CN104591766B - A kind of wear-resistant ceramic material and preparation method thereof - Google Patents
A kind of wear-resistant ceramic material and preparation method thereof Download PDFInfo
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- CN104591766B CN104591766B CN201510012947.9A CN201510012947A CN104591766B CN 104591766 B CN104591766 B CN 104591766B CN 201510012947 A CN201510012947 A CN 201510012947A CN 104591766 B CN104591766 B CN 104591766B
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Abstract
The invention discloses a kind of wear-resistant ceramic material and preparation method thereof, this wear-resistant ceramic material, is made up of the component comprising following weight portion: nano-aluminium oxide 65 70 parts, 10 15 parts of magnesium carbonate, kaolin 10 12 parts, titanium diboride fiber 5 12 parts, 58 parts of carborundum, sodium acid carbonate 35 parts, antimony oxide 57 parts and 35 parts of red soil.Present invention also offers the preparation method of a kind of wear-resistant ceramic material, the method comprises the following steps: (1) weighs 10 15 parts of magnesium carbonate, kaolin 10 12 parts, titanium diboride fiber 5 12 parts, 58 parts of carborundum, sodium acid carbonate 35 parts, antimony oxide 57 parts and 35 parts of red soil, adds in high pressure homogenizer and mixes；(2) by the product of step 1, add the nano-aluminium oxide 65 70 parts of abundant ball milling under an inert atmosphere, be warming up to 700 710 DEG C, react 12 hours；(3) by compressing for the product of step 2, it is heated to 1,300 1350 DEG C with the heating rate of 5 DEG C/min and burns till, be incubated 24 hours, after cooling, prepare wear-resistant ceramic material.
Description
Technical field
The invention belongs to ceramic material field, particularly to a kind of wear-resistant ceramic material and preparation method thereof.
Background technology
Wear-resistant ceramic is with Al2O3For primary raw material, add various ingredients, through the extraordinary corundum ceramic of high-temperature roasting,
The product combined with the organic/inorganic adhesive of specific rubber and high intensity the most respectively.
The ceramic material utilizing the pottery specific function with the physical properties such as sound, optical, electrical, magnetic, heat and manufacture claims
For function ceramics.Function ceramics is of a great variety, and purposes is different.Such as, can be made into conduction pottery according to the difference of pottery electrical properties
The electronic materials such as porcelain, semiconductive ceramic, dielectric ceramic, insulating ceramics.The optical property utilizing pottery can manufacture Solid State Laser material
Material, optical fiber, optical storage material and various ceramic sensor element.
Each ceramic material has the merits and demerits of himself, it is therefore necessary to the condition used for pottery is filled
The analysis divided and research.Affect the principal element of ceramic performance have use temperature range and change, corrosive medium, stressing conditions,
Grit collision incidence angle and Particle Erosion intensity.When use condition is unsatisfactory for, pottery will be unable to reach intended and uses effect
Really.
Summary of the invention
For above-mentioned demand, invention especially provides a kind of wear-resistant ceramic material and preparation method thereof.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of wear-resistant ceramic material, is made up of the component comprising following weight portion:
Nano-aluminium oxide 65-70 part,
Magnesium carbonate 10-15 part,
Kaolin 10-12 part,
Titanium diboride fiber 5-12 part,
Carborundum 5-8 part,
Sodium acid carbonate 3-5 part,
Antimony oxide 5-7 part,
Red soil 3-5 part.
The particle diameter of described nano-aluminium oxide is 45-50 nanometer.
A diameter of 10-15 micron of described titanium diboride fiber.
Described titanium diboride fiber is 8-10 weight portion.
A kind of preparation method of wear-resistant ceramic material, the method comprises the following steps:
(1) magnesium carbonate 10-15 part, kaolin 10-12 part, titanium diboride fiber 5-12 part, carborundum 5-8 part, carbon are weighed
Acid hydrogen sodium 3-5 part, antimony oxide 5-7 part and red soil 3-5 part, add in high pressure homogenizer and mix；
(2) by the product of step 1, add nano-aluminium oxide 65-70 part of abundant ball milling under an inert atmosphere, heat up
To 700-710 DEG C, react 1-2 hour；
(3) by compressing for the product of step 2, it is heated to 1300-1350 DEG C with the heating rate of 5 DEG C/min and burns till,
It is incubated 2-4 hour, after cooling, prepares wear-resistant ceramic material.
The pressure of high pressure homogenizer described in step 1 is 20.5-21Mpa.
Compared with prior art, it has the beneficial effect that the present invention
(1) wear-resistant ceramic material that the present invention prepares has good mechanical property, good anti-wear performance and uses the longevity
The feature that life is long.
(2) wear-resistant ceramic material that the present invention prepares remains to keep good stability and resistance to different use in environment
Hou Xing.
(3) wear-resistant ceramic material of the present invention, its preparation method is simple, it is easy to industrialized production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) weigh magnesium carbonate 10kg, kaolin 10kg, the titanium diboride fiber 5kg of a diameter of 10 microns, carborundum 5kg,
Sodium acid carbonate 4kg, antimony oxide 6kg and red soil 3kg, add in high pressure homogenizer, mix under 20.5Mpa；
(2) by the product of step 1, the alundum (Al2O3) that particle diameter is 45 nanometers of abundant ball milling is added under an inert atmosphere
65kg, is warming up to 700 DEG C, reacts 1 hour；
(3) by compressing for the product of step 2, it is heated to 1350 DEG C with the heating rate of 5 DEG C/min and burns till, be incubated 2
Hour, after cooling, prepare wear-resistant ceramic material.
The performance test results preparing wear-resistant ceramic material is as shown in table 1.
Embodiment 2
(1) weigh magnesium carbonate 15kg, kaolin 11kg, the titanium diboride fiber 8kg of a diameter of 15 microns, carborundum 8kg,
Sodium acid carbonate 3kg, antimony oxide 7kg and red soil 5kg, add in high pressure homogenizer, mix under 21Mpa；
(2) by the product of step 1, the alundum (Al2O3) that particle diameter is 50 nanometers of abundant ball milling is added under an inert atmosphere
70kg, is warming up to 705 DEG C, reacts 2 hours；
(3) by compressing for the product of step 2, it is heated to 1350 DEG C with the heating rate of 5 DEG C/min and burns till, be incubated 2
Hour, after cooling, prepare wear-resistant ceramic material.
The performance test results preparing wear-resistant ceramic material is as shown in table 1.
Embodiment 3
(1) magnesium carbonate 12kg, kaolin 12kg, the titanium diboride fiber 12kg of a diameter of 12 microns, carborundum are weighed
6kg, sodium acid carbonate 5kg, antimony oxide 5kg and red soil 4kg, add in high pressure homogenizer, mix under 20.5Mpa；
(2) by the product of step 1, the alundum (Al2O3) that particle diameter is 45 nanometers of abundant ball milling is added under an inert atmosphere
65kg, is warming up to 710 DEG C, reacts 1 hour；
(3) by compressing for the product of step 2, it is heated to 1350 DEG C with the heating rate of 5 DEG C/min and burns till, be incubated 2
Hour, after cooling, prepare wear-resistant ceramic material.
The performance test results preparing wear-resistant ceramic material is as shown in table 1.
Embodiment 4
(1) weigh magnesium carbonate 15kg, kaolin 10kg, the titanium diboride fiber 5kg of a diameter of 13 microns, carborundum 5kg,
Sodium acid carbonate 3kg, antimony oxide 5kg and red soil 5 kg, add in high pressure homogenizer, mix under 21Mpa；
(2) by the product of step 1, the alundum (Al2O3) that particle diameter is 45 nanometers of abundant ball milling is added under an inert atmosphere
65kg, is warming up to 700 DEG C, reacts 2 hours；
(3) by compressing for the product of step 2, it is heated to 1300 DEG C with the heating rate of 5 DEG C/min and burns till, be incubated 4
Hour, after cooling, prepare wear-resistant ceramic material.
The performance test results preparing wear-resistant ceramic material is as shown in table 1.
Table 1
| Test event | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Conductance (%IACS) | 83.6 | 81.4 | 85.3 | 81.6 |
| Pencil hardness (level) | 2H | H+ | 2H | H |
The invention is not restricted to embodiment here, those skilled in the art are according to the announcement of the present invention, without departing from the present invention
Improvement and amendment that category is made all should be within protection scope of the present invention.
Claims (6)
1. a wear-resistant ceramic material, it is characterised in that be made up of the component comprising following weight portion:
Nano-aluminium oxide 65-70 part,
Magnesium carbonate 10-15 part,
Kaolin 10-12 part,
Titanium diboride fiber 5-12 part,
Carborundum 5-8 part,
Sodium acid carbonate 3-5 part,
Antimony oxide 5-7 part,
Red soil 3-5 part.
Wear-resistant ceramic material the most according to claim 1, it is characterised in that the particle diameter of described nano-aluminium oxide is 45-
50 nanometers.
Wear-resistant ceramic material the most according to claim 1, it is characterised in that a diameter of 10-15 of described titanium diboride fiber
Micron.
Wear-resistant ceramic material the most according to claim 1, it is characterised in that described titanium diboride fiber is 8-10 weight portion.
5. the preparation method of a wear-resistant ceramic material, it is characterised in that the method comprises the following steps:
(1) magnesium carbonate 10-15 part of weight portion, kaolin 10-12 part, titanium diboride fiber 5-12 part, carborundum 5-8 are weighed
Part, sodium acid carbonate 3-5 part, antimony oxide 5-7 part and red soil 3-5 part, add in high pressure homogenizer and mix；
(2) by the product of step 1, add nano-aluminium oxide 65-70 part of abundant ball milling under an inert atmosphere, be warming up to
700-710 DEG C, react 1-2 hour；
(3) by compressing for the product of step 2, it is heated to 1300-1350 DEG C with the heating rate of 5 DEG C/min and burns till, insulation
2-4 hour, after cooling, prepare wear-resistant ceramic material.
The preparation method of wear-resistant ceramic material the most according to claim 5, it is characterised in that described in step 1, high pressure is equal
The pressure of matter machine is 20.5-21MPa.
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| CN105236939A (en) * | 2015-09-01 | 2016-01-13 | 广西南宁智翠科技咨询有限公司 | High-hardness wear-resistance aluminum oxide ceramic and preparation method of same |
| CN105174921A (en) * | 2015-09-15 | 2015-12-23 | 苏州亿馨源光电科技有限公司 | Heat-resisting conductive ceramic material and preparation method thereof |
| CN107032751A (en) * | 2016-11-21 | 2017-08-11 | 郑州诚合信息技术有限公司 | A kind of cermet material and preparation method thereof |
| CN106518123A (en) * | 2016-11-21 | 2017-03-22 | 郑州诚合信息技术有限公司 | Metal special ceramic material and preparation method thereof |
| CN107010921A (en) * | 2017-05-24 | 2017-08-04 | 佛山市蓝瑞欧特信息服务有限公司 | A kind of composite ceramic material |
| CN107663098A (en) * | 2017-09-30 | 2018-02-06 | 徐州金盟新型建材有限公司 | A kind of wear-resistant ceramic material |
| CN108218459A (en) * | 2018-03-22 | 2018-06-29 | 湖南工程学院 | A kind of Pottery Art of Life product and preparation method thereof |
| CN109294063B (en) * | 2018-09-20 | 2020-05-29 | 安徽江淮汽车集团股份有限公司 | Wear-resistant filler and preparation method thereof |
| CN112573910A (en) * | 2020-12-16 | 2021-03-30 | 徐州亚苏尔高新材料有限公司 | Wear-resistant quartz ceramic material and preparation method thereof |
| CN112811889A (en) * | 2021-03-02 | 2021-05-18 | 徐州亚苏尔高新材料有限公司 | Wear-resistant ceramic roller and preparation method thereof |
| CN113264778B (en) * | 2021-05-17 | 2022-10-14 | 厦门理工学院 | Boron nitride composite ceramic and preparation method and application thereof |
| CN114437574A (en) * | 2022-03-04 | 2022-05-06 | 锦益得节能环保科技(山东)有限公司 | Inorganic flame-retardant heat-insulating coating for interior wall |
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| CN101696112B (en) * | 2009-10-30 | 2011-10-26 | 蓝辉 | Method for preparing medium and high-aluminum abrasion-resistant ceramic product by using rolling rod waste |
| CN103482922B (en) * | 2013-09-29 | 2015-01-07 | 曾琼 | Wear-resistant ceramic paint and preparation method |
| CN103964794B (en) * | 2014-04-25 | 2015-06-17 | 焦作安泰新型耐磨材料有限公司 | Nano-enhanced wear-resistant corrosion-protection ceramic material, and preparation method and use method thereof |
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