CN104586653B - Shampoo used also as bath lotion suitable for infant and preparation method thereof - Google Patents
Shampoo used also as bath lotion suitable for infant and preparation method thereof Download PDFInfo
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- CN104586653B CN104586653B CN201510081785.4A CN201510081785A CN104586653B CN 104586653 B CN104586653 B CN 104586653B CN 201510081785 A CN201510081785 A CN 201510081785A CN 104586653 B CN104586653 B CN 104586653B
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Abstract
The invention discloses a kind of suitable for shampoo used also as bath lotion of infant and preparation method thereof.Described shampoo used also as bath lotion contains the compositions such as the esters of caprylic/capric glyceride type polyglycereol 10, lauryl glucoside, the distearates of PEG 150, laureth sodium sulfovinate, Cocoamidopropyl betaine, cocoyl glucoside/glyceryl oleate, its property is gentle, it is nonirritant, and dioxane equivalent risk material will not be produced, it is particularly suitable for the use of infant.
Description
Technical field
It is more particularly to a kind of suitable for infant, nothing the present invention relates to a kind of shampoo used also as bath lotion and preparation method thereof
Irritating shampoo used also as bath lotion and preparation method thereof.
Background technology
The skin of infant triggers disease of skin than adult's exquisiteness, easily stimulated, infection.Therefore, infant
Hair washing, shower class product, the control to excitant, specified risk material require more strict.
Traditional infant's shampoo used also as bath lotion, generally using sodium lauroyl sarcosine, PEG-80 anhydrous sorbitol bays
Acid esters, laureth sodium sulfovinate, laureth sulfosuccinate disodium, Cocoamidopropyl betaine, lauryl
Glucoside, methylisothiazolinone, methylchloroisothiazandnone, DMDMH etc. are used as primary raw material.Wherein, lauroyl
Sodium sarcosinate, PEG-80 anhydrous sorbitols laurate, laureth sodium sulfovinate are main surfactant, with good
Good foaming is removed contamination performance, but sodium lauroyl sarcosine, laureth sodium sulfovinate are larger to the excitant of eyes, and PEG-
80 anhydrous sorbitol laurates can remain specified risk material dioxane in process of production.Methylisothiazolinone, methyl chloride are different
Thiazolinone, DMDMH the experiment proved that methylisothiazolinone, methylchloroisothiazandnone have as preservative
There are cytotoxicity and neurotoxicity, and DMDMH understands release formaldehyde equivalent risk material, easily causes skin irritation.Cause
This, traditional infant's shampoo used also as bath lotion, the problem of having that excitant is big, easily produce dioxane, formaldehyde equivalent risk material,
It is not suitable for the long-term use of infant.
The content of the invention
Based on this, it is an object of the present invention to provide a kind of shampoo used also as bath lotion suitable for infant, it is without skin irritatin
It is property, good without eye irritation, cleanliness factor, and dioxane equivalent risk material will not be produced.
It is a further object of the invention to provide the preparation method of the shampoo used also as bath lotion.
A kind of shampoo used also as bath lotion, by weight percentage including following component：
And the purified water of its surplus.
In one of the embodiments, one kind in cocoyl glucoside, glyceryl oleate of described tax fat agent or
Two kinds of combination.
In one of the embodiments, described preservative is selected from one or both of Phenoxyethanol, methyl hydroxybenzoate
Combination.
In one of the embodiments, described anti-corrosion synergist is selected from the smooth caprylate of sorb.
In one of the embodiments, described complexing agent is selected from one or both of EDETATE SODIUM, the sodium of EDTA tetra-
Combination.
In one of the embodiments, described pH adjusting agent in citric acid, lactic acid, butanedioic acid, anisic acid one
Plant or two or more mixing.
The preparation method of shampoo used also as bath lotion of the present invention, comprises the following steps：Caprylic/capric glyceride is birdsed of the same feather flock together sweet
Oily -10 esters, lauryl glucoside, laureth sodium sulfovinate, Cocoamidopropyl betaine, PEG-150 distearyls acid
Ester, the agent of tax fat, complexing agent, pH adjusting agent, preservative, anti-corrosion synergist are added in purified water, and being heated with stirring to 90~100 DEG C makes
Be completely dissolved, insulated and stirred 10~20 minutes is cooled to 40~45 DEG C；Then essence is added, is stirred, 38 DEG C are cooled to
Hereinafter, discharge, obtain described shampoo used also as bath lotion.
Shampoo used also as bath lotion of the present invention has property gentle, good etc. without skin irritation, without eye irritation, cleanliness factor
Advantage, and dioxane, formaldehyde, phenol equivalent risk material will not be produced, it is applicable to the long-term use of infant.
In shampoo used also as bath lotion of the present invention, caprylic/capric glyceride type Natrulon H-10 esters, lauryl glucoside
For principal surfactant, laureth sodium sulfovinate, Cocoamidopropyl betaine are cosurfactant, and it coordinates
Use, the excitant of formula can be significantly reduced, and optimal collaboration can be formed in terms of detergency, cleanliness factor, foaming characteristic
Effect.
Shampoo used also as bath lotion of the present invention, using caprylic/capric glyceride type Natrulon H-10 esters, instead of tradition
Conventional use of PEG-80 anhydrous sorbitols laurate in infant's shampoo used also as bath lotion, it is to avoid drawing for specified risk material dioxane
Enter.Caprylic/capric glyceride type Natrulon H-10 esters are the surfactant of natural origin, and its property is gentle, safe, stingless
Swash property, and dioxanes equivalent risk material will not be produced；Anion surfactant is combined with laureth sodium sulfovinate etc. for it
In use, the excitant of anion surfactant can also be significantly reduced, it is thus possible to prepare nonirritant hair washing and take a shower
Dew.
Shampoo used also as bath lotion of the present invention, using PEG-150 distearates as thickener, to the table in this formula
Face activating agent has good thickening power, and denseness will not produce significant change with temperature, can prevent in microthermal climate (10
Below DEG C) there is " jelly " phenomenon.
Shampoo used also as bath lotion of the present invention, using cocoyl glucoside, glyceryl oleate as fat agent is assigned, after cleaning
Give skin appropriate grease, it is to avoid to produce tight feeling after skin cleaning, and the normal barrier function after skin cleaning can be maintained.
Shampoo used also as bath lotion of the present invention, using Phenoxyethanol, methyl hydroxybenzoate as preservative, while it is smooth to add sorb
Caprylate is as anti-corrosion synergist, and its property is gentle, safety, will not also produce phenol, dioxane equivalent risk materials, will not discharge
Formaldehyde, and three uses cooperatively, and can produce optimal collaboration antiseptic effect, so that the consumption of preservative is reduced, reduction formula
Excitant.
Embodiment
Embodiment one：The preparation of shampoo used also as bath lotion of the present invention
According to the formula shown in table 1 below, each component is weighed respectively.
Table 1
| Composition | Consumption |
| Caprylic/capric glyceride type Natrulon H-10 esters | 5.6g |
| Lauryl glucoside | 5.0g |
| Laureth sodium sulfovinate | 2.5g |
| Cocoamidopropyl betaine | 2.0g |
| PEG-150 distearates | 2.3g |
| Cocoyl glucoside | 0.4g |
| Glyceryl oleate | 0.4g |
| EDETATE SODIUM | 0.05g |
| Citric acid | 0.05g |
| Phenoxyethanol | 0.5g |
| Methyl hydroxybenzoate | 0.2g |
| The smooth caprylate of sorb | 0.3g |
| Essence | 0.2g |
| Purified water | Add to 100g |
By caprylic/capric glyceride type Natrulon H-10 esters, lauryl glucoside, laureth sodium sulfovinate, cocounut oil
Amido propyl betaine, PEG-150 distearates, cocoyl glucoside, glyceryl oleate, EDETATE SODIUM, citric acid, benzene oxygen
The smooth caprylate of ethanol, methyl hydroxybenzoate, sorb is added in purified water, is heated with stirring to 95 DEG C and is allowed to be completely dissolved, insulated and stirred 15
Minute, it is cooled to 45 DEG C；Then essence is added, is stirred, less than 38 DEG C are cooled to, discharging obtains of the present invention wash
Send out shower cream.
Embodiment two：The preparation of traditional infant's shampoo used also as bath lotion
According to the formula shown in table 2 below, each component is weighed respectively.
Table 2
| Composition | Consumption |
| Sodium lauroyl sarcosine | 5.0g |
| PEG-80 anhydrous sorbitol laurates | 3.0g |
| Laureth sodium sulfovinate | 3.0g |
| Laureth sulfosuccinate disodium | 3.0g |
| Cocoamidopropyl betaine | 3.0g |
| Lauryl glucoside | 2.0g |
| EDETATE SODIUM | 0.05g |
| Methylisothiazolinone | 0.002g |
| Methylchloroisothiazandnone | 0.006g |
| DMDMH | 0.3g |
| Essence | 0.2g |
| Purified water | Add to 100g |
Sodium lauroyl sarcosine, PEG-80 anhydrous sorbitols laurate, laureth sodium sulfovinate, laruyl alcohol are gathered
Ether sulfosuccinates disodium, Cocoamidopropyl betaine, lauryl glucoside, EDETATE SODIUM are added in purified water, stirring
It is heated to 95 DEG C to be allowed to be completely dissolved, insulated and stirred 15 minutes；45 DEG C are cooled to, methylisothiazolinone, methyl is then added
Chloroisothiazole quinoline ketone, DMDMH and essence, stir, and are cooled to less than 38 DEG C, discharging obtains traditional infant
Use shampoo used also as bath lotion.
Embodiment three：Acute eye irritation and acute skin irritation experiment
1st, acute ocular irritation test
From rabbit as animal subject, acute ocular irritation test is carried out.Used in 24 hours before on-test
Fluorescein sodium checks that two eyes tested with rabbit the rabbit of passed examination is used to test.Wherein, sample sets are used
Shampoo used also as bath lotion prepared by embodiment one is as tested material, and traditional infant that control group is prepared using embodiment two is washed one's hair with hair washing
Bath lotion is as tested material, and every group is selected the rabbit of 3 passed examinations as animal subject.
0.1g tested materials are instilled in the conjunctival sac of one eye of rabbit respectively, make palpebra inferior passively closure 1 second, to the
At 30 seconds, 30 seconds (controlling flow rate of water flow in order to avoid causing rabbit eye injury) is rinsed with enough, quick current, another eyes are not
Handle to make own control.
Instill tested material the 1st, 24,48,72 hours and the 4th day, the 7th day, respectively with handheld slit lamp to rabbit
Eyes checked, record ocular damage situation, according to《Cosmetics health specification》(version in 2007) Part II Section 5
Eye infringement standards of grading in acute ocular irritation test, the integration of record eye irritation reaction；According to the 24th, 48,72 hours
The top of record and recovery time, according to《Cosmetics health specification》(version in 2007) Part II Section 5 acute ocular is pierced
Swash the eye irritation reaction classification in property experiment, judge stimulus intensity of the tested material to rabbit eyes.After inspection terminates, respectively
The eyes of rabbit are checked with fluorescein sodium.Result of the test is as shown in table 3.
Table 3
The result of the test of table 3 shows：Result of the shampoo used also as bath lotion (sample sets) of the present invention to rabbit eyes irritant test
It is nonirritant；And traditional infant of embodiment two is with result of the shampoo used also as bath lotion (control group) to rabbit eyes irritant test
It is excitant.
2nd, acute skin irritation is tested
From rabbit as animal subject, acute skin irritation experiment is carried out.Sample sets are prepared using embodiment one
Shampoo used also as bath lotion is as tested material, and traditional infant that control group is prepared using embodiment two is with shampoo used also as bath lotion as tested
Thing.Test method, judgment criteria according to《Cosmetics health specification》The relevant rule of (2007 editions) skin irritation/corrosion test
It is fixed.Result of the test is as shown in table 4.
Table 4
The result of the test of table 4 shows：The shampoo used also as bath lotion (sample sets) of the present invention is to Rabbits with Acute Skin Irritation Test
Result is nonirritant, and traditional infant of embodiment two is tried Rabbits with Acute skin irritatin with shampoo used also as bath lotion (control group)
The result tested is subexcite.
Example IV：The excitant of surfactant, toxicity test
1st, skin irritation test
A piece of intact region is selected in healthy human body arm, it is 10% to dip mass concentration respectively with cotton of the same size
Laureth sodium sulfovinate (AES) solution, Cocoamidopropyl betaine (CAB) solution, lauryl glucoside (APG) it is molten
Liquid, caprylic/capric glyceride type Natrulon H-10 esters (CGPE10) solution and purified water, are applied on arm skin respectively, use
Adhesive plaster is pasted.Adhesive plaster is removed after 24 hours, observes and records experiment skin and recover to the time with surrounding skin solid colour.Examination
Test result as shown in table 5.
Table 5
| Group | The time required to skin recovers normal |
| 10%AES | 12 hours |
| 10%CAB | 6.5 hour |
| 10%APG | 3 hours |
| 10%CGPE10 | 2.5 hour |
| Purified water | 2 hours |
The result of the test of table 5 shows that the excitant size order of surfactant is：Laureth sodium sulfovinate is (cloudy
Ionic surface active agent) ＞ Cocoamidopropyl betaines (amphoteric surfactant) ＞ lauryl glucoside (non-ionic surfaces
Activating agent) ＞ caprylic/capric glyceride type Natrulon H-10 esters (nonionic surfactant).With the result of the test of purified water
Contrast, shows that the excitant of caprylic/capric glyceride type Natrulon H-10 esters and lauryl glucoside is low.
Laureth sodium sulfovinate, Cocoamidopropyl betaine have the advantages that foaming characteristic is good, strong detergency, but deposit
In the big shortcoming of excitant.The shampoo used also as bath lotion of the present invention, using caprylic/capric glyceride type Natrulon H-10 esters, lauryl
Glucoside combines compounding with laureth sodium sulfovinate, Cocoamidopropyl betaine, in guarantee foaming characteristic, the base of detergency
On plinth, the excitant of surfactant system can be integrally reduced.
2nd, cell toxicity test
Caprylic/capric glyceride type Natrulon H-10 esters (CGPE10), laureth sulfuric ester are determined using mtt assay
The cytotoxicity of sodium (AES).The caprylic/capric glyceride type Natrulon H-10 esters of different quality concentration and laureth sulphur
Cell survival rate when acid esters sodium is used in combination is as shown in table 6 below.
Table 6
| Group | Cell survival rate |
| 5%AES | 21.5% |
| 5%AES+1%CGPE10 | 51.7% |
| 5%AES+3%CGPE10 | 78.2% |
| 5%AES+5%CGPE10 | 97.3% |
| 5%CGPE10 | 98.7% |
| Purified water | 100% |
The result of the test of table 6 shows：The excitant of caprylic/capric glyceride type Natrulon H-10 esters is extremely low, and itself and the moon
When laureth sodium sulfovinate is used in combination, the excitant of laureth sodium sulfovinate can be also significantly decreased, is existed mutually
Cooperate with facilitation.
Embodiment five：Specified risk material is tested
According to SN/T 1784-2006《Import and export the measure gas-chromatography tandem mass spectrum of dioxanes residual quantity in cosmetics
Method》Standard, respectively determine embodiment one, embodiment two prepare shampoo used also as bath lotion in dioxane contents.According to《Cosmetics
Hygienic practice》Method as defined in (2007 editions), determines the phenol in shampoo used also as bath lotion prepared by embodiment one, embodiment two respectively
Content, content of formaldehyde.Measurement result is as shown in table 7.
Table 7
The measurement result of table 7 shows：The shampoo used also as bath lotion of the present invention of embodiment one does not detect specified risk material dioxane, phenol
And formaldehyde；And traditional infant of embodiment two detects a small amount of dioxanes and formaldehyde with shampoo used also as bath lotion.
Embodiment six：The performance evaluation of shampoo used also as bath lotion
The skin of infant is more tender and lovely, than the stimulation that adult is more vulnerable to the external world, therefore, infant's shampoo used also as bath lotion
Need to meet claimed below：(1) excitant is low, to eyes, no skin irritation；(2) detergency is moderate, it is to avoid to normal skin
Skin structure causes damage；(3) wash degree is high, easily cleaning, it is to avoid remained in skin surface formation；(4) foaming characteristic is low, reduces thorn
Swash, it is to avoid accidentally injure eyes；(5) without tight feeling, the normal barrier function of skin is kept.
The shampoo used also as bath lotion that respectively prepared by Example one, embodiment two, according to《Cosmetics health specification》(2007 editions)
Pertinent regulations, its excitant, detergency, wash degree, foaming characteristic, tight feeling are tested and scored respectively (5 points system), knot
Fruit is as shown in table 8.
Table 8
The test result of table 8 shows：The shampoo used also as bath lotion of the invention of embodiment one is nonirritant, detergency is moderate, clean
Degree is high, foaming characteristic is low, without tight feeling；And traditional infant of embodiment two has weak excitant with shampoo used also as bath lotion, wash degree
Height, detergency, foaming characteristic are higher, there is tight feeling after cleaning.
Embodiment seven：Anti-corrosive properties are tested
According to American Pharmacopeia USP32<51>Antimicrobial preservation efficacy test method, to the preservative system of the present invention
Anti-corrosive properties are tested, and test result is as shown in table 9.
Table 9
The test result of table 9 shows：When Phenoxyethanol is used alone, antiseptic effect is poor；Phenoxyethanol and methyl hydroxybenzoate
When being used in combination, with good antiseptic effect；Phenoxyethanol, methyl hydroxybenzoate and the smooth caprylate of sorb are used in combination, with association
Same facilitation, can significantly improve antiseptic effect.
Embodiment described above only expresses the several embodiments of the present invention, and it describes more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention
Protect scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (7)
1. a kind of shampoo used also as bath lotion, by weight percentage including following component：
And the purified water of its surplus.
2. shampoo used also as bath lotion according to claim 1, it is characterised in that：Described tax fat agent be selected from cocoyl glucoside,
The combination of one or both of glyceryl oleate.
3. shampoo used also as bath lotion according to claim 1, it is characterised in that：Described preservative is selected from Phenoxyethanol, oxybenzene
The combination of one or both of methyl esters.
4. shampoo used also as bath lotion according to claim 1, it is characterised in that：Described anti-corrosion synergist is selected from the smooth octanoic acid of sorb
Ester.
5. shampoo used also as bath lotion according to claim 1, it is characterised in that：Described complexing agent is selected from EDETATE SODIUM, EDTA
The combination of one or both of four sodium.
6. shampoo used also as bath lotion according to claim 1, it is characterised in that：Described pH adjusting agent be selected from citric acid, lactic acid,
Mixing more than one or both of butanedioic acid, anisic acid.
7. the preparation method of the shampoo used also as bath lotion described in claim 1, comprises the following steps：Caprylic/capric glyceride is birdsed of the same feather flock together
The esters of glycerine -10, lauryl glucoside, laureth sodium sulfovinate, Cocoamidopropyl betaine, PEG-150 distearyls
Acid esters, the agent of tax fat, complexing agent, pH adjusting agent, preservative, anti-corrosion synergist are added in purified water, are heated with stirring to 90~100 DEG C
It is allowed to be completely dissolved, insulated and stirred 10~20 minutes is cooled to 40~45 DEG C；Then essence is added, is stirred, 38 are cooled to
Below DEG C, discharging obtains described shampoo used also as bath lotion.
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| CN106726869A (en) * | 2016-11-18 | 2017-05-31 | 广州环亚化妆品科技有限公司 | A kind of shampoo of natural no stimulation and preparation method thereof |
| JP6719655B2 (en) * | 2017-03-29 | 2020-07-08 | 株式会社マンダム | Hair dye composition |
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| CN107669551B (en) * | 2017-10-31 | 2019-08-16 | 思拓科（上海）生物科技股份有限公司 | Organic baby's shampoo used also as bath lotion and preparation method thereof |
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| CN110623887A (en) * | 2019-11-01 | 2019-12-31 | 苏州东方之宝生物药业有限公司 | Shampoo shower gel |
| CN111449980A (en) * | 2020-04-08 | 2020-07-28 | 广州旭升化工科技有限公司 | Shampoo shower gel and preparation method thereof |
| CN111888294A (en) * | 2020-08-20 | 2020-11-06 | 澳宝化妆品（惠州）有限公司 | Mild and hypoallergenic infant shampoo and bath composition containing plantain herb extract |
| CN114366693B (en) * | 2022-01-10 | 2023-08-22 | 广州天然国度生物科技有限公司 | Shampoo bath lotion for infants |
| CN115192476B (en) * | 2022-08-31 | 2023-08-29 | 完美（广东）日用品有限公司 | Non-irritating shampoo bath lotion and preparation method thereof |
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