰ interpolation water quality are adjusted by injecting adding set 11 to return discharge opeing holding vessel 6 supplementing weight ratio Joint agent, and inject thickening agent so that it is viscosity increases to more than 30mPa s;
5) it is sent in fracturing fluid holding vessel 7 store by the mixing liquid obtained through step 4).
Described Selid propping agent is quartz sand or haydite.
A kind of fracturing outlet liquid of the present invention processes recycling flow process, by high pressure cyclone desanding device 2, low voltage three-phase Segregation apparatus 4 and 5 three processing modules of fine filtration device are constituted, and each module independently becomes to prize, supporting reducing pressure by regulating flow manifold 3, Proppant is collected container 10, is returned discharge opeing temporary storage tank 8, fracturing outlet liquid storage tank 6, fracturing fluid storage tank 7.According to fracturing outlet liquid Character and Oil/gas Well type are different, packaging technology circuit of arranging in pairs or groups.
Described well head 1 is also associated with returning discharge opeing temporary storage tank 8, described in return the outlet of discharge opeing temporary storage tank 8 and separate with low voltage three-phase The entrance of device 4 connects.
The present invention can realize online treatment and the recycling of fracturing outlet liquid, and treating capacity is not less than 60m3/ h, can be full Foot Oil/gas Well open flow discharge opeing requirement.
Returning discharge opeing recovery system, to have execute-in-place simple, returns discharge opeing organic efficiency higher than 98%, reusable edible excellent Point.
Return discharge opeing recovery and processing system and can reduce fracturing fluid discharging of waste liquid, save water blanket, lead by the row of returning of 65-85%, That reclaims returns discharge opeing for the dosing water constructed again, shortening construction period, monolayer about 1 day engineering time of shortening.
Embodiment 2:
On the basis of embodiment 1,
1), after natural gas well pressing crack construction terminates, the fracturing outlet liquid that well head 1 open flow goes out is through high pressure cyclone depassing unit 2, the gas in fracturing outlet liquid is separated to gas transmission line 9, liquid and Selid propping agent mixed liquor are separated;
2) in step 1) through high pressure cyclone depassing unit 2 process after liquid and Selid propping agent mixed liquor through throttling Blood pressure lowering manifold 3 blood pressure lowering, by fracturing control at 2MPa;
3) by step 2) through separation after mixed liquor through low voltage three-phase segregation apparatus 4, by the gas in mixed liquor, liquid Body and Selid propping agent separate, and gas separates to intake pipeline 9, and Selid propping agent is collected container 10 by proppant and received Collection;
4) isolated liquid in step 3) is sent into fine filtration device 5, through coarse filtration and finly filtration, reduce the row of returning The content of float in liquid so that it is content is not higher than 200mg/L;
5) fracturing outlet liquid after fine filtration device 5 processes in step 4) is sent to fracturing outlet liquid holding vessel In 6, detect pH value and viscosity through detector 12, when pH value > 5 time, add pH adjusting agent so that pH value≤5, the pH of liquid After value is adjusted to pH value≤5, it is that 3 ‰ interpolation water quality are adjusted by injecting adding set 11 to return discharge opeing holding vessel 6 supplementing weight ratio Joint agent, and inject thickening agent so that it is viscosity increases to more than 30mPa s;
6) it is sent in fracturing fluid holding vessel 7 store by the mixing liquid obtained through step 5).
In described step 1) through high pressure cyclone depassing unit 2 process after liquid and Selid propping agent mixed liquor through celebrating a festival Stream blood pressure lowering manifold 3 blood pressure lowering, is re-fed into after being controlled within 2MPa by the pressure of mixed liquor in low voltage three-phase segregation apparatus 4.
The present embodiment increases reducing pressure by regulating flow manifold 3, the impact returning discharge opeing to low voltage three-phase segregation apparatus 4 can be reduced, also Pressure can be controlled so that in the case of 2MPa, carry out subsequent step, protect low voltage three-phase segregation apparatus 4, add the longevity Life.
First the fracturing outlet liquid that described well head 1 open flow goes out branch can also be stored into and return in discharge opeing temporary storage tank 8, then send Enter to low voltage three-phase segregation apparatus 4.
Discharge opeing temporary storage tank 8 is returned in addition can alleviate the impact returning discharge opeing at well head 1 open flow, it is also possible to standby, can be effective Prevent due to open flow excessive velocities, and the problem that gas row is the cleanest.
Embodiment 3:
Using the water conditioner of Hubei Hai Li Environmental Protection Technology Co., Ltd in the present embodiment, water conditioner is mainly removed The part ion impact on fracturing fluid character in water.Water conditioner can be pH adjusting agent, regulates pH value postemphasis proportion so that Final pH value is less than or equal to 5, meets the requirement reconfiguring fracturing fluid.
The fracturing outlet liquid that open flow goes out, has the most had previously been stored in and has returned in the temporary storage tank of discharge opeing 8, reaches to slow down the energy of open flow flow Power, it is also possible to be directly entered low voltage three-phase segregation apparatus 4, carries out separating air-liquid and Selid propping agent.
The process flow of the present invention: gas well returns discharge opeing disposal ability 4m3/ min, gas 20 × 104m3/d;Liquids recovery rate 99%, gas-liquid separation rate 99%, separate desanding rate 99%;Oil well returns discharge opeing disposal ability 3m3/ min, liquids recovery rate 99%, separate Desanding rate 99%;Return discharge opeing suspension content and be not higher than 200mg/L.
Fine filtration device 5 returns discharge opeing suspension content after processing and is not higher than 200mg/L.
This cover system can realize online treatment and the recycling of fracturing outlet liquid, and treating capacity is not less than 60m3/ h, energy Meet Oil/gas Well open flow discharge opeing requirement.
Returning discharge opeing recovery system, to have execute-in-place simple, returns discharge opeing organic efficiency higher than 98%, reusable edible excellent Point.
Return discharge opeing recovery and processing system and can reduce fracturing fluid discharging of waste liquid, save water blanket, lead by the row of returning of 65-85%, That reclaims returns discharge opeing for the dosing water constructed again, shortening construction period, monolayer about 1 day engineering time of shortening.
Low voltage three-phase segregation apparatus 4 in above-described embodiment is three phase separator, and high pressure cyclone depassing unit 2 is degasification Device, fine filtration device 5 are fine filter, inject adding set and use technology known to this.The present embodiment is chatted the most in detail The parts stated and structure belong to the well-known components of the industry and common structure or conventional means, describe the most one by one.
Exemplified as above is only the illustration to the present invention, is not intended that the restriction to protection scope of the present invention, all It is within design same or analogous with the present invention belongs to protection scope of the present invention.

Claims (4)

1. fracturing outlet liquid processes a recycling flow process, specifically comprises the following steps that
1), after natural gas well pressing crack construction terminates, the fracturing outlet liquid that well head (1) open flow goes out is through high pressure cyclone depassing unit (2), the gas in fracturing outlet liquid is separated to gas transmission line (9), liquid and Selid propping agent mixed liquor are separated;
2) by step 1) through separation after mixed liquor through low voltage three-phase segregation apparatus (4), by the gas in mixed liquor, liquid And Selid propping agent separates, gas separates to gas transmission line (9), and Selid propping agent collects container (10) by proppant Collect;
3) by step 2) in isolated liquid send into fine filtration device (5), through coarse filtration and finly filtration, reduce and return discharge opeing The content of middle float so that it is content is not higher than 200mg/L;
4) by step 3) through fine filtration device (5) process after fracturing outlet liquid be sent to fracturing outlet liquid holding vessel (6) in, through detector (12) detection pH value and viscosity, when pH value > 5 time, add pH adjusting agent so that pH value≤5, liquid PH value be adjusted to pH value≤5 after, be 3 ‰ to add by injecting adding set (11) to return discharge opeing holding vessel (6) supplementing weight ratio Add water conditioner, and inject thickening agent so that it is viscosity increases to more than 30mPa s;
5) it is sent to the mixing liquid obtained through step 4) in fracturing fluid holding vessel (7) store.
A kind of fracturing outlet liquid the most according to claim 1 processes recycling flow process, it is characterised in that: in described step 1) Through high pressure cyclone depassing unit (2) process after liquid and Selid propping agent mixed liquor through reducing pressure by regulating flow manifold (3) blood pressure lowering, It is re-fed into after the pressure of mixed liquor is controlled within 2MPa in low voltage three-phase segregation apparatus (4).
A kind of fracturing outlet liquid the most according to claim 1 processes recycling flow process, it is characterised in that: described well head (1) The fracturing outlet liquid that open flow goes out when instantaneous delivery more than flow processing ability time, it is also possible to first branch be stored into return discharge opeing keep in In tank (8), it is then fed into low voltage three-phase segregation apparatus (4).
A kind of fracturing outlet liquid the most according to claim 1 processes recycling flow process, it is characterised in that: described solid support Agent is quartz sand or haydite.
CN201410845813.0A 2014-12-31 2014-12-31 A kind of fracturing outlet liquid processes recycling flow process Active CN104649471B (en)

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CN107176731A (en) * 2016-03-09 2017-09-19 中国石油化工股份有限公司 Fracturing outlet liquid processing unit and method
CN107840481A (en) * 2017-09-29 2018-03-27 中国石油天然气股份有限公司 A kind of recovery processing process for fracturing return liquid
CN108975535B (en) * 2018-07-27 2019-05-28 中国石油大学(北京) The recovery system and method that test is split in row pressure are returned for shale gas
CN109267986A (en) * 2018-09-30 2019-01-25 中国石油天然气股份有限公司 A kind of anhydrous pressure break liquid device of lower carbon number hydrocarbons and fracturing process
CN114622887A (en) * 2022-02-10 2022-06-14 中国石油化工集团有限公司 Single-well zipper-type fracturing gas testing construction method

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US7699994B2 (en) * 2007-08-02 2010-04-20 Ecosphere Technologies, Inc. Enhanced water treatment for reclamation of waste fluids and increased efficiency treatment of potable waters
CN102992524B (en) * 2012-04-23 2014-12-17 北京矿冶研究总院 Treatment method of fracturing flow-back fluid
CN203683451U (en) * 2014-02-12 2014-07-02 四川锦矗高乐油气科技有限责任公司 Fracturing fluid recycling system
CN104069678B (en) * 2014-06-23 2015-09-16 中国石油集团川庆钻探工程有限公司工程技术研究院 A kind of fracturing fluid recovery is box carries slotting desanding method

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