CN104543672B - Syrup special for moon cake and preparation method thereof - Google Patents
Syrup special for moon cake and preparation method thereof Download PDFInfo
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- CN104543672B CN104543672B CN201410845040.6A CN201410845040A CN104543672B CN 104543672 B CN104543672 B CN 104543672B CN 201410845040 A CN201410845040 A CN 201410845040A CN 104543672 B CN104543672 B CN 104543672B
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- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title claims abstract description 62
- 235000020357 syrup Nutrition 0.000 title claims abstract description 50
- 239000006188 syrup Substances 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title claims abstract description 23
- 239000007788 liquid Substances 0.000 claims abstract description 108
- 235000020429 malt syrup Nutrition 0.000 claims abstract description 51
- 239000000706 filtrate Substances 0.000 claims abstract description 41
- 238000002156 mixing Methods 0.000 claims abstract description 35
- 229920002472 Starch Polymers 0.000 claims abstract description 27
- 235000019698 starch Nutrition 0.000 claims abstract description 27
- 239000008107 starch Substances 0.000 claims abstract description 27
- 238000005984 hydrogenation reaction Methods 0.000 claims abstract description 25
- 235000010449 maltitol Nutrition 0.000 claims abstract description 20
- 239000000845 maltitol Substances 0.000 claims abstract description 20
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 claims abstract description 20
- 229940035436 maltitol Drugs 0.000 claims abstract description 20
- 238000005119 centrifugation Methods 0.000 claims abstract description 13
- 238000001914 filtration Methods 0.000 claims abstract description 11
- 238000013329 compounding Methods 0.000 claims abstract description 10
- 229920002261 Corn starch Polymers 0.000 claims abstract description 9
- 239000008120 corn starch Substances 0.000 claims abstract description 9
- 229940099112 cornstarch Drugs 0.000 claims abstract description 9
- 238000001704 evaporation Methods 0.000 claims abstract description 9
- 230000008020 evaporation Effects 0.000 claims abstract description 9
- 238000000746 purification Methods 0.000 claims abstract description 4
- 238000002347 injection Methods 0.000 claims description 24
- 239000007924 injection Substances 0.000 claims description 24
- 239000002002 slurry Substances 0.000 claims description 18
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
- 150000001768 cations Chemical class 0.000 claims description 16
- 150000004043 trisaccharides Chemical class 0.000 claims description 16
- 230000002378 acidificating effect Effects 0.000 claims description 15
- 150000001450 anions Chemical class 0.000 claims description 15
- 230000000694 effects Effects 0.000 claims description 12
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 9
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 9
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 8
- 239000004382 Amylase Substances 0.000 claims description 8
- 108010065511 Amylases Proteins 0.000 claims description 8
- 102000013142 Amylases Human genes 0.000 claims description 8
- 108090000790 Enzymes Proteins 0.000 claims description 8
- 102000004190 Enzymes Human genes 0.000 claims description 8
- 239000000956 alloy Substances 0.000 claims description 8
- 229910045601 alloy Inorganic materials 0.000 claims description 8
- 108090000637 alpha-Amylases Proteins 0.000 claims description 8
- 235000019418 amylase Nutrition 0.000 claims description 8
- 108010089934 carbohydrase Proteins 0.000 claims description 8
- 239000003054 catalyst Substances 0.000 claims description 8
- 230000002538 fungal effect Effects 0.000 claims description 8
- 239000012535 impurity Substances 0.000 claims description 8
- 239000003456 ion exchange resin Substances 0.000 claims description 8
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 8
- 229920002521 macromolecule Polymers 0.000 claims description 8
- 229910052759 nickel Inorganic materials 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000007599 discharging Methods 0.000 claims description 6
- 239000011552 falling film Substances 0.000 claims description 6
- 238000007701 flash-distillation Methods 0.000 claims 1
- 241000209140 Triticum Species 0.000 abstract description 8
- 235000021307 Triticum Nutrition 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 108090000623 proteins and genes Proteins 0.000 abstract description 3
- 102000004169 proteins and genes Human genes 0.000 abstract description 3
- 238000009413 insulation Methods 0.000 description 7
- 150000005846 sugar alcohols Chemical class 0.000 description 7
- 230000033228 biological regulation Effects 0.000 description 6
- 238000007670 refining Methods 0.000 description 5
- 239000003513 alkali Substances 0.000 description 4
- 206010012601 diabetes mellitus Diseases 0.000 description 3
- 230000000675 anti-caries Effects 0.000 description 2
- 239000010408 film Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 230000003020 moisturizing effect Effects 0.000 description 2
- GXCLVBGFBYZDAG-UHFFFAOYSA-N N-[2-(1H-indol-3-yl)ethyl]-N-methylprop-2-en-1-amine Chemical compound CN(CCC1=CNC2=C1C=CC=C2)CC=C GXCLVBGFBYZDAG-UHFFFAOYSA-N 0.000 description 1
- 240000000111 Saccharum officinarum Species 0.000 description 1
- 235000007201 Saccharum officinarum Nutrition 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 235000019219 chocolate Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 235000013325 dietary fiber Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000029219 regulation of pH Effects 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 235000011888 snacks Nutrition 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
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- Confectionery (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
The invention discloses a kind of preparation method of syrup special for moon cake, comprise the following steps：（1）Size mixing：By wheaten starch with cornstarch using weight ratio to be mixed；（2）Liquefaction；（3）Saccharification；（4）Centrifugation obtains saccharified liquid centrifugate；（5）Saccharified liquid filtrate is made in filtering；（6）Decolourize；（7）From friendship；（8）Malt syrup is made in evaporation；（9）Hydrogenation：After hydrogenation maltitol is obtained by refined, purification；（10）Compounding：By the step（9）Obtained maltitol is compounded with remaining malt syrup, obtains syrup special for moon cake.Using the preparation method of the present invention, abundant wheat resource can be made full use of, and the macromolecular such as pentosan and protein is removed by bipyramid horizontal screw centrifuge, improve the rate of filtration of subsequent handling, substantially reduce production cost, not only the economic benefit of enterprise had been improved but also had brought good social benefit, syrup special for moon cake of the present invention also has simple to operate.
Description
Technical field
The invention belongs to the production field of syrup, and in particular to a kind of syrup special for moon cake and preparation method thereof.
Background technology
Moon cake is a kind of traditional festival featured delicious food being loved by people, and its is with a long history, with the hair of food industry
Exhibition, the making of moon cake is developed by traditional handicraft workshop towards industrialized production direction, and its species also tends to diversification, market
On occur in that guang-type moon cake, capital formula moon cake, Soviet Union's formula moon cake, tidal moon cake and the new-type moon cake being combined with Western Culture.When
Preceding people eat moon cake and have been not limited solely to some red-letter day, and moon cake is enjoyed by people as a kind of leisure snack, except right
Its quality requirements, people increasingly focus on the nutrition of moon cake, health care.Moon cake primary raw material includes flour, carbohydrate, grease etc., sugar
Class is larger to moon cake qualitative effects, and the effect of moisturizing is may also function as in addition to as sweetener.Traditional moon cake syrup is with sugarcane
Based on sugar, but the characteristics of because of moon cake " high sugar, high heat ", many crowd's inedibilities are caused.
The content of the invention
For problems of the prior art, the present invention provides a kind of syrup special for moon cake and preparation method thereof, this hair
Bright obtained moon cake candy is adapted to many people and eaten.
To achieve the above object, the present invention uses following technical scheme：
A kind of preparation method of syrup special for moon cake, comprises the following steps：（1）Size mixing：By wheaten starch and cornstarch
Using weight ratio as 1.2：1-3：1 is mixed, and is added water and is sized mixing to 16~20 Baume degrees, and mixing starch slurries are made；（2）Liquefaction：
The pH to 5.6~6.0 of mixing starch slurries is adjusted, high temperature resistant α~0.3~0.5 ㎏ of amylase/ton butt is then added, passes through
Continuous injection makes mixing starch slurries liquefy twice；The first time injection temperation is 105~109 DEG C, through flashing after liquefaction
Laminar flow tank is incubated 90~120min, and second of injection temperation is 125~130 DEG C, and the DE values for obtaining liquefier are 15~18%；（3）
Saccharification：By step（2）Obtained liquefier pH is adjusted to 4.2~4.4, adds carbohydrase 0.1~0.15L/ tons of butts, fungal enzymes
0.2~0.25L/ tons of butts, 0.1~0.2L/ tons of butts of Pullulanase, 18~20 hours are incubated at 60-62 DEG C, gained saccharification
The DE values of liquid are 60~65%；（4）Centrifugation：By step（3）Obtained saccharified liquid is pumped into bipyramid horizontal screw centrifuge, is in rotating speed
Macromolecular substances in saccharified liquid are removed under 3000-3500r/min, saccharified liquid centrifugate is obtained；（5）Filtering：To the step（4）
0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press, the saccharified liquid
Temperature be 65~70 DEG C, the pressure of plate and frame filter press be 0.2~0.4Mpa, saccharified liquid filtrate is made；（6）Decolourize：By step
（5）The saccharified liquid filtrate of gained further filters decolouring by Ah agate's filter, and the temperature of the saccharified liquid filtrate is 75~80
℃；（7）From friendship：The temperature for adjusting saccharified liquid filtrate is 45~50 DEG C, by highly acidic cation → weakly-basic anion → strong acid
Property cation → weakly-basic anion order by ion exchange resin remove saccharified liquid filtrate in impurity, it is described from friendship after
The discharging electrical conductivity of saccharified liquid≤50 μ s/cm, pH are 4.5~5.0；（8）Evaporation：By the step（7）From the saccharified liquid after friendship
It is pumped into five effect falling film evaporators and is evaporated and be concentrated into mass percentage concentration for 45~50%, the drop temperature is 75~80 DEG C,
Malt syrup is made；（9）Hydrogenation：Take the step（8）The malt syrup of the percentage by volume 45~50% of malt syrup is made,
Addition takes malt syrup mass percentage concentration 0.3-0.7% nickel alumin(i)um alloys as catalyst, enters under 5.0~8.0Mpa pressure
Row malt syrup is hydrogenated with, and obtaining maltitol delicate mouthfeel, sugariness by refined, purification after hydrogenation declines, diabetic
It is edible；（10）Compounding：By the step（9）Obtained maltitol is compounded with remaining malt syrup, obtains moon cake special
Use syrup.
Syrup special for moon cake made from a kind of preparation method of syrup special for moon cake contains following components：Maltitol 40-
42%th, maltose 50-55%, trisaccharide and trisaccharide above 3-10%.
Compared with prior art, beneficial effects of the present invention are：1. using the preparation method of the present invention, it can make full use of
Abundant wheat resource, and the macromolecular such as pentosan and protein is removed by bipyramid horizontal screw centrifuge, improve subsequent handling
The rate of filtration, substantially reduces production cost, has not only improved the economic benefit of enterprise but also has brought good social benefit, the present invention
Syrup special for moon cake also have it is simple to operate, the features such as easy to use；2. the syrup special for moon cake after present invention compounding, which has, forms sediment
The characteristic of pulverized sugar：Mouthfeel sugariness is 0.7 times of sucrose；Due to containing maltose, has malty fragrance；Because using maltitol
Compounded with malt syrup, make syrup mouthfeel soft and feel with the exquisiteness similar in appearance to chocolate；Due to containing DP2,
DP3, more than DP4 sugar cause syrup special for moon cake to have the function of anti-caries；3. syrup special for moon cake of the present invention is adapted to diabetes
People eats, and the dietary fiber in syrup meets effect of functional sugar, can breed the profitable strain in human body intestinal canal, play health care
Effect, baby, children, pregnant, middle old man can safe edible, in a word, syrup special for moon cake of the present invention be collect moon cake mouthfeel, battalion
The features such as foster, moisturizing, health care, anti-caries and Shelf-life, is in the special high-quality syrup of moon cake of one.
Embodiment
Embodiment 1
The preparation method of the present embodiment syrup special for moon cake, comprises the following steps：（1）Size mixing：By wheaten starch and corn
Starch is using weight ratio as 1.2：1 is mixed, and is added water and is sized mixing to 16 Baume degrees, and mixing starch slurries are made；（2）Liquefaction：Regulation
The pH of mixing starch slurries to 5.6, then adds high temperature resistant α~0.3 ㎏ of amylase/ton butt, is made by continuous injection twice
Mixing starch slurries liquefy；The first time injection temperation is 105 DEG C, through flashing after liquefaction laminar flow tank insulation 90min, second
Secondary injection temperation is 125 DEG C, and the DE values for obtaining liquefier are 15%；（3）Saccharification：By step（2）Obtained liquefier pH adjust to
4.2,0.1L/ tons of butts of carbohydrase, 0.2L/ tons of butts of fungal enzyme, 0.1L/ tons of butts of Pullulanase are added, are incubated at 60 DEG C
18 hours, the DE values of gained saccharified liquid were 60%；（4）Centrifugation：By step（3）Obtained saccharified liquid is pumped into bipyramid horizontal screw centrifuge,
The macromolecular substances such as protein, obtain saccharified liquid centrifugate in saccharified liquid is removed under rotating speed is 3000r/min；（5）Filtering：To
The step（4）0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press,
The temperature of the saccharified liquid is 65 DEG C, the pressure of plate and frame filter press is 0.2Mpa, and saccharified liquid filtrate is made；（6）Decolourize：By step
（5）The saccharified liquid filtrate of gained further filters decolouring by Ah agate's filter, and the temperature of the saccharified liquid filtrate is 75 DEG C；
（7）From friendship：The temperature for adjusting saccharified liquid filtrate is 45 DEG C, by highly acidic cation → weakly-basic anion → highly acidic cation
The order of → weakly-basic anion removes the impurity in saccharified liquid filtrate by ion exchange resin, described from saccharified liquid after friendship
The electrical conductivity that discharges is that 50 μ s/cm, pH are 4.5；（8）Evaporation：By the step（7）Five effect falling liquid films are pumped into from the saccharified liquid after friendship to steam
It is 45% that hair device, which is evaporated and is concentrated into mass percentage concentration, and the drop temperature is 75 DEG C, and malt syrup is made；（9）Hydrogenation：
Take the step（8）The malt syrup of the percentage by volume 45% of malt syrup is made, addition takes malt syrup quality percentage dense
The nickel alumin(i)um alloy of degree 0.3% carries out malt syrup hydrogenation, by refining, carrying after hydrogenation as catalyst under 5.0~Mpa pressure
It is pure to obtain maltitol；（10）Compounding：By the step（9）Obtained maltitol is compounded with remaining malt syrup,
Obtain syrup special for moon cake.
Contain following components according to syrup special for moon cake made from the preparation method of the present embodiment syrup special for moon cake：Malt
More than sugar alcohol 40%, maltose 50%, trisaccharide and trisaccharide 10%.
Embodiment 2
The preparation method of the present embodiment syrup special for moon cake, comprises the following steps：（1）Size mixing：By wheaten starch and corn
Starch is using weight ratio as 1.5：1 is mixed, and is added water and is sized mixing to 18 Baume degrees, and mixing starch slurries are made；（2）Liquefaction：Regulation
The pH of mixing starch slurries to 5.8, then adds high temperature resistant α~0.4 ㎏ of amylase/ton butt, is made by continuous injection twice
Mixing starch slurries liquefy；The first time injection temperation is 106 DEG C, through flashing after liquefaction laminar flow tank insulation 95min, second
Secondary injection temperation is 126 DEG C, and the DE values for obtaining liquefier are 17%；（3）Saccharification：By step（2）Obtained liquefier pH adjust to
4.3,0.12L/ tons of butts of carbohydrase, 0.22L/ tons of butts of fungal enzyme, 0.11L/ tons of butts of Pullulanase are added, are protected at 61 DEG C
Temperature 19 hours, the DE values of gained saccharified liquid are 62%；（4）Centrifugation：By step（3）Obtained saccharified liquid is pumped into the sleeping spiral shell centrifugation of bipyramid
Machine, the macromolecular substances in saccharified liquid is removed under rotating speed is 3200r/min, obtains saccharified liquid centrifugate；（5）Filtering：To described
Step（4）0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press, it is described
The temperature of saccharified liquid is 68 DEG C, the pressure of plate and frame filter press is 0.25Mpa, and saccharified liquid filtrate is made；（6）Decolourize：By step（5）
The saccharified liquid filtrate of gained further filters decolouring by Ah agate's filter, and the temperature of the saccharified liquid filtrate is 78 DEG C；（7）From
Hand over：The temperature for adjusting saccharified liquid filtrate is 46 DEG C, by highly acidic cation → weakly-basic anion → highly acidic cation → weak
The order of alkali anion removes the impurity in saccharified liquid filtrate, the discharging from saccharified liquid after friendship by ion exchange resin
Electrical conductivity is that 48 μ s/cm, pH are 4.6；（8）Evaporation：By the step（7）Five effect falling film evaporators are pumped into from the saccharified liquid after friendship
It is 46% to be evaporated and be concentrated into mass percentage concentration, and the drop temperature is 77 DEG C, and malt syrup is made；（9）Hydrogenation：Take institute
State step（8）The malt syrup of the percentage by volume 48% of malt syrup is made, addition takes malt syrup mass percentage concentration
0.6% nickel alumin(i)um alloy carries out malt syrup hydrogenation, by refining, purifying after hydrogenation as catalyst under 6.0Mpa pressure
To maltitol（Diabetic patients, delicate mouthfeel, sugariness decline）；（10）Compounding：By the step（9）Obtained wheat
Bud sugar alcohol is compounded with remaining malt syrup, obtains syrup special for moon cake.
According to syrup special for moon cake made from the preparation method of the present embodiment syrup special for moon cake, contain following components：Wheat
More than bud sugar alcohol 42%, maltose 55%, trisaccharide and trisaccharide 3%.
Embodiment 3
The preparation method of the present embodiment syrup special for moon cake, comprises the following steps：（1）Size mixing：By wheaten starch and corn
Starch is using weight ratio as 2：1 is mixed, and is added water and is sized mixing to 18 Baume degrees, and mixing starch slurries are made；（2）Liquefaction：Regulation is mixed
The pH to 5.8 of farinaceous size is closed, high temperature resistant α~0.3 ㎏ of amylase/ton butt is then added, makes to mix by continuous injection twice
Close farinaceous size liquefaction；The first time injection temperation is 107 DEG C, through flashing after liquefaction laminar flow tank insulation 100min, second
Secondary injection temperation is 126 DEG C, and the DE values for obtaining liquefier are 17%；（3）Saccharification：By step（2）Obtained liquefier pH adjust to
4.2,0.1L/ tons of butts of carbohydrase, 0.23L/ tons of butts of fungal enzyme, 0.15L/ tons of butts of Pullulanase are added, are protected at 62 DEG C
Temperature 20 hours, the DE values of gained saccharified liquid are 63%；（4）Centrifugation：By step（3）Obtained saccharified liquid is pumped into the sleeping spiral shell centrifugation of bipyramid
Machine, the macromolecular substances in saccharified liquid is removed under rotating speed is 3300r/min, obtains saccharified liquid centrifugate；（5）Filtering：To described
Step（4）0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press, it is described
The temperature of saccharified liquid is 68 DEG C, the pressure of plate and frame filter press is 0.4Mpa, and saccharified liquid filtrate is made；（6）Decolourize：By step（5）
The saccharified liquid filtrate of gained further filters decolouring by Ah agate's filter, and the temperature of the saccharified liquid filtrate is 80 DEG C；（7）From
Hand over：The temperature for adjusting saccharified liquid filtrate is 50 DEG C, by highly acidic cation → weakly-basic anion → highly acidic cation → weak
The order of alkali anion removes the impurity in saccharified liquid filtrate, the discharging from saccharified liquid after friendship by ion exchange resin
Electrical conductivity is that 40 μ s/cm, pH are 5.0；（8）Evaporation：By the step（7）Five effect falling film evaporators are pumped into from the saccharified liquid after friendship
It is 48% to be evaporated and be concentrated into mass percentage concentration, and the drop temperature is 78 DEG C, and malt syrup is made；（9）Hydrogenation：Take institute
State step（8）The malt syrup of the percentage by volume 46% of malt syrup is made, addition takes malt syrup mass percentage concentration
0.5% nickel alumin(i)um alloy carries out malt syrup hydrogenation, by refining, purifying after hydrogenation as catalyst under 7.0Mpa pressure
To maltitol；（10）Compounding：By the step（9）Obtained maltitol is compounded with remaining malt syrup, is obtained
Syrup special for moon cake.
According to syrup special for moon cake made from the preparation method of the present embodiment syrup special for moon cake, contain following components：Wheat
More than bud sugar alcohol 41%, maltose 54%, trisaccharide and trisaccharide 5%.
Embodiment 4
The preparation method of the present embodiment syrup special for moon cake, comprises the following steps：（1）Size mixing：By wheaten starch and corn
Starch is using weight ratio as 3：1 is mixed, and is added water and is sized mixing to 20 Baume degrees, and mixing starch slurries are made；（2）Liquefaction：Regulation is mixed
The pH to 6.0 of farinaceous size is closed, high temperature resistant α~0.5 ㎏ of amylase/ton butt is then added, makes to mix by continuous injection twice
Close farinaceous size liquefaction；The first time injection temperation is 109 DEG C, through flashing after liquefaction laminar flow tank insulation 120min, second
Secondary injection temperation is 130 DEG C, and the DE values for obtaining liquefier are 18%；（3）Saccharification：By step（2）Obtained liquefier pH adjust to
4.4,0.15L/ tons of butts of carbohydrase, 0.25L/ tons of butts of fungal enzyme, 0.2L/ tons of butts of Pullulanase are added, are protected at 62 DEG C
Temperature 20 hours, the DE values of gained saccharified liquid are 65%；（4）Centrifugation：By step（3）Obtained saccharified liquid is pumped into the sleeping spiral shell centrifugation of bipyramid
Machine, the macromolecular substances in saccharified liquid is removed under rotating speed is 3500r/min, obtains saccharified liquid centrifugate；（5）Filtering：To described
Step（4）0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press, it is described
The temperature of saccharified liquid is 70 DEG C, the pressure of plate and frame filter press is 0.4Mpa, and saccharified liquid filtrate is made；（6）Decolourize：By step（5）
The saccharified liquid filtrate of gained further filters decolouring by Ah agate's filter, and the temperature of the saccharified liquid filtrate is 80 DEG C；（7）From
Hand over：The temperature for adjusting saccharified liquid filtrate is 50 DEG C, by highly acidic cation → weakly-basic anion → highly acidic cation → weak
The order of alkali anion removes the impurity in saccharified liquid filtrate, the discharging from saccharified liquid after friendship by ion exchange resin
Electrical conductivity is that 30 μ s/cm, pH are 4.5；（8）Evaporation：By the step（7）Five effect falling film evaporators are pumped into from the saccharified liquid after friendship
It is 50% to be evaporated and be concentrated into mass percentage concentration, and the drop temperature is 80 DEG C, and malt syrup is made；（9）Hydrogenation：Take institute
State step（8）The malt syrup of the percentage by volume 50% of malt syrup is made, addition takes malt syrup mass percentage concentration
0.7% nickel alumin(i)um alloy carries out malt syrup hydrogenation, by refining, purifying after hydrogenation as catalyst under 8.0Mpa pressure
To maltitol；（10）Compounding：By the step（9）Obtained maltitol is compounded with remaining malt syrup, is obtained
Syrup special for moon cake.
According to syrup special for moon cake made from the preparation method of the present embodiment syrup special for moon cake, contain following components：Wheat
More than bud sugar alcohol 42%, maltose 50%, trisaccharide and trisaccharide 8%.
Embodiment 5
The preparation method of the present embodiment syrup special for moon cake, comprises the following steps：（1）Size mixing：By wheaten starch and corn
Starch is using weight ratio as 2.5：1 is mixed, and is added water and is sized mixing to 17 Baume degrees, and mixing starch slurries are made；（2）Liquefaction：Regulation
The pH of mixing starch slurries to 5.7, then adds high temperature resistant α~0.5 ㎏ of amylase/ton butt, is made by continuous injection twice
Mixing starch slurries liquefy；The first time injection temperation is 108 DEG C, through flashing after liquefaction laminar flow tank insulation 110min, the
Secondary injection temperature is 128 DEG C, and the DE values for obtaining liquefier are 17%；（3）Saccharification：By step（2）Obtained liquefier pH regulations
To 4.3,0.14L/ tons of butts of carbohydrase, 0.22L/ tons of butts of fungal enzyme, 0.16L/ tons of butts of Pullulanase are added, at 61 DEG C
Insulation 18 hours, the DE values of gained saccharified liquid are 60%；（4）Centrifugation：By step（3）Obtained saccharified liquid be pumped into bipyramid crouch spiral shell from
Scheming, the macromolecular substances in saccharified liquid is removed under rotating speed is 3400r/min, obtains saccharified liquid centrifugate；（5）Filtering：To institute
State step（4）0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press, institute
The temperature for stating saccharified liquid is 69 DEG C, the pressure of plate and frame filter press is 0.3Mpa, and saccharified liquid filtrate is made；（6）Decolourize：By step
（5）The saccharified liquid filtrate of gained further filters decolouring by Ah agate's filter, and the temperature of the saccharified liquid filtrate is 76 DEG C；
（7）From friendship：The temperature for adjusting saccharified liquid filtrate is 47 DEG C, by highly acidic cation → weakly-basic anion → highly acidic cation
The order of → weakly-basic anion removes the impurity in saccharified liquid filtrate by ion exchange resin, described from saccharified liquid after friendship
The electrical conductivity that discharges is that 40 μ s/cm, pH are 4.6；（8）Evaporation：By the step（7）Five effect falling liquid films are pumped into from the saccharified liquid after friendship to steam
It is 48% that hair device, which is evaporated and is concentrated into mass percentage concentration, and the drop temperature is 78 DEG C, and malt syrup is made；（9）Hydrogenation：
Take the step（8）The malt syrup of the percentage by volume 48% of malt syrup is made, addition takes malt syrup quality percentage dense
The nickel alumin(i)um alloy of degree 0.5% carries out malt syrup hydrogenation as catalyst under 6.0Mpa pressure, by refined, purification after hydrogenation
Obtain maltitol；（10）Compounding：By the step（9）Obtained maltitol is compounded with remaining malt syrup, is obtained
To syrup special for moon cake.
According to syrup special for moon cake made from the preparation method of the present embodiment syrup special for moon cake, contain following components：Wheat
More than bud sugar alcohol 41.5%, maltose 53.5%, trisaccharide and trisaccharide 5%.
Embodiment 6
The preparation method of the present embodiment syrup special for moon cake, comprises the following steps：（1）Size mixing：By wheaten starch and corn
Starch is using weight ratio as 3：1 is mixed, and is added water and is sized mixing to 18 Baume degrees, and mixing starch slurries are made；（2）Liquefaction：Regulation is mixed
The pH to 5.6 of farinaceous size is closed, high temperature resistant α~0.4 ㎏ of amylase/ton butt is then added, makes to mix by continuous injection twice
Close farinaceous size liquefaction；The first time injection temperation is 106 DEG C, through flashing after liquefaction laminar flow tank insulation 110min, second
Secondary injection temperation is 128 DEG C, and the DE values for obtaining liquefier are 17%；（3）Saccharification：By step（2）Obtained liquefier pH adjust to
4.3,0.13L/ tons of butts of carbohydrase, 0.24L/ tons of butts of fungal enzyme, 0.18L/ tons of butts of Pullulanase are added, are protected at 60 DEG C
Temperature 18 hours, the DE values of gained saccharified liquid are 64%；（4）Centrifugation：By step（3）Obtained saccharified liquid is pumped into the sleeping spiral shell centrifugation of bipyramid
Machine, the macromolecular substances in saccharified liquid is removed under rotating speed is 3500r/min, obtains saccharified liquid centrifugate；（5）Filtering：To described
Step（4）0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press, it is described
The temperature of saccharified liquid is 66 DEG C, the pressure of plate and frame filter press is 0.35Mpa, and saccharified liquid filtrate is made；（6）Decolourize：By step（5）
The saccharified liquid filtrate of gained further filters decolouring by Ah agate's filter, and the temperature of the saccharified liquid filtrate is 76 DEG C；（7）From
Hand over：The temperature for adjusting saccharified liquid filtrate is 47 DEG C, by highly acidic cation → weakly-basic anion → highly acidic cation → weak
The order of alkali anion removes the impurity in saccharified liquid filtrate, the discharging from saccharified liquid after friendship by ion exchange resin
Electrical conductivity is that 45 μ s/cm, pH are 4.7；（8）Evaporation：By the step（7）Five effect falling film evaporators are pumped into from the saccharified liquid after friendship
It is 48% to be evaporated and be concentrated into mass percentage concentration, and the drop temperature is 77 DEG C, and malt syrup is made；（9）Hydrogenation：Take institute
State step（8）The malt syrup of the percentage by volume 49% of malt syrup is made, addition takes malt syrup mass percentage concentration
0.6% nickel alumin(i)um alloy carries out malt syrup hydrogenation, by refining, purifying after hydrogenation as catalyst under 7.0Mpa pressure
To maltitol；（10）Compounding：By the step（9）Obtained maltitol is compounded with remaining malt syrup, is obtained
Syrup special for moon cake.
According to syrup special for moon cake made from the preparation method of the present embodiment syrup special for moon cake, contain following components：Wheat
More than bud sugar alcohol 41%, maltose 51%, trisaccharide and trisaccharide 8%.
Claims (2)
1. a kind of preparation method of syrup special for moon cake, it is characterised in that comprise the following steps：（1）Size mixing：By wheaten starch with
Cornstarch is using weight ratio as 1.2：1-3：1 is mixed, and is added water and is sized mixing to 16~20 Baume degrees, and mixing starch slurries are made；
（2）Liquefaction：The pH to 5.6~6.0 of mixing starch slurries is adjusted, high temperature resistant α~0.3~0.5 ㎏ of amylase/ton is then added and does
Base, makes mixing starch slurries liquefy by continuous injection twice；The first time injection temperation is 105~109 DEG C, after flash distillation
90~120min being incubated in liquefaction laminar flow tank, second injection temperation is 125~130 DEG C, the DE values for obtaining liquefier are 15~
18%；（3）Saccharification：By step（2）Obtained liquefier pH is adjusted to 4.2~4.4, is added 0.1~0.15L/ tons of carbohydrase and is done
Base, 0.2~0.25L/ tons of butts of fungal enzyme, 0.1~0.2L/ tons of butts of Pullulanase, are incubated 18~20 small at 60-62 DEG C
When, the DE values of gained saccharified liquid are 60~65%；（4）Centrifugation：By step（3）Obtained saccharified liquid is pumped into bipyramid horizontal screw centrifuge,
The macromolecular substances in saccharified liquid is removed under rotating speed is 3000-3500r/min, obtain saccharified liquid centrifugate；（5）Filtering：To institute
State step（4）0.1 ㎏ of diatomite/ton butt is added in obtained saccharified liquid centrifugate, is filtered using plate and frame filter press, institute
The temperature for stating saccharified liquid is 65~70 DEG C, the pressure of plate and frame filter press is 0.2~0.4MPa, and saccharified liquid filtrate is made；（6）It is de-
Color：By step（5）The saccharified liquid filtrate of gained further filters decolouring, the temperature of the saccharified liquid filtrate by Ah agate's filter
For 75~80 DEG C；（7）From friendship：The temperature for adjusting saccharified liquid filtrate is 45~50 DEG C, by highly acidic cation → alkalescent it is cloudy from
The order of son → highly acidic cation → weakly-basic anion removes the impurity in saccharified liquid filtrate, institute by ion exchange resin
It is 4.5~5.0 to state discharging electrical conductivity from saccharified liquid after friendship≤50 μ s/cm, pH；（8）Evaporation：By the step（7）After friendship
Saccharified liquid be pumped into five effect falling film evaporators and be evaporated and be concentrated into mass percentage concentration for 45~50%, the drop temperature is
75~80 DEG C, malt syrup is made；（9）Hydrogenation：Take the step（8）The percentage by volume 45~50% of malt syrup is made
Malt syrup, adds and takes malt syrup mass percentage concentration 0.3-0.7% nickel alumin(i)um alloy as catalyst, 5.0~
Malt syrup hydrogenation is carried out under 8.0MPa pressure, maltitol is obtained by refined, purification after hydrogenation；（10）Compounding：Will be described
Step（9）Obtained maltitol is compounded with remaining malt syrup, obtains syrup special for moon cake.
2. syrup special for moon cake made from a kind of preparation method according to the syrup special for moon cake described in claim 1, its feature
It is：Contain following components in the syrup special for moon cake：Maltitol 40-42%, maltose 50-55%, trisaccharide and trisaccharide with
Upper 3-10%.
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105475583A (en) * | 2015-12-28 | 2016-04-13 | 河南飞天农业开发股份有限公司 | Production process for syrup special for chocolate |
| CN105482933B (en) * | 2015-12-28 | 2018-07-03 | 河南飞天农业开发股份有限公司 | A kind of preparation method of high-attenuation degree beer syrup |
| CN106259597A (en) * | 2016-08-06 | 2017-01-04 | 安徽老约翰食品有限公司 | A kind of baking processes the special malt sugar of moon cake |
| CN106720838A (en) * | 2016-12-22 | 2017-05-31 | 河南飞天农业开发股份有限公司 | A kind of syrup dedicated production method of nougat |
| CN109043487A (en) * | 2018-07-18 | 2018-12-21 | 合肥华盖生物科技有限公司 | A kind of special syrup for bread and preparation method thereof |
| CN109090574A (en) * | 2018-07-18 | 2018-12-28 | 合肥华盖生物科技有限公司 | A kind of honey is syrup dedicated and preparation method thereof |
| CN111455000A (en) * | 2020-04-16 | 2020-07-28 | 黑龙江昊天玉米开发有限公司 | Preparation method of corn-made maltose syrup |
| CN112322680A (en) * | 2020-11-12 | 2021-02-05 | 河南飞天农业开发股份有限公司 | Maltose preparation process |
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