CN104479836A - Concrete release agent prepared from mineral oil and preparation method of concrete release agent - Google Patents

Concrete release agent prepared from mineral oil and preparation method of concrete release agent Download PDF

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Publication number
CN104479836A
CN104479836A CN201410786398.6A CN201410786398A CN104479836A CN 104479836 A CN104479836 A CN 104479836A CN 201410786398 A CN201410786398 A CN 201410786398A CN 104479836 A CN104479836 A CN 104479836A
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CN
China
Prior art keywords
mineral oil
parts
release agent
concrete
deionized water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410786398.6A
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Chinese (zh)
Inventor
张勇飞
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MENGCHENG COUNTY TECHNOLOGY INNOVATION SERVICE CENTER
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MENGCHENG COUNTY TECHNOLOGY INNOVATION SERVICE CENTER
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Publication date
Application filed by MENGCHENG COUNTY TECHNOLOGY INNOVATION SERVICE CENTER filed Critical MENGCHENG COUNTY TECHNOLOGY INNOVATION SERVICE CENTER
Priority to CN201410786398.6A priority Critical patent/CN104479836A/en
Publication of CN104479836A publication Critical patent/CN104479836A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a concrete release agent prepared from mineral oil and a preparation method of the concrete release agent. The concrete release agent is prepared from the following raw materials in parts by weight: 40-45 parts of modified mineral oil, 25-30 parts of sodium laurate, 0.4-0.5 part of trilaurin, 2-4 parts of triethanolamine, 0.6-0.8 part of polyvinylpyrrolidone, 2-4 parts of magnesium sulfate, 1.5-2.0 parts of sodium hexametaphoshpate, 3-5 parts of cyclodextrin, 0.4-0.5 part of glucan, 5-10 parts of a silane coupling agent KH-500 and 250-280 parts of deionized water. With modified mineral oil as a main material, the chemical property is neutral; the prepared release agent has no peculiar smell and is good in demolding effect, free of corrosion to a template, non-toxic and odorless; the mold is low in concrete adhesion; and in addition, the assistants such as a coupling reagent, an emulsifier and a stabilizer are added, so that the prepared release agent has the characteristic of oil-water compatibility, can be widely applied to demolding of concrete parts, and is also suitable for various templates.

Description

A kind of concrete parting agent made with mineral oil and preparation method thereof
Technical field
The invention provides a kind of concrete parting agent, particularly a kind of concrete parting agent made with mineral oil and preparation method thereof.
Background technology
Concrete parting agent is also known as concrete isolation agent or demoulding lubricant; Be one be applied to template inwall rise lubrication and buffer action, make concrete can depart from template smoothly when form removal, keep the intact material of concrete shape, traditional release materials adds diesel oil with machine oil or used oil, find in the engineering constructions such as long-term water conservancy and hydropower, highway, railway, use used oil brushing template, concrete surface is produced and pollutes, pollution in various degree is also caused to environment simultaneously; But existing releasing agent exist stripping result not good, be difficult to remove in template, and ineffective to template maintenance, operating efficiency etc. is affected also increases construction cost.
Summary of the invention
The object of the present invention is to provide a kind of concrete parting agent made with mineral oil and preparation method thereof.
The present invention adopts following technical scheme to achieve these goals:
With the concrete parting agent that mineral oil is made, the weight part of its constitutive material is: modified mineral matter oil 40-45, sodium laurate 25-30, triglycerin fatty acid ester 0.4-0.5, trolamine 2-4, polyvinylpyrrolidone 0.6-0.8, magnesium sulfate 2-4, sodium hexametaphosphate 1.5-2.0, cyclodextrin 3-5, dextran 0.4-0.5, silane resin acceptor kh-550 5-10 and deionized water 250-280.
With the concrete parting agent that mineral oil is made, the weight part of its constitutive material is: modified mineral matter oil 42, sodium laurate 28, triglycerin fatty acid ester 0.5, trolamine 3, polyvinylpyrrolidone 0.7, magnesium sulfate 3, sodium hexametaphosphate 1.8, cyclodextrin 4, dextran 0.5, silane resin acceptor kh-550 8 and deionized water 250.
The preparation method of the concrete parting agent made with mineral oil, comprises following content:
(1) preparation of modified mineral oil: first mineral oil is heated to 50-60 DEG C; Then the 3.5-4.0% ferrous sulfate of mineral oil quality, 8-10% carbon fiber, 10-15% bamboo fibers is added wherein; Be uniformly mixed and place 2-3 hour, and then add the potassium humate powder of mineral oil 4-5%, be warming up to uniform stirring 1-2 hour under the condition of 80-90 DEG C, naturally cool to room temperature, regulator solution pH value is to 2-3; Again with deionized water in mass ratio 1:5 mix, stir 30-40 minute, centrifugation obtains filtrate;
(2) take by weight modified mineral oil and deionized water pour in reactor stand-by; Cyclodextrin, dextran is added after being heated to 85-100 DEG C; Stir and be incubated 20-30min; And then pour other residue constitutive material into, be warming up to 150-180 DEG C, continue to stir 3-5 minute; Finally cooling leaves standstill homogenizing.
Beneficial effect of the present invention:
The present invention is oily for major ingredient with modified mineral, learn stable in properties in neutral, free from extraneous odour, the releasing agent stripping result made is good, not Erodent Algorithm, nontoxic odorless, the sticky amount of mould concrete is few, in addition, the present invention adds the auxiliary agents such as coupling agent, emulsifying agent, stablizer, and the releasing agent of preparation has the compatible feature of profit, the demoulding of concrete article can be widely used in, also be applicable to various template.
Embodiment
Embodiment 1: the concrete parting agent made with mineral oil, the weight part (kg) of its constitutive material is: modified mineral matter oil 42, sodium laurate 28, triglycerin fatty acid ester 0.5, trolamine 3, polyvinylpyrrolidone 0.7, magnesium sulfate 3, sodium hexametaphosphate 1.8, cyclodextrin 4, dextran 0.5, silane resin acceptor kh-550 8 and deionized water 250.
The preparation method of the concrete parting agent made with mineral oil, comprises following content:
(1) preparation of modified mineral oil: first mineral oil is heated to 55 DEG C; Then 3.8% ferrous sulfate of mineral oil quality, 8% carbon fiber, 12% bamboo fibers is added wherein; Be uniformly mixed and place 2-3 hour, and then add the potassium humate powder of mineral oil 4.5%, be warming up to uniform stirring 1-2 hour under the condition of 85 DEG C, naturally cool to room temperature, regulator solution pH value is to 2-3; Again with deionized water in mass ratio 1:5 mix, stir 35 minutes, centrifugation obtains filtrate;
(2) take by weight modified mineral oil and deionized water pour in reactor stand-by; Cyclodextrin, dextran is added after being heated to 90 DEG C; Stir and be incubated 25min; And then pour other residue constitutive material into, be warming up to 160 DEG C, continue to stir 3-5 minute; Finally cooling leaves standstill homogenizing.
Above-mentioned obtained concrete parting agent solid content≤4.8%; To steel plate without any corrosion harmfulness, dry film time 30-33min; Concrete surface is smooth, and adhesive capacity is 4.6g/m 2, meet the service requirements of concrete parting agent.

Claims (3)

1. with the concrete parting agent that mineral oil is made, it is characterized in that the weight part of its constitutive material is: modified mineral matter oil 40-45, sodium laurate 25-30, triglycerin fatty acid ester 0.4-0.5, trolamine 2-4, polyvinylpyrrolidone 0.6-0.8, magnesium sulfate 2-4, sodium hexametaphosphate 1.5-2.0, cyclodextrin 3-5, dextran 0.4-0.5, silane resin acceptor kh-550 5-10 and deionized water 250-280.
2. the concrete parting agent made with mineral oil according to claim 1, is characterized in that the weight part of its constitutive material is: modified mineral matter oil 42, sodium laurate 28, triglycerin fatty acid ester 0.5, trolamine 3, polyvinylpyrrolidone 0.7, magnesium sulfate 3, sodium hexametaphosphate 1.8, cyclodextrin 4, dextran 0.5, silane resin acceptor kh-550 8 and deionized water 250.
3. a preparation method for the concrete parting agent made with mineral oil as claimed in claim 1, is characterized in that comprising following content:
(1) preparation of modified mineral oil: first mineral oil is heated to 50-60 DEG C; Then the 3.5-4.0% ferrous sulfate of mineral oil quality, 8-10% carbon fiber, 10-15% bamboo fibers is added wherein; Be uniformly mixed and place 2-3 hour, and then add the potassium humate powder of mineral oil 4-5%, be warming up to uniform stirring 1-2 hour under the condition of 80-90 DEG C, naturally cool to room temperature, regulator solution pH value is to 2-3; Again with deionized water in mass ratio 1:5 mix, stir 30-40 minute, centrifugation obtains filtrate;
(2) take by weight modified mineral oil and deionized water pour in reactor stand-by; Cyclodextrin, dextran is added after being heated to 85-100 DEG C; Stir and be incubated 20-30min; And then pour other residue constitutive material into, be warming up to 150-180 DEG C, continue to stir 3-5 minute; Finally cooling leaves standstill homogenizing.
CN201410786398.6A 2014-12-18 2014-12-18 Concrete release agent prepared from mineral oil and preparation method of concrete release agent Pending CN104479836A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410786398.6A CN104479836A (en) 2014-12-18 2014-12-18 Concrete release agent prepared from mineral oil and preparation method of concrete release agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410786398.6A CN104479836A (en) 2014-12-18 2014-12-18 Concrete release agent prepared from mineral oil and preparation method of concrete release agent

Publications (1)

Publication Number Publication Date
CN104479836A true CN104479836A (en) 2015-04-01

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017167649A1 (en) 2016-03-29 2017-10-05 Wacker Chemie Ag A release agent composition for inorganic construction materials and applications thereof
CN108102768A (en) * 2017-12-27 2018-06-01 江苏百瑞吉新材料有限公司 A kind of concrete parting agent and preparation method thereof
CN114181763A (en) * 2021-12-16 2022-03-15 武汉金安顺科技有限公司 High-adhesion prefabricated part release agent and preparation method thereof

Citations (10)

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CN1075330A (en) * 1992-02-06 1993-08-18 瑞士隆萨股份有限公司 Produce the lubricant for mandrel of seamless tube
CN1554524A (en) * 2003-12-26 2004-12-15 四川东方绝缘材料股份有限公司 Method for preparing demolding agent for roducing epoxy glass fibre reinforced plastic composite material
CN1596178A (en) * 2001-11-28 2005-03-16 拜尔材料科学股份公司 Mold release agent and method for producing plastic molded parts
CN101812362A (en) * 2009-12-18 2010-08-25 河南省绿韵建材有限公司 Emulsified paraffin release agent and manufacturing method thereof
CN103103011A (en) * 2013-01-24 2013-05-15 江苏博特新材料有限公司 Special release agent for concrete and preparation method thereof
CN103756774A (en) * 2014-01-28 2014-04-30 中国水利水电第三工程局有限公司 Environment-friendly oily emulsion release agent and preparation method thereof
CN103789074A (en) * 2014-01-21 2014-05-14 江苏龙蟠科技股份有限公司 Environment-friendly concrete member release agent and preparation method thereof
CN104031719A (en) * 2014-06-27 2014-09-10 无锡市崇安区科技创业服务中心 Anti-rust and wear-resistant lubricant and preparation method thereof
CN104059729A (en) * 2014-06-26 2014-09-24 青岛宝泰新能源科技有限公司 Lubricating oil for precision machines
CN104194903A (en) * 2014-07-31 2014-12-10 寿县维东建材商贸有限公司 Anticorrosive concrete release agent and preparation method thereof

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1075330A (en) * 1992-02-06 1993-08-18 瑞士隆萨股份有限公司 Produce the lubricant for mandrel of seamless tube
CN1596178A (en) * 2001-11-28 2005-03-16 拜尔材料科学股份公司 Mold release agent and method for producing plastic molded parts
CN1554524A (en) * 2003-12-26 2004-12-15 四川东方绝缘材料股份有限公司 Method for preparing demolding agent for roducing epoxy glass fibre reinforced plastic composite material
CN101812362A (en) * 2009-12-18 2010-08-25 河南省绿韵建材有限公司 Emulsified paraffin release agent and manufacturing method thereof
CN103103011A (en) * 2013-01-24 2013-05-15 江苏博特新材料有限公司 Special release agent for concrete and preparation method thereof
CN103789074A (en) * 2014-01-21 2014-05-14 江苏龙蟠科技股份有限公司 Environment-friendly concrete member release agent and preparation method thereof
CN103756774A (en) * 2014-01-28 2014-04-30 中国水利水电第三工程局有限公司 Environment-friendly oily emulsion release agent and preparation method thereof
CN104059729A (en) * 2014-06-26 2014-09-24 青岛宝泰新能源科技有限公司 Lubricating oil for precision machines
CN104031719A (en) * 2014-06-27 2014-09-10 无锡市崇安区科技创业服务中心 Anti-rust and wear-resistant lubricant and preparation method thereof
CN104194903A (en) * 2014-07-31 2014-12-10 寿县维东建材商贸有限公司 Anticorrosive concrete release agent and preparation method thereof

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2017167649A1 (en) 2016-03-29 2017-10-05 Wacker Chemie Ag A release agent composition for inorganic construction materials and applications thereof
CN108102768A (en) * 2017-12-27 2018-06-01 江苏百瑞吉新材料有限公司 A kind of concrete parting agent and preparation method thereof
CN114181763A (en) * 2021-12-16 2022-03-15 武汉金安顺科技有限公司 High-adhesion prefabricated part release agent and preparation method thereof

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Application publication date: 20150401