CN104497873A - High-gloss environment-friendly natural wood oil and preparation method thereof - Google Patents
High-gloss environment-friendly natural wood oil and preparation method thereof Download PDFInfo
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- CN104497873A CN104497873A CN201410741027.6A CN201410741027A CN104497873A CN 104497873 A CN104497873 A CN 104497873A CN 201410741027 A CN201410741027 A CN 201410741027A CN 104497873 A CN104497873 A CN 104497873A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D191/00—Coating compositions based on oils, fats or waxes; Coating compositions based on derivatives thereof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/46—Anti-skinning agents
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention relates to high-gloss environment-friendly natural wood oil which comprises the following components in parts by weight: 20-35 parts of vegetable oil, 20-30 parts of natural vegetable resin, 40-60 parts of an environment-friendly solvent, 0.1-0.5 part of an anti-skinning agent and 1-3 parts of an environment-friendly drier, wherein the vegetable oil is one or more of crude tung oil, linseed oil and soybean oil. The components of the oil provided by the invention are environment-friendly components and the vegetable oil, the natural vegetal resin and the environment-friendly solvent are natural vegetable extracts, so that the oil is environment-friendly and pollution-free; a coating formed by matching the vegetable oil and the natural vegetable resin has extremely high glossiness as well as excellent adhesive force, hardness, weather resistance, water resistance and wear resistance, so that the oil can be widely applied to protecting and decorating indoor and outdoor timbers and wooden products.
Description
Technical field
What the present invention relates to is Environment-friendlynatural natural wood oil, and what especially relate to is a kind of high gloss Environment-friendlynatural natural wood oil and preparation method thereof.
Background technology
Now, common wood oil, whether-resisting wood oil are all developed by tung oil or Synolac, all there are some shortcomings:
(1) all contain organic solvent VOC, comprising: toluene, dimethylbenzene, solvent oil, formaldehyde, ethanol etc.; In various degree containing the heavy metal objectionable impurities such as lead, cobalt, manganese, arsenic, selenium;
(2) wood oil based on tung oil or whether-resisting wood oil, its distinctive tung oil taste is heavier, is difficult to remove; Glossiness is general, and decorative effect is bad; Perviousness is poor, cannot go deep into wood surface, can not protect well; Time of drying is slow, even needs 2-5 days ability to do solid work completely, can not meet construction requirement well; Manufacturing technique requirent is high, causes cost higher;
(3) wood oil based on Synolac or whether-resisting wood oil, its weathering resistance, water tolerance, yellowing resistance are poor, can not play long-lived effect; Poor permeability, can only form one deck paint film on surface, to wood preservation poor effect;
(4) Chinese patent " 201210065719.4 " discloses a kind of by IPDI modified soyabean oil urushiol acid resin, the environmental protection wood oil of simple dilution is carried out using hydrocarbon-containifirst solvent as thinner, similar with traditional paint, VOC content is high, really cannot accomplish nontoxic pollution-free, and perviousness is poor, weather resistance is poor;
(5) Chinese patent " 200610062061.6 " discloses and a kind of carries out by tung oil chemical reagent such as poly-merga pass Tianna solution under 300-320 DEG C of high temperature the whether-resisting wood oil diluted, VOC content is high, glossiness is lower, time of drying is slow and be polymerized for a long time through high temperature, molecular weight is large, poor permeability, protection effect is poor; , under high temperature, there is potential safety hazard in complex manufacturing.
Summary of the invention
The object of the invention is to overcome current wood oil Problems existing, providing a kind of and have that high gloss, perviousness are strong, the high gloss Environment-friendlynatural natural wood oil of good weatherability, fast drying, pure natural and preparation method thereof.
For achieving the above object, technical solution of the present invention is: a kind of high gloss Environment-friendlynatural natural wood oil, comprises the component of following parts by weight:
Vegetables oil 20-35 parts
Natural phant resin 20-30 parts
Environmentally friendly solvent 40-60 parts
Anti-skinning agent 0.1-0.5 part
Environmental protection siccative 1-3 parts.
Preferably, described vegetables oil is made a living one or more in tung oil, oleum lini and soybean oil.
Preferably, described vegetables oil comprises oleum lini 5-20 parts, raw tung oil 15-30 parts.
Preferably, described natural phant resin is one or more in terpine resin, dammar gum and modified rosin resin.
Preferably, described environmentally friendly solvent is D-hesperidene.
Preferably, described anti-skinning agent is Diacetylmonoxime.
Preferably, described environmental protection siccative is rare earth drier.
The preparation method of high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
A, take each component by described parts by weight;
B, vegetables oil is being placed in prepolymerization under 220-260 ° of C environment until viscosity reaches 10,000-2 ten thousand Pas;
C, by environment temperature reduction to 150-160 DEG C, add natural phant resin agitating dissolve after, be again cooled to 80-90 DEG C, add environmentally friendly solvent, anti-skinning agent and environmental protection siccative, mixing and stirring;
D, be down to normal temperature filter.
Preferably, the vegetables oil that described step a takes includes oleum lini 5-20 parts, raw tung oil 15-30 parts, the concrete pre-polymerization process of described step b is: prepolymerization 4-6 hours at first oleum lini being placed in 240-260 DEG C, add raw tung oil again to stir evenly, be polymerized 1-1.5 hours under the condition of 220-240 DEG C.
Preferably, oleum lini described in step b, prepolymerization 5 hours at 245 DEG C.
Beneficial effect of the present invention: the present invention with the addition of the natural phant resin of self-drying type, improves the hardness of coating, accelerates the rate of drying from dry vegetable oil simultaneously, normal temperature gets final product surface drying in lower 3 hours, within 6-10 hours, can do solid work; The D-limonene extracted in natural fruit, vegetables and spices, as solvent, adds the perviousness of wood oil, and makes this product odour pure and fresh pleasant, really accomplishes Pure natural nontoxic environmental protection; Reach the reduction polymerization degree by the polymerization temperature reducing vegetables oil, the perviousness of vegetables oil can be added well, better timber and woodwork are protected; Add natural phant resin, make product improve a class on the basis of siccative oil poor gloss degree, reach high gloss.Adopt oleum lini and raw tung oil with the use of, oleum lini helps to control raw tung oil polymerization.
In preparation method, reduce polymerization temperature, make whole process be in controlled range, reduce potential risks, reduce the comprehensive cost of whole product, increase economic efficiency.
Embodiment
For a better understanding of the present invention, below by specific embodiment, the present invention is further described.
embodiment 1:
A preparation method for high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
Measure according to parts by weight: oleum lini 5 parts, raw tung oil 20 parts, terpine resin 15 parts, D-limonene 58.7 parts, Diacetylmonoxime 0.1 part, rare earth drier 1.2 parts; At oleum lini being placed in 240 DEG C, prepolymerization is after 5 hours, adds raw tung oil fast and stirs, and is cooled to 225 DEG C and carries out insulation 1 hour; Again be cooled to 150 DEG C, add terpine resin fast, stirring and dissolving; Be cooled to 80 DEG C further, add D-limonene, Diacetylmonoxime and rare earth drier fast, dispersed with stirring is even, is finally down to normal temperature and filters, can obtain this product.
embodiment 2:
A preparation method for high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
Measure according to parts by weight: oleum lini 5 parts, raw tung oil 25 parts, terpine resin 15 parts, dammar gum 10 parts, D-limonene 43.4 parts, Diacetylmonoxime 0.4 part, rare earth drier 1.2 parts; At oleum lini being placed in 245 DEG C, prepolymerization is after 5 hours, adds raw tung oil fast and stirs, and is cooled to 220 DEG C and carries out insulation 1.5 hours; Again be cooled to 160 DEG C, add terpine resin and dammar gum fast, stirring and dissolving; Be cooled to 90 DEG C further, add D-limonene, Diacetylmonoxime and rare earth drier fast, dispersed with stirring is even, is finally down to normal temperature and filters, can obtain this product.
embodiment 3:
A preparation method for high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
Measure according to parts by weight: oleum lini 7.5 parts, soybean oil 17.5 parts, modified rosin resin 15 parts, D-limonene 58.4 parts, Diacetylmonoxime 0.1 part, rare earth drier 1.5 parts; At oleum lini being placed in 260 DEG C, prepolymerization is after 4.5 hours, adds raw tung oil fast and stirs, and is cooled to 240 DEG C and carries out insulation 1.5 hours; Again be cooled to 150 DEG C, add modified rosin resin fast, stirring and dissolving; Be cooled to 80 DEG C further, add D-limonene, Diacetylmonoxime and rare earth drier fast, dispersed with stirring is even, is finally down to normal temperature and filters, can obtain this product.
embodiment 4:
A preparation method for high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
Get according to parts by weight quantity: soybean oil 5 parts, raw tung oil 20 parts, terpine resin 10 parts, dammar gum 10 parts, modified rosin resin 10 parts, D-limonene 43.5 parts, Diacetylmonoxime 0.2 part, rare earth drier 1.3 parts; At soybean oil being placed in 250 DEG C, prepolymerization is after 4 hours, adds raw tung oil fast and stirs, and is cooled to 230 DEG C and carries out insulation 1.5 hours; Again be cooled to 150 DEG C, add terpine resin and modified rosin resin fast, stirring and dissolving; Be cooled to 85 DEG C further, add D-limonene, Diacetylmonoxime and rare earth drier fast, dispersed with stirring is even, is finally down to normal temperature and filters, can obtain this product.
embodiment 5:
A preparation method for high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
Measure according to parts by weight: raw tung oil 30 parts, terpine resin 20 parts, D-limonene 48 parts, Diacetylmonoxime 0.3 part, rare earth drier 1.7 parts; At life tung oil is placed in 240 DEG C, prepolymerization is after 4 hours; Be cooled to 155 DEG C, add modified rosin resin fast, stirring and dissolving; Be cooled to 80 DEG C further, add D-limonene, Diacetylmonoxime and rare earth drier fast, dispersed with stirring is even, is finally down to normal temperature and filters, can obtain this product.
embodiment 6:
A preparation method for high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
Measure according to parts by weight: soybean oil 35 parts, terpine resin 5 parts, dammar gum 15 parts, D-limonene 42.6 parts, Diacetylmonoxime 0.1 part, rare earth drier 2.3 parts; At soybean oil being placed in 240 DEG C, prepolymerization is after 4 hours; Be cooled to 150 DEG C, add modified rosin resin fast, stirring and dissolving; Be cooled to 80 DEG C further, add D-limonene, Diacetylmonoxime and rare earth drier fast, dispersed with stirring is even, is finally down to normal temperature and filters, can obtain this product.
embodiment 7:
A preparation method for high gloss Environment-friendlynatural natural wood oil, comprises the following steps:
Measure according to parts by weight: oleum lini 30 parts, terpine resin 20 parts, D-limonene 47.4 parts, Diacetylmonoxime 0.2 part, rare earth drier 2.4 parts; At oleum lini being placed in 240 DEG C, prepolymerization is after 4 hours; Be cooled to 150 DEG C, add modified rosin resin fast, stirring and dissolving; Be cooled to 80 DEG C further, add D-limonene, Diacetylmonoxime and rare earth drier fast, dispersed with stirring is even, is finally down to normal temperature and filters, can obtain this product.
The foregoing is only and be described in further detail the invention provides, and be not used to limit the scope of the invention, all various changes of doing within the spirit and principles in the present invention scope and improvement, all should be included within protection scope of the present invention.
Claims (10)
1. a high gloss Environment-friendlynatural natural wood oil, is characterized in that, comprises the component of following parts by weight:
Vegetables oil 20-35 parts
Natural phant resin 20-30 parts
Environmentally friendly solvent 40-60 parts
Anti-skinning agent 0.1-0.5 part
Environmental protection siccative 1-3 parts.
2. high gloss Environment-friendlynatural natural wood oil according to claim 1, is characterized in that: described vegetables oil make a living in tung oil, oleum lini and soybean oil one or more.
3. high gloss Environment-friendlynatural natural wood oil according to claim 2, is characterized in that: described vegetables oil comprises oleum lini 5-20 parts, raw tung oil 15-30 parts.
4. high gloss Environment-friendlynatural natural wood oil according to claim 1, is characterized in that: described natural phant resin is one or more in terpine resin, dammar gum and modified rosin resin.
5. high gloss Environment-friendlynatural natural wood oil according to claim 1, is characterized in that: described environmentally friendly solvent is D-hesperidene.
6. high gloss Environment-friendlynatural natural wood oil according to claim 1, is characterized in that: described anti-skinning agent is Diacetylmonoxime.
7. high gloss Environment-friendlynatural natural wood oil according to claim 1, is characterized in that: described environmental protection siccative is rare earth drier.
8. the preparation method of high gloss Environment-friendlynatural natural wood oil according to claim 1-7, is characterized in that, comprise the following steps:
A, take each component by described parts by weight;
B, vegetables oil is being placed in prepolymerization under 220-260 ° of C environment until viscosity reaches 10,000-2 ten thousand Pas;
C, by environment temperature reduction to 150-160 DEG C, add natural phant resin agitating dissolve after, be again cooled to 80-90 DEG C, add environmentally friendly solvent, anti-skinning agent and environmental protection siccative, mixing and stirring;
D, be down to normal temperature filter.
9. the preparation method of high gloss Environment-friendlynatural natural wood oil according to claim 8, it is characterized in that, the vegetables oil that described step a takes includes oleum lini 5-20 parts, raw tung oil 15-30 parts, the concrete pre-polymerization process of described step b is: prepolymerization 4-6 hours at first oleum lini being placed in 240-260 DEG C, add after raw tung oil mixes thoroughly again, then be polymerized 1-1.5 hours under the condition of 220-240 DEG C.
10. the preparation method of high gloss Environment-friendlynatural natural wood oil according to claim 9, is characterized in that: oleum lini described in step b, prepolymerization 5 hours at 245 DEG C.
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Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104817874A (en) * | 2015-04-17 | 2015-08-05 | 陆开云 | Environmental-friendly drying agent for printing ink |
CN105038588A (en) * | 2015-07-03 | 2015-11-11 | 四川理工学院 | Environmentally-friendly wood wax oil and preparation method thereof |
CN105925188A (en) * | 2016-05-28 | 2016-09-07 | 常德湘联生物科技有限公司 | Environment-friendly emulsified modified tung-oil resin liquid and preparing method thereof |
CN106945142A (en) * | 2017-03-28 | 2017-07-14 | 安徽中煦环保新材料科技有限公司 | Environmentally friendly conserving material of a kind of solid wood furniture and preparation method thereof |
CN107057461A (en) * | 2017-03-22 | 2017-08-18 | 佛山市高明丰霖新型材料有限公司 | A kind of digital ceramic ink binder and preparation method thereof |
CN111019524A (en) * | 2019-12-17 | 2020-04-17 | 湖南林邑新能源有限公司 | Environment-friendly waterproof tung oil and preparation method thereof |
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Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104817874A (en) * | 2015-04-17 | 2015-08-05 | 陆开云 | Environmental-friendly drying agent for printing ink |
CN105038588A (en) * | 2015-07-03 | 2015-11-11 | 四川理工学院 | Environmentally-friendly wood wax oil and preparation method thereof |
CN105925188A (en) * | 2016-05-28 | 2016-09-07 | 常德湘联生物科技有限公司 | Environment-friendly emulsified modified tung-oil resin liquid and preparing method thereof |
CN105925188B (en) * | 2016-05-28 | 2018-04-10 | 常德湘联生物科技有限公司 | A kind of environment-friendly type emulsification modified tung oil resin liquid and preparation method thereof |
CN107057461A (en) * | 2017-03-22 | 2017-08-18 | 佛山市高明丰霖新型材料有限公司 | A kind of digital ceramic ink binder and preparation method thereof |
CN106945142A (en) * | 2017-03-28 | 2017-07-14 | 安徽中煦环保新材料科技有限公司 | Environmentally friendly conserving material of a kind of solid wood furniture and preparation method thereof |
CN111019524A (en) * | 2019-12-17 | 2020-04-17 | 湖南林邑新能源有限公司 | Environment-friendly waterproof tung oil and preparation method thereof |
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Application publication date: 20150408 |