CN104585871A - Seabuckthorn flavone antioxidant electronic cigarette juice - Google Patents
Seabuckthorn flavone antioxidant electronic cigarette juice Download PDFInfo
- Publication number
- CN104585871A CN104585871A CN201510027975.8A CN201510027975A CN104585871A CN 104585871 A CN104585871 A CN 104585871A CN 201510027975 A CN201510027975 A CN 201510027975A CN 104585871 A CN104585871 A CN 104585871A
- Authority
- CN
- China
- Prior art keywords
- parts
- extract
- tobacco
- mass concentration
- hippophate flavone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a seabuckthorn flavone antioxidant electronic cigarette juice which is prepared by mixing the following materials by weight percent: 5-10% of tobacco leaf extractives, 5-8% of tobacco flavors, 1-5% of tobacco spices, 5-15% of deionized water, 10-20% of glycerol, 3-15% of seabuckthorn flavone and the balance of propylene glycol, wherein the tobacco leaf extractives are preferably selected as Zimbabwe tobacco leaf extractives. The electronic cigarette juice provided by the invention contains seabuckthorn flavone, so that the electronic cigarette fragrance is more soft and delicate, the stimulation is reduced, the comfort is enhanced and the electronic cigarette juice has the health care functions of oxidation resistance and anti-aging. The electronic cigarette juice provided by the invention is used for atomizing the electronic cigarette, no tar and CO (carbon monoxide) are generated, the harm to the consumer is greatly reduced, and no second hand smoking damage is generated by the application of the electronic cigarette juice. The raw materials of the formula of the electronic cigarette juice containing the seabuckthorn flavone are easily acquired, and the seabuckthorn flavone antioxidant electronic cigarette juice is conformed to the international and national laws and regulations, and the production technique is simple.
Description
Technical field
Embodiments of the present invention relate to Field of Tobacco, and more specifically, embodiments of the present invention relate to the anti-oxidant tobacco juice for electronic smoke of a kind of Hippophate flavone.
Background technology
Along with the development of global Tobacco Control campaign, smoking and health are more and more subject to social concerns, for smoking and the health requirements of satisfied different consumer, novel tobacco goods achieve fast development in recent years, mainly comprise smoke-free tobacco product, low temperature cigarette and electronic cigarette.Wherein, electronic cigarette does not produce the harmful substances such as tar, and the tobacco juice through atomization is diluted rapidly in atmosphere, does not have side-stream smoke, and can not form second-hand-cigarette harm, be a kind of cigarette substitute popular gradually.
Electronic cigarette external form is similar to regular-size cigarette, is a kind of device that nicotine solution can be vaporized into fog, smokes true, bring stimulation to smoker by simulation.Its principle is, when sucking electronic cigarette, electronic cigarette battery is powered to electronic smoke atomizer, and atomizer is started working, and the tobacco juice atomization being stored at electronic cigarette is produced smog.Tobacco juice in electronic cigarette, also claims " tobacco tar ", is actually a formula essence, and when sucking electronic cigarette, tobacco juice atomization is " smog ", and smog comprises glycerine, propane diols and the fragrance matter etc. that evaporate in tobacco juice.Whether tobacco juice for electronic smoke is electronic cigarette aroma source, decides the taste style of electronic cigarette, decide product and be esthetically acceptable to the consumers.Therefore, the tobacco juice formula technique of electronic cigarette is one of key technology of electronic cigarette.
Sea-buckthorn has another name called arrow-leaved oleaster, sour willow fruit, Elaeangnaceae acid thorn platymiscium.Record in " Chinese medicine voluminous dictionary ", sea-buckthorn " warm in nature, sour-puckery flavor ", modern pharmacological research shows, has phlegm reduction of blood circulation promoting, wide chest tonifying spleen stomach invigorating, promotes the production of body fluid to quench thirst, effect of clearing away heat to stop diarrhea.Cholesterol, allevating angina pectoris outbreak can be reduced, prevent and treat the effect of coronary atherosclerotic heart disease in addition.Hippophate flavone is the flavone compound extracted from fructus hippophae, it is a kind of reactive compound in sea-buckthorn, there is scavenging free radicals and lipoid peroxidization resistant, modern study proves, Hippophate flavone can reduce blood fat, cholesterol, triglycerides, there is good curative effect reduction blood viscosity, Antiaggregating activity on platelet, prevention thrombosis aspect, thus reduce the incidence of cardiovascular and cerebrovascular disease.Hippophate flavone is to one of drug of first choice of resisting cardiovascular disease.
ASE (Accelerate solvent extraction technology) is a kind of brand-new extracting process proposed by (1995) such as Richter, it uses the temperature and pressure improved to reach in the short time object completing extraction, is recommended as a kind of extracting process of standard by American National Environmental Protection Agency (EPA).
At present, more existing patent reports about tobacco juice for electronic smoke, but suction aesthetic quality well has again the electronic cigarette oil starvation of health care.Chinese patent application CN201410312006.2 discloses a kind of tobacco juice for electronic smoke being rich in plant flavone, there is effect that is anti-oxidant, anti-aging, immunity moderation power, certain health-care effect is had to cardiovascular and cerebrovascular, this patent application is mainly considered to improve the health-care effect of tobacco juice for electronic smoke but is not emphatically considered mouthfeel and the quality of tobacco juice for electronic smoke, also unexposed using Hippophate flavone as the proportioning between the amount that should use during the component of tobacco juice for electronic smoke and other composition and the collocation between each component of tobacco juice for electronic smoke.At present, there is not yet the report that Hippophate flavone is applied to tobacco juice for electronic smoke.
Summary of the invention
Instant invention overcomes the deficiencies in the prior art, a kind of embodiment of the tobacco juice for electronic smoke containing Hippophate flavone is provided, to expect the suction mouthfeel and the quality that improve electronic cigarette, and improve the health-care effect of electronic cigarette.
For solving above-mentioned technical problem, one embodiment of the present invention by the following technical solutions:
The anti-oxidant tobacco juice for electronic smoke of a kind of Hippophate flavone, it is mixed by the following component in mass content:
Leaf tobacco extract 5 ~ 10%, flavouring essence for tobacco 5 ~ 8%, tobacco aromatics 1 ~ 5%, deionized water 5 ~ 15%, glycerine 10 ~ 20%, Hippophate flavone 3 ~ 15%, surplus is propane diols.
Further technical scheme is, the anti-oxidant tobacco juice for electronic smoke of described Hippophate flavone is mixed by the following component in mass content:
Leaf tobacco extract 8 ~ 10%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 7 ~ 10%, surplus is propane diols.
Consider the quality of tobacco juice for electronic smoke, mouthfeel and health-care effect, a kind of is preferred embodiment that the described anti-oxidant tobacco juice for electronic smoke of Hippophate flavone is mixed by the following component in mass content:
Leaf tobacco extract 10%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 10%, surplus is propane diols.
Consider the quality of tobacco juice for electronic smoke, mouthfeel and health-care effect, another preferred embodiment is that the described anti-oxidant tobacco juice for electronic smoke of Hippophate flavone is mixed by the following component in mass content:
Leaf tobacco extract 8%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 7%, surplus is propane diols.
Further technical scheme is: described leaf tobacco extract is Zimbabwe's leaf tobacco extract.This Zimbabwe's leaf tobacco extract is purchased from Guangzhou Huabao Flavor Co., Ltd..
Further technical scheme is: described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2 ~ 3 parts, Peru's medicinal extract 0.5 ~ 1 part, Ethyl vanillin 0.1 ~ 3 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 3 ~ 5 parts, maltol 0.05 ~ 0.1 part, 2-acetyl group pyrazine 0.5 ~ 1.0 part, 2, 3, 5-trimethylpyrazine 0.5 ~ 1 part, iso-amyl iso-valeriate 1.0 ~ 1.5 parts, menthyl acetate 0.1 ~ 0.5 part, the oxidation isophorone of mass concentration 1% 0.5 ~ 1 part, the damascenone of mass concentration 1% 1.0 ~ 2.0 parts, the damascone of mass concentration 1% 0.5 ~ 1 part, the Megastigmatrienone of mass concentration 1% 0.5 ~ 1 part, the lavender oil of mass concentration 1% 1.0 ~ 2.0 parts, the coriander seed oil of mass concentration 1% 1.5 ~ 2.0 parts, vanilla bean tincture 7.0 ~ 7.0 parts, red date tincture 9 ~ 11 parts, angelica grosseserrata root tincture 2.0 ~ 4.0 parts, propane diols 18.0 ~ 22.0 parts, ethanol 40.0 ~ 45.0 parts.
Preferably, described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2.2 parts, Peru's medicinal extract 0.6 part, Ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the lavender oil of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propane diols 20 parts, ethanol 43.35 parts.
Further technical scheme is: described tobacco aromatics is made by being uniformly mixed at temperature 50 ~ 60 DEG C with the following component of parts by weight: honey 5 ~ 7 parts, Fructus Monordicae extract 2 ~ 4 parts, licorice 4 ~ 6 parts, tamarind medicinal extract 5 ~ 7 parts, fig medicinal extract 5 ~ 7 parts, vanilla extract 4 ~ 6 parts, apple extract 5 ~ 7 parts, apricot extract 5 ~ 7 parts, plum extract 7 ~ 10 parts, tree moss concrete 4 ~ 6 parts, radix valerianae extract 2 ~ 4 parts, tamarind extract 6 ~ 8 parts, red date absolute oil 4 ~ 6 parts, deionized water 12 ~ 16 parts, propane diols 13 ~ 16 parts.
Preferably, described tobacco aromatics is made by being uniformly mixed at temperature 50 ~ 60 DEG C with the following component of parts by weight: honey 6 parts, Fructus Monordicae extract 3 parts, licorice 5 parts, tamarind medicinal extract 6 parts, fig medicinal extract 6 parts, vanilla extract 5 parts, apple extract 6 parts, apricot extract 6 parts, plum extract 8 parts, tree moss concrete 5 parts, radix valerianae extract 3 parts, tamarind extract 7 parts, red date absolute oil 5 parts, deionized water 14 parts, propane diols 15 parts.
Further technical scheme is: the preparation method of described Hippophate flavone is:
(1) after sea-buckthorn dry fruit being cleaned removal of impurities, be placed in 40 DEG C of baking ovens and dry, then pulverize and obtain Seabuckthorn Fruit;
(2) Seabuckthorn Fruit is joined in the abstraction pool of ASE abstraction instrument, be solvent with the ethanol of concentration 60 ~ 85%, extraction temperature 80 ~ 110 DEG C, heat time 4 ~ 15min, static extracting time 10 ~ 15min, extracting pressure 1200 ~ 1700psi, extraction cycle number of times 1 ~ 3 time, elution volume 40 ~ 60%, nitrogen adds extraction heat under blowing the condition of time 200 ~ 280s, collect extract, by extract reduced pressure concentration;
(3) by macroporous resin column absorption on the extract after reduced pressure concentration, first wash with water, then use concentration 30 ~ 50% ethanol elution, collect eluent, reduced pressure concentration, concentrate cryogenic vacuum is dried to constant weight, 30 ~ 50 DEG C of vacuum drying can be adopted, obtain brownish-yellow powder shape Hippophate flavone.The concentration of ethanol all refers to the volume fraction of ethanol in ethanolic solution.
Compared with prior art, one of beneficial effect of the present invention is:
The present invention aims to provide a kind of tobacco juice for electronic smoke containing Hippophate flavone, can meet the smoking aesthetic quality demand of smoker, make the softer exquisiteness of electronic cigarette fragrance, reduces and stimulates, and increases comfort, has again and removes human free radical and anti-oxidation health effect; The tobacco juice for electronic smoke that the present invention produces is used for electronic cigarette atomizing, does not produce tar and CO, greatly reduces the harm of consumer, and the application of this product can not produce second-hand-cigarette harm; And provide the preparation method utilizing ASE to extract Hippophate flavone simultaneously.It is few, fast simple to operate that the method has solvent load compared with traditional extraction process, and extraction efficiency significantly improves, and maintains the outstanding advantages such as the biologically active of flavonoid substance simultaneously.
Detailed description of the invention
In order to make object of the present invention, technical scheme and advantage clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not intended to limit the present invention.
The extraction of Hippophate flavone
After sea-buckthorn dry fruit is cleaned removal of impurities, be placed in 40 DEG C of baking ovens and dry, pulverize and obtain Seabuckthorn Fruit.100g Seabuckthorn Fruit is claimed to join in the abstraction pool of ASE abstraction instrument, be solvent with the ethanol of concentration 70%, extraction temperature 100 DEG C, heat time 15min, the static extracting time: 15min, extracting pressure: 1500psi, extraction cycle number of times: 3 times, elution volume 60%, nitrogen blows time 250s, add extraction heat, collect extract, reduced pressure concentration.On the concentrate obtained, macroporous resin column absorption, first washes with water, then uses concentration 40% ethanol elution, collects eluent, reduced pressure concentration, and concentrate cryogenic vacuum is dried to constant weight, obtains 3.54g brownish-yellow powder, i.e. Hippophate flavone, yield 3.54%.The Hippophate flavone that following embodiment all adopts the method to prepare and obtains.
Flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2.2 parts, Peru's medicinal extract 0.6 part, Ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the lavender oil of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propane diols 20 parts, ethanol 43.35 parts.
Tobacco aromatics is made by being uniformly mixed at temperature 50 ~ 60 DEG C with the following component of parts by weight: honey 6 parts, Fructus Monordicae extract 3 parts, licorice 5 parts, tamarind medicinal extract 6 parts, fig medicinal extract 6 parts, vanilla extract 5 parts, apple extract 6 parts, apricot extract 6 parts, plum extract 8 parts, tree moss concrete 5 parts, radix valerianae extract 3 parts, tamarind extract 7 parts, red date absolute oil 5 parts, deionized water 14 parts, propane diols 15 parts.
Above-mentioned Hippophate flavone, flavouring essence for tobacco, tobacco aromatics are used for following each embodiment.
Embodiment 1
Containing a tobacco juice for electronic smoke for Hippophate flavone, its component comprises: Zimbabwe's leaf tobacco extract 10%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 20%, Hippophate flavone 15%, surplus is propane diols, and the consumption of each component is in mass content.
When preparing tobacco juice for electronic smoke, get out said components, then they are mixed, stir 30min at normal temperatures and each component is fully mixed.
Embodiment 2
Containing a tobacco juice for electronic smoke for Hippophate flavone, its component comprises: Zimbabwe's leaf tobacco extract 10%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 10%, surplus is propane diols, and the consumption of each component is in mass content.
When preparing tobacco juice for electronic smoke, get out said components, then they are mixed, stir 30min at normal temperatures and each component is fully mixed.
Embodiment 3
Containing a tobacco juice for electronic smoke for Hippophate flavone, its component comprises: Zimbabwe's leaf tobacco extract 8%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 7%, surplus is propane diols, and the consumption of each component is in mass content.
When preparing tobacco juice for electronic smoke, get out said components, then they are mixed, stir 30min at normal temperatures and each component is fully mixed.
Embodiment 4
Containing a tobacco juice for electronic smoke for Hippophate flavone, its component comprises: Zimbabwe's leaf tobacco extract 5%, flavouring essence for tobacco 8%, tobacco aromatics 5%, deionized water 15%, glycerine 10%, Hippophate flavone 3%, surplus is propane diols, and the consumption of each component is in mass content.
When preparing tobacco juice for electronic smoke, get out said components, then they are mixed, stir 30min at normal temperatures and each component is fully mixed.
Comparative example 1
A kind of tobacco juice for electronic smoke, it is not containing Hippophate flavone, and its component comprises: Zimbabwe's leaf tobacco extract 10%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, and surplus is propane diols, and the consumption of each component is in mass content.
When preparing tobacco juice for electronic smoke, get out said components, then they are mixed, stir 30min at normal temperatures and each component is fully mixed.
Be added in electronic cigarette by electronic cigarette liquid prepared by embodiment 1, embodiment 2, embodiment 3, embodiment 4, comparative example 1 and carry out sensory quality assessment, evaluation result is in table 2.
Electronic cigarette sensory quality assessment method carrys out method (CN 201310030063.7) with reference to Zhu east:
Sensory quality assessment project and scale are arranged: arrange 7 projects, are respectively aroma quality, perfume quantity, concentration, excitant, assorted gas, strength, pleasant impression; The maximum scale of each project is 9, and individual project is divided into scoring unit with 1, corresponding to the meaning of each scale value of projects in table 1.
Table 1 tobacco juice for electronic smoke sensory quality assessment corresponds to the meaning of each scale value of projects
| Score value | Aroma quality | Perfume quantity | Concentration | Excitant | Assorted gas | Strength | Pleasant impression |
| 9 | Very well | Sufficient | Dense | Very little | Very light | Very large | Very well |
| 8 | Good | Foot | Dense | Little | Gently | Greatly | Good |
| 7 | Better | More sufficient | Denseer | Less | Lighter | Larger | Better |
| 6 | Slightly good | Still sufficient | Slightly dense | Slightly little | Still light | Slightly large | Slightly good |
| 5 | In | In | In | In | In | In | In |
| 4 | Slightly poor | Slightly | Slightly light | Slightly large | Slightly heavy | Slightly little | Slightly poor |
| 3 | Poor | Lighter | Lighter | Larger | Heavier | Less | Poor |
| 2 | Difference | Flat | Light | Greatly | Heavy | Little | Difference |
| 1 | Very poor | Very light | Very light | Very large | Very heavy | Very little | Very poor |
Table 2 Analyses Methods for Sensory Evaluation Results
As shown in Table 2, the tobacco juice for electronic smoke that the present invention utilizes Hippophate flavone to prepare, in Zimbabwe's different proportion extract, compared with the contrast tobacco juice for electronic smoke not adding Hippophate flavone, the aesthetic quality's score that with the addition of the tobacco juice for electronic smoke of Hippophate flavone all has raising in various degree, more fine and smooth soft, the excitant of fragrance and assorted gas decrease, and pleasant impression is more comfortable.Wherein, when Fructus Hippophae polysaccharide addition is 7 ~ 10%, it is comparatively obvious that the aesthetic quality of tobacco juice for electronic smoke improves effect.
Although with reference to multiple explanatory embodiment of the present invention, invention has been described here, but, should be appreciated that, those skilled in the art can design a lot of other amendment and embodiment, these amendments and embodiment will drop within spirit disclosed in the present application and spirit.More particularly, in the scope of and claim open in the application, multiple modification and improvement can be carried out to the building block of subject combination layout and/or layout.Except the modification of carrying out building block and/or layout is with except improvement, to those skilled in the art, other purposes also will be obvious.
Claims (10)
1. the anti-oxidant tobacco juice for electronic smoke of Hippophate flavone, is characterized in that it is mixed by the following component in mass content:
Leaf tobacco extract 5 ~ 10%, flavouring essence for tobacco 5 ~ 8%, tobacco aromatics 1 ~ 5%, deionized water 5 ~ 15%, glycerine 10 ~ 20%, Hippophate flavone 3 ~ 15%, surplus is propane diols.
2. the anti-oxidant tobacco juice for electronic smoke of Hippophate flavone according to claim 1, is characterized in that it is mixed by the following component in mass content:
Leaf tobacco extract 8 ~ 10%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 7 ~ 10%, surplus is propane diols.
3. the anti-oxidant tobacco juice for electronic smoke of Hippophate flavone according to claim 2, is characterized in that it is mixed by the following component in mass content:
Leaf tobacco extract 10%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 10%, surplus is propane diols.
4. the anti-oxidant tobacco juice for electronic smoke of Hippophate flavone according to claim 2, is characterized in that it is mixed by the following component in mass content:
Leaf tobacco extract 8%, flavouring essence for tobacco 5%, tobacco aromatics 2%, deionized water 15%, glycerine 10%, Hippophate flavone 7%, surplus is propane diols.
5. the anti-oxidant tobacco juice for electronic smoke of the Hippophate flavone according to Claims 1 to 4 any one, is characterized in that described leaf tobacco extract is Zimbabwe's leaf tobacco extract.
6. the anti-oxidant tobacco juice for electronic smoke of the Hippophate flavone according to Claims 1 to 4 any one, it is characterized in that described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2 ~ 3 parts, Peru's medicinal extract 0.5 ~ 1 part, Ethyl vanillin 0.1 ~ 3 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 3 ~ 5 parts, maltol 0.05 ~ 0.1 part, 2-acetyl group pyrazine 0.5 ~ 1.0 part, 2, 3, 5-trimethylpyrazine 0.5 ~ 1 part, iso-amyl iso-valeriate 1.0 ~ 1.5 parts, menthyl acetate 0.1 ~ 0.5 part, the oxidation isophorone of mass concentration 1% 0.5 ~ 1 part, the damascenone of mass concentration 1% 1.0 ~ 2.0 parts, the damascone of mass concentration 1% 0.5 ~ 1 part, the Megastigmatrienone of mass concentration 1% 0.5 ~ 1 part, the lavender oil of mass concentration 1% 1.0 ~ 2.0 parts, the coriander seed oil of mass concentration 1% 1.5 ~ 2.0 parts, vanilla bean tincture 7.0 ~ 8.0 parts, red date tincture 9 ~ 11 parts, angelica grosseserrata root tincture 2.0 ~ 4.0 parts, propane diols 18.0 ~ 22.0 parts, ethanol 40.0 ~ 45.0 parts.
7. the anti-oxidant tobacco juice for electronic smoke of Hippophate flavone according to claim 6, it is characterized in that described flavouring essence for tobacco is made by being at room temperature uniformly mixed with the following component of parts by weight: cloud and mist absolute oil 2.2 parts, Peru's medicinal extract 0.6 part, Ethyl vanillin 0.2 part, the 2-hydroxyl-2 of mass concentration 10%, 6, 6-trimethylcyclohexanone 4.0 parts, maltol 0.05 part, 2-acetyl group pyrazine 1.0 parts, 2, 3, 5-trimethylpyrazine 0.5 part, iso-amyl iso-valeriate 1.0 parts, menthyl acetate 0.2 part, the oxidation isophorone of mass concentration 1% 0.9 part, the damascenone of mass concentration 1% 1.5 parts, the damascone of mass concentration 1% 0.5 part, the Megastigmatrienone of mass concentration 1% 0.5 part, the lavender oil of mass concentration 1% 1.0 parts, the coriander seed oil of mass concentration 1% 1.5 parts, vanilla bean tincture 8.0 parts, red date tincture 10 parts, angelica grosseserrata root tincture 3.0 parts, propane diols 20 parts, ethanol 43.35 parts.
8. the anti-oxidant tobacco juice for electronic smoke of the Hippophate flavone according to Claims 1 to 4 any one, it is characterized in that described tobacco aromatics is made by being uniformly mixed at temperature 50 ~ 60 DEG C with the following component of parts by weight: honey 5 ~ 7 parts, Fructus Monordicae extract 2 ~ 4 parts, licorice 4 ~ 6 parts, tamarind medicinal extract 5 ~ 7 parts, fig medicinal extract 5 ~ 7 parts, vanilla extract 4 ~ 6 parts, apple extract 5 ~ 7 parts, apricot extract 5 ~ 7 parts, plum extract 7 ~ 10 parts, tree moss concrete 4 ~ 6 parts, radix valerianae extract 2 ~ 4 parts, tamarind extract 6 ~ 8 parts, red date absolute oil 4 ~ 6 parts, deionized water 12 ~ 16 parts, propane diols 13 ~ 16 parts.
9. the anti-oxidant tobacco juice for electronic smoke of Hippophate flavone according to claim 8, it is characterized in that described tobacco aromatics is made by being uniformly mixed at temperature 50 ~ 60 DEG C with the following component of parts by weight: honey 6 parts, Fructus Monordicae extract 3 parts, licorice 5 parts, tamarind medicinal extract 6 parts, fig medicinal extract 6 parts, vanilla extract 5 parts, apple extract 6 parts, apricot extract 6 parts, plum extract 8 parts, tree moss concrete 5 parts, radix valerianae extract 3 parts, tamarind extract 7 parts, red date absolute oil 5 parts, deionized water 14 parts, propane diols 15 parts.
10. the anti-oxidant tobacco juice for electronic smoke of the Hippophate flavone according to Claims 1 to 4 any one, is characterized in that the preparation method of described Hippophate flavone is:
(1) after sea-buckthorn dry fruit being cleaned removal of impurities, be placed in 40 DEG C of baking ovens and dry, then pulverize and obtain Seabuckthorn Fruit;
(2) Seabuckthorn Fruit is joined in the abstraction pool of ASE abstraction instrument, be solvent with the ethanol of concentration 60 ~ 85%, extraction temperature 80 ~ 110 DEG C, heat time 4 ~ 15min, static extracting time 10 ~ 15min, extracting pressure 1200 ~ 1700psi, extraction cycle number of times 1 ~ 3 time, elution volume 40 ~ 60%, nitrogen adds extraction heat under blowing the condition of time 200 ~ 280s, collect extract, by extract reduced pressure concentration;
(3) by macroporous resin column absorption on the extract after reduced pressure concentration, first wash with water, then use concentration 30 ~ 50% ethanol elution, collect eluent, reduced pressure concentration, concentrate cryogenic vacuum is dried to constant weight, obtains brownish-yellow powder shape Hippophate flavone.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510027975.8A CN104585871B (en) | 2015-01-20 | 2015-01-20 | The anti-oxidant tobacco juice for electronic smoke of a kind of Hippophate flavone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510027975.8A CN104585871B (en) | 2015-01-20 | 2015-01-20 | The anti-oxidant tobacco juice for electronic smoke of a kind of Hippophate flavone |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104585871A true CN104585871A (en) | 2015-05-06 |
| CN104585871B CN104585871B (en) | 2016-02-03 |
Family
ID=53112204
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510027975.8A Active CN104585871B (en) | 2015-01-20 | 2015-01-20 | The anti-oxidant tobacco juice for electronic smoke of a kind of Hippophate flavone |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104585871B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104886764A (en) * | 2015-05-14 | 2015-09-09 | 湖北中烟工业有限责任公司 | Production method of eucalyptus leaf extract for cigarettes |
| WO2021102654A1 (en) * | 2019-11-25 | 2021-06-03 | 深圳雾芯科技有限公司 | Electronic cigarette liquid |
| CN113693263A (en) * | 2021-08-30 | 2021-11-26 | 深圳市真味生物科技有限公司 | Seabuckthorn flavone antioxidant electronic cigarette liquid and preparation method thereof |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107343668A (en) * | 2017-08-31 | 2017-11-14 | 云南巴菰生物科技有限公司 | A kind of purposes of the electronics tobacco tar for lifting fragrance texture and preparation method thereof with it |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1980163A1 (en) * | 2007-04-10 | 2008-10-15 | Litesso-Anstalt | Method for treating tobacco leaves and tobacco leaves and their utilisation |
| CN101386615A (en) * | 2008-11-05 | 2009-03-18 | 中国科学院西北高原生物研究所 | Method for extracting procyanidine from sea-buckthorn seed |
| CN102090712A (en) * | 2010-12-29 | 2011-06-15 | 华宝食用香精香料（上海）有限公司 | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes |
| CN102920007A (en) * | 2011-08-08 | 2013-02-13 | 邳州市华泰银杏叶制品有限公司 | Method for preparing health-care cigarettes |
| CN103505612A (en) * | 2012-06-28 | 2014-01-15 | 天津天狮生物发展有限公司 | Traditional Chinese medicine composition containing total flavonoids of sea-buckthorn and preparation method of composition |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
-
2015
- 2015-01-20 CN CN201510027975.8A patent/CN104585871B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1980163A1 (en) * | 2007-04-10 | 2008-10-15 | Litesso-Anstalt | Method for treating tobacco leaves and tobacco leaves and their utilisation |
| CN101386615A (en) * | 2008-11-05 | 2009-03-18 | 中国科学院西北高原生物研究所 | Method for extracting procyanidine from sea-buckthorn seed |
| CN102090712A (en) * | 2010-12-29 | 2011-06-15 | 华宝食用香精香料（上海）有限公司 | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes |
| CN102920007A (en) * | 2011-08-08 | 2013-02-13 | 邳州市华泰银杏叶制品有限公司 | Method for preparing health-care cigarettes |
| CN103505612A (en) * | 2012-06-28 | 2014-01-15 | 天津天狮生物发展有限公司 | Traditional Chinese medicine composition containing total flavonoids of sea-buckthorn and preparation method of composition |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104886764A (en) * | 2015-05-14 | 2015-09-09 | 湖北中烟工业有限责任公司 | Production method of eucalyptus leaf extract for cigarettes |
| WO2021102654A1 (en) * | 2019-11-25 | 2021-06-03 | 深圳雾芯科技有限公司 | Electronic cigarette liquid |
| CN113693263A (en) * | 2021-08-30 | 2021-11-26 | 深圳市真味生物科技有限公司 | Seabuckthorn flavone antioxidant electronic cigarette liquid and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104585871B (en) | 2016-02-03 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104585871B (en) | The anti-oxidant tobacco juice for electronic smoke of a kind of Hippophate flavone | |
| CN104687240B (en) | There is electronic cigarette liquid of Ambra Grisea fragrance and preparation method thereof | |
| CN103070473A (en) | Electronic cigarette liquid prepared from fen-flavor tobacco leaves | |
| CN104585864B (en) | A kind of tobacco juice for electronic smoke containing Fructus Hippophae polysaccharide | |
| CN106867675A (en) | A kind of cigarette preparation method of Momordica grosvenori essence | |
| CN103054172A (en) | Electronic cigarette liquid prepared from strong-flavor tobacco leaves | |
| CN109619656A (en) | It is a kind of to have effects that the tobacco juice for electronic smoke of antiphlogistic antibacterial | |
| CN105815808A (en) | Novel healthcare cigarette free of tobacco ingredients | |
| CN106307602A (en) | Electronic cigarette liquid for freshening breath | |
| CN103351950A (en) | Cigarette essence perfume containing coke hawthorn extract and cigarettes containing same | |
| CN104687239B (en) | A kind of tobacco juice for electronic smoke training element rich in ultrafine green tea powder and tea | |
| CN104705777B (en) | A kind of tobacco juice for electronic smoke containing natural built-up thing | |
| CN108142986A (en) | A kind of Chinese herbal medicine composite extract, preparation method and its application in cigarette | |
| CN101371720A (en) | Tobacco additive agent as well as preparation method and use thereof | |
| CN105105316B (en) | A kind of agilawood essential oil atomized liquid and preparation method thereof | |
| CN106858705A (en) | A kind of tobacco juice for electronic smoke for containing 3 oxo-alpha violet alcohol radical β D glucopyranosides | |
| CN106723302A (en) | Tobacco tar and preparation method thereof | |
| CN1045379C (en) | Health cigarette made of ginkgo leaf | |
| CN104983054A (en) | Preparation method and application of extract to improving cigarette sour and sweet note | |
| CN104585869B (en) | A kind of tobacco juice for electronic smoke containing glucosides | |
| CN104585867B (en) | Containing the tobacco juice for electronic smoke of Flue-cured Tobacco flower extract | |
| CN104687243A (en) | Natural compound humectant with cigarette sensory humectation function | |
| CN105018231B (en) | A kind of cigarette peel extract and application | |
| CN101116537A (en) | Nuisance-free innovation cigarette | |
| CN103385538A (en) | Corn-chocolate cigarette and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20161228 Address after: 610000, Sichuan, Chengdu, Longquanyi economic and Technological Development Zone, Jackie Chan Road, Longquan, No. 2, paragraph Patentee after: CHINA TOBACCO SICHUAN INDUSTRIAL CO., LTD. Patentee after: CHONGQING CHINA TOBACCO INDUSTRIAL CO., LTD. Address before: 610000 Jackie Chan Road, Chengdu economic and Technological Development Zone, Longquanyi District, Sichuan, China, No. 2, No. Patentee before: China Tobacco Chuanyu Industry Co., Ltd. |