CN104465315B - The chip separation method of 3D Stacked Die Packaging devices - Google Patents

The chip separation method of 3D Stacked Die Packaging devices Download PDF

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Publication number
CN104465315B
CN104465315B CN201310439837.1A CN201310439837A CN104465315B CN 104465315 B CN104465315 B CN 104465315B CN 201310439837 A CN201310439837 A CN 201310439837A CN 104465315 B CN104465315 B CN 104465315B
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chip
grinding
stacked die
separation method
abrasive
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CN104465315A (en
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林晓玲
章晓文
陆裕东
苏菊花
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Fifth Electronics Research Institute of Ministry of Industry and Information Technology
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    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/04Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
    • H01L21/18Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
    • H01L21/30Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26
    • H01L21/302Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26 to change their surface-physical characteristics or shape, e.g. etching, polishing, cutting
    • H01L21/304Mechanical treatment, e.g. grinding, polishing, cutting
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/04Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
    • H01L21/18Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
    • H01L21/30Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26
    • H01L21/302Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26 to change their surface-physical characteristics or shape, e.g. etching, polishing, cutting
    • H01L21/306Chemical or electrical treatment, e.g. electrolytic etching
    • H01L21/30604Chemical etching
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L22/00Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
    • H01L22/20Sequence of activities consisting of a plurality of measurements, corrections, marking or sorting steps
    • H01L22/26Acting in response to an ongoing measurement without interruption of processing, e.g. endpoint detection, in-situ thickness measurement

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  • Engineering & Computer Science (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Physics & Mathematics (AREA)
  • Power Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Encapsulation Of And Coatings For Semiconductor Or Solid State Devices (AREA)

Abstract

The invention discloses a kind of chip separation method of 3D Stacked Die Packagings device, comprises the steps:The internal structure of the micro- detection 3D Stacked Die Packaging ULSI samples of acoustic scan, it is determined that required abrasive areas and its area;3D Stacked Die Packaging ULSI samples are fixed on grinding table with hot melt wax;Grinding:According to the area of above-mentioned abrasive areas, abrasive drill, grinding dynamics and grinding direction are selected, encapsulating material and chip is removed, is ground to the protective layer of objective chip surface covering;Using chemical corrosion method, above-mentioned protective layer is removed.The present invention is based on grinding, supplemented by chemical attack;Grinding needle is removed to specific localized areas, does not damage lower layer chip internal structure and its bonding wire;The protective layer covered on objective chip surface or chip binding agent are removed by chemical corrosion method, objective chip exposure;Bonding wire in the objective chip internal structure and chip of gained is not completely damaged, and facilitates follow-up electrical measurement to analyze.

Description

The chip separation method of 3D Stacked Die Packaging devices
Technical field
The present invention relates to chip separation method, more particularly to a kind of chip separation side of 3D Stacked Die Packagings device Method.
Background technology
3D Stacked Die Packaging technologies realize multichip interconnection using solid space, in the premise for not changing package body sizes Under, two are stacked using the mode such as wire bonding or through-silicon-via TSV interconnection in vertical direction in vivo in same encapsulation Or more chip.3D Stacked Die Packaging super large-scale integration(ULSI)While circuit performance is improved, greatly drop The low power consumption of circuit, becomes the new lover of high performance device.
At present, for brand-new 3D ULSI products, sometimes by destructive physical analysis, its internal structure is checked, This needs successively to expose the multilayer chiop inside 3D ULSI, and the internal structure to each layer carries out interior visual inspection, to verify which Whether internal material, design and structure meet applicable design document requirement or other regulations are required.
And the 3D ULSI to using and occurring to fail, need first with defect location technological orientation to defect concrete Which layer chip, then this layer of chip is come out carry out physical analysis, morphology observation analysis and failure machine are carried out to rejected region Reason confirms.When defect is on top layer chip, the separation method of ULSI is encapsulated using one chip, i.e., by traditional chemistry The corrosive liquids such as etch nitric acid are realized removing to the corrosiveness of plastic encapsulant, or by mechanical Kaifeng method file Or ceramics or Metal Packaging cover plate are levered up and are removed by small milling machine.Both sample treatments can realize plastic seal The removal of various encapsulating materials such as dress, ceramic package, packed by metal casing;But 3D Stacked Die Packaging ULSI contain two or with Upper chip, when defect is on non-top layer chip, in addition to the encapsulating material for getting rid of ULSI, also needs on objective chip Other chips are gone divided by exposing objective chip and be analyzed;In addition, 3D Stacked Die Packaging ULSI are in addition to encapsulating material, There are other chips and chip chamber binding agent.And, after the non-top layer chip of 3D ULSI comes out, it may be necessary to carry out Defect location again.The existing Detection Techniques for chip-scale defect, such as mechanical probes, light transmitting microtechnic, red Outer thermal imagery method, liquid crystal Method, electron beam tester etc., are required to device plus certain voltage bias to reappear failure phenomenon, this Require that the electrical property of device is good.Therefore, when the 3D Stacked Die Packagings ULSI to failing carries out non-top layer chip exposure, must Must ensure while encapsulating material, upper strata chip etc. is removed, it is ensured that the electrical property of objective chip layer is good, i.e. objective chip layer Internal structure, the bonding welding pad on chip, bonding wire etc. all intact must not be damaged.
As chip material is silicon(Si), it is impossible to removed with chemical corrosion method, even using hydrofluoric acid(HF)Immersion, also not Can be by its erosion removal.And mechanical Kaifeng method is mainly used for the Kaifeng of ceramic cover plate encapsulation or metal-back packaging, lead to Package casing material is removed by the method that overground or sled combines, and exposes encapsulation inner chamber, but the method cannot be in package cavity body Chip carry out Local treatment and reserved lead it is lossless.
Therefore, traditional chemical attack or mechanical Kaifeng method cannot meet the non-top layer chip things of 3D Stacked Die Packaging ULSI The demand of reason analysis.How the chip on objective chip to be removed, be 3D Stacked Die Packagings ULSI failure analyses/physics point The thorny problem run into during analysis.
The content of the invention
Based on this, it is an object of the invention to provide a kind of chip separation method of 3D Stacked Die Packagings device.
The concrete technical scheme for solving above-mentioned technical problem is as follows:
A kind of chip separation method of 3D Stacked Die Packagings device, comprises the steps:
(1)Determine abrasive areas and its area
The internal structure of the micro- detection 3D Stacked Die Packaging ULSI samples of acoustic scan, the such as chip layer of device inside Number, chip area size, and determine abrasive areas and its area;
(2)It is fixed
3D Stacked Die Packaging ULSI samples are fixed on grinding table with hot melt wax;
(3)Grinding
According to step(1)Determined by abrasive areas and its area, select abrasive drill, grinding dynamics, depth and speed, The encapsulating material and chip of abrasive areas are removed, the protective layer of objective chip surface covering is ground to;In the grinding:If grinding Area is 3-6mm, and abrasive drill is 1mm, if milling area be 7-15mm, abrasive drill is 3mm, if milling area be more than 15mm, abrasive drill are 5mm;
(4)Chemical attack
Using chemical corrosion method, removal step(3)Described protective layer.
Wherein in some embodiments, step(3)
It is wherein in some embodiments, described to be ground to step-by-step movement grinding, i.e. stepping applying grinding dynamics, for same Material, when initial, dynamics is larger, example:The 1/4-1/2 of total grinding thickness is ground once, with the carrying out of grinding, dynamics gradually subtracts It is few.Grinding dynamics refers to and arrange the thickness of grinding downwards and apply corresponding power by dialing knob;Grinding dynamics is determined often The thickness that secondary grinding is removed.
Wherein in some embodiments, step(3)Described grinding dynamics is step(3)The grinding direction is:XY side To or X-direction or Y-direction.
Wherein in some embodiments, step(2)Described fixation and step(3)Also include calibration in described grinding: The calibration is the thickness by measuring difference on abrasive areas surface, while the height of grinding table is adjusted, to adjust grinding The flatness in face.
Wherein in some embodiments, the chemical corrosion method is:Corroded using the concentrated sulfuric acid.
Wherein in some embodiments, also including monitoring:Using metallographic microscope monitoring step(3)The grinding and step (4)The progress of the chemical attack.
A kind of chip separation method of 3D Stacked Die Packagings device of the present invention has the advantage that and beneficial effect Really:
(1)In chip separation method of the present invention, based on grinding technique, supplemented by chemical corrosion method;It is main to utilize Region sample preparation grinding technique realizes micron-sized region grinding, can be deep into encapsulation inside cavity, for specific localized areas (Such as the upper area only to chip area size)De-layer is ground, certain layer of chip and encapsulating material is being removed, while not damaging Hinder lower layer chip internal structure and its bonding wire;Wherein, in the grinding:If milling area is 3-6mm, abrasive drill is 1mm, if milling area is 7-15mm, abrasive drill is 3mm, if milling area is more than 15mm, abrasive drill is 5mm;It is auxiliary again The protective layer covered on objective chip surface or chip binding agent are removed with chemical corrosion method, make objective chip surface clearly sudden and violent Expose;The objective chip for being come out, the bonding wire in internal structure and chip etc. are not completely damaged, i.e., electrical property is good Good, the convenient electrical measurement subsequently to this layer of chip is analyzed;
(2)In chip separation method of the present invention, the method for fixing sample using hot melt wax is avoided and adopts fixture When being fixedly clamped to encapsulate that inside chip causes be forced to rupture or warpage is damaged, when making grinding, the thickness of sample, size be not It is constrained;
(3)In chip separation method of the present invention, using multiple spot thickness measure, coordinate the calibration side of adjustment grinding table Method makes lapped face smooth, it is to avoid unnecessary inclination grinding damage.
(4)In chip separation method of the present invention, also using metallography microscope sem observation each material in process of lapping In color change with realize real-time monitoring grinding progress, accordingly adjust grinding dynamics, not only broken away to sample size according to Rely, also further ensure that the size of abrasive areas, depth are controllable, it is to avoid overmastication or grinding are not enough;
(5)Chip separation method of the present invention realizes 3D Stacked Die Packaging device insides multilayer chiop successively Exposure, solves the problems, such as that the non-top layer chip makes physical analysis of 3D Stacked Die Packaging devices is difficult, can also make some 3D laminated chips The failure analysis of the ineffective part of encapsulation is smoothly completed, and determines its final failure cause and mechanism, prevents the weight for failing Appear again existing, the reliability to improving device is significant.
Description of the drawings
Fig. 1 is the techniqueflow chart of the memory chips separation method described in embodiment 1;
Fig. 2 is the internal structure schematic diagram of the memory described in embodiment 1;Wherein, 1 is ground floor chip, and 2 is the second layer Chip;
Local pattern metallographic microscope figures of the Fig. 3 for second layer chip in the memory described in embodiment 1;
Fig. 4 is second layer chip local pattern and lead pattern metallographic microscope figure in the memory described in embodiment 1.
Specific embodiment
Below with reference to specific embodiment, the present invention will be further described.
Wherein, the micro- detection of acoustic scan described in following embodiments refers to ultrasonic scanning microscope, abbreviation C-SAM;
ALLIED companies of the U.S. of the hot melt wax manufacturer.
Embodiment 1
The present embodiment is including two chips of NAND Flash+Mobile SDRAM(Layers of chips adopts cross type Refracting films)Memory as a example by, obtain second layer chip by separating, its separation method comprises the steps(Techniqueflow Figure is referring to Fig. 1):
(1)Determine abrasive areas and its area
The micro- detection of acoustic scan(C-SAM)The internal structure of memory, as shown in Fig. 2 memory is cross type Bilateral lead packages, wherein, 1 is ground floor chip, and 2 is second layer chip;Determine abrasive areas for encapsulating material and 1 first Layer chip, area is 8mm;Memory original depth is measured simultaneously is about 1mm, rule of thumb, the encapsulating material of the usual the superiors The 1/3 of memory gross thickness is accounted for, this provides reference for grinding dynamics when encapsulating material is ground in follow-up grinding steps;
(2)It is fixed
Memory sample is fixed on grinding table with hot wax melting;Can flow as hot melt wax is heated, may make during cooling Into the out-of-flatness of device surface, by the thickness for measuring difference chip on abrasive areas surface, while coordinate adjusting grinding table Height, to adjust the flatness of abradant surface.
(3)Grinding
According to step(1)The abrasive areas and its area, select abrasive drill 3mm, metallographic microscope monitoring grind into Degree, while being ground using step-by-step movement, initial grinding dynamics is set to 100 μm of grinding downwards, carries out from two directions of grinding direction X, Y Grinding, removes the upper strata chip of encapsulating material and second layer chip, is ground to the protective layer of second layer chip surface covering, i.e., thoroughly Cross the protective layer transparent material to can be observed to stop grinding during this layer of chip internal structure;In process of lapping, according to metallography microscope The memory inside material color of mirror monitoring, pattern change, observe the process of grinding, and adjust grinding dynamics, for same Material, grinding dynamics are gradually decreased.The plastic packaging material not being ground is in black, and the plastic packaging material color being ground is in light gray, and Pattern is careful.Silicon chip before not being ground, in light mirror-like.After being ground, color is formed after grinding in light gray Pattern can be significantly coarse.When upper strata silicon chip is ground to very thin one layer, the interior of lower layer chip can be seen through the thin layer Portion's structure.Continue grinding, it can be seen that the protective layer on second layer chip(Usually polyimides), in orange-yellow transparence, thoroughly The protective layer is crossed, the internal structure of lower layer chip can be more clearly seen.
(4)Chemical attack
Using concentrated sulfuric acid removal step(3)The protective layer that described second layer chip surface is covered(Usually polyamides is sub- Amine), you can expose the second layer chip surface of complete display.Device is carefully detected by metallographic microscope, second layer core is observed Bonding wire on the internal structure of piece, chip, as a result referring to Fig. 3 and Fig. 4, wherein, local patterns of the Fig. 3 for second layer chip Figure, Fig. 4 are second layer chip local pattern and lead shape appearance figure.
Knowable to Fig. 3 and Fig. 4:Using separation method of the present invention, the bonding of the separated objective chip for obtaining draws Line is completely intact, and the internal structure and its bonding wire of lower layer chip are completely intact.
If objective chip is the third layer of other 3D Stacked Die Packaging devices, the chip such as the 4th layer, repeat above-mentioned Grind and steps of chemical attack is to remove the chip of more lower.
Embodiment described above only expresses the several embodiments of the present invention, and its description is more concrete and detailed, but and Therefore the restriction to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art For, without departing from the inventive concept of the premise, some deformations and improvement can also be made, these belong to the guarantor of the present invention Shield scope.Therefore, the protection domain of patent of the present invention should be defined by claims.

Claims (6)

1. a kind of chip separation method of 3D Stacked Die Packagings device, it is characterised in that comprise the steps:
(1) abrasive areas and its area are determined:
The internal structure of the micro- detection 3D Stacked Die Packaging ULSI samples of acoustic scan, determines abrasive areas and its area;
(2) it is fixed:
3D Stacked Die Packaging ULSI samples are fixed on grinding table with hot melt wax;
(3) grind:
Abrasive areas and its area according to determined by step (1), select abrasive drill, grinding dynamics and grinding direction, remove The encapsulating material and chip of abrasive areas, is ground to the protective layer of objective chip surface covering;In the grinding:If milling area For 3-6mm2, abrasive drill is 1mm, if milling area is 7-15mm2, abrasive drill is 3mm, if milling area be more than 15mm2, abrasive drill is 5mm;
(4) chemical attack:
Using chemical corrosion method, the protective layer described in removal step (3).
2. the chip separation method of 3D Stacked Die Packagings device according to claim 1, it is characterised in that step (3) It is described to be ground to step-by-step movement grinding.
3. the chip separation method of 3D Stacked Die Packagings device according to claim 1, it is characterised in that step (3) The grinding direction is:XY directions or X-direction or Y-direction.
4. the chip separation method of 3D Stacked Die Packagings device according to claim 1, it is characterised in that step (4) The chemical corrosion method is:The concentrated sulfuric acid corrodes.
5. the chip separation method of 3D Stacked Die Packagings device according to claim 1, it is characterised in that step (2) Also include calibration in grinding described in described fixation and step (3):The calibration is by measuring on abrasive areas surface not With the thickness of point, while the height of grinding table is adjusted, to adjust the flatness of abradant surface.
6. the chip separation method of the 3D Stacked Die Packaging devices according to any one of claim 1-5, it is characterised in that Also include monitoring:Using metallographic microscope monitoring step (3) grinding and the progress of step (4) chemical attack.
CN201310439837.1A 2013-09-24 2013-09-24 The chip separation method of 3D Stacked Die Packaging devices Active CN104465315B (en)

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CN114496824A (en) * 2020-10-23 2022-05-13 长鑫存储技术有限公司 Bare chip taking-out method
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