CN104450231A - Electronic part washing agent and preparation method thereof - Google Patents
Electronic part washing agent and preparation method thereof Download PDFInfo
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- CN104450231A CN104450231A CN201410641170.8A CN201410641170A CN104450231A CN 104450231 A CN104450231 A CN 104450231A CN 201410641170 A CN201410641170 A CN 201410641170A CN 104450231 A CN104450231 A CN 104450231A
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Abstract
The invention relates to an electronic part washing agent and a preparation method thereof. The electronic part washing agent comprises the following components in percentage by weight: 25%-35% of coconut oil glycol amide, 5%-10% of diethanol amine, 3%-6% of sodium silicate, 1%-5% of citric acid, 3%-8% of tripropylene glycol monomethyl ether, 3%-5% of an antirust agent, 1%-35 of a penetrating agent, 0.3%-1% of a stabilizer and the balance of deionized water. The preparation method of the electronic part washing agent comprises the following steps: preparing all the components according to the weight ratio, mixing coconut oil glycol amide, diethanol amine, sodium silicate, citric acid and tripropylene glycol monomethyl ether with the deionized water, heating to 40-50 DEG C by stirring at a rotation rate of 800-1000 rotations per minute, adding the antirust agent, the penetrating agent and the stabilizer, and continuing to stir for 10-15 minutes. The electronic part washing agent is high in washing efficiency, strong in decontamination capability, high in safety performance, free of the environment pollution and low in washing cost; the energy is saved; the damage to electronic parts in the washing process can be avoided.
Description
Technical field
The present invention relates to a kind of electronic component clean-out system and preparation method, belong to sanitising agent technical field.
Background technology
Along with the fast development of world's electronics and information industry, the electronic component industry development as electronics and information industry basis is also rapidly abnormal.Electronic component is just entering the components and parts epoch of new generation based on new electronic component, it will replace traditional components and parts substantially, electronic devices and components require to be main improvement by original the miniaturization for adaptation complete machine and novel process thereof, become to meet digital technique, to develop the characteristic requirements proposed be master to microelectronics, and be the complete satisfied industrialized development stage.Electronic component is the basis of composition electronic product, and it is study that the kind of the electronic component that understanding is conventional, properity also can correctly be selected, grasp the basic of electronic technology.Conventional electronic component has: resistance, electric capacity, inductance, potentiometer, transformer, triode, diode, IC etc., with regard to mounting means, can be divided into conventional mounting (also known as through hole dress and DIP) and the large class of surface mounting two at present.
Clean-out system solvent is a very large category, of a great variety, comprises inorganic cleaning and the large class of organic washing two.Briefly, organic clear numerous agent is exactly the clean-out system made containing carbon compound, and inorganic clear numerous agent is exactly the clean-out system that carbon-free compound is made, and therefore they belong to inorganics in the difference of organic washing agent and inorganic clean-out system.
Water is most important clean-out system, has the irreplaceable function and position of other any clean-out system.Common water is easy to obtain from occurring in nature, and water has very strong solvency power and dispersion force.But the surface tension of water is large, in use need to add tensio-active agent, to reduce surface tension, increase surface moist.In general industry cleaning, acid, the proportioning of alkali and water is more common, and some metal washes with water and will add rust-preventive agent.Aq. type clean-out system is mixed with by tensio-active agent (as sodium alkyl benzene sulfonate, sodium alkyl sulfate) and various auxiliary agent (as tripoly phosphate sodium STPP), auxiliary, during dirt on washes surface, the surface tension of the aqueous solution can be reduced, improve the material of clean effect.Solid detergent, liquid washing agent is divided into by product appearance form.Solid detergent output is maximum, claims washing powder traditionally, comprises finely powdered, particulate state and hollow bead shape etc.Also have between detergent paste therebetween, also claim washing cream.All kinds of synthetic detergent has different production technique, wherein complicated with solid detergent.Countries in the world generally produce hollow bead shape solid detergent, adopt high tower spray drying method, and its master operation has Pulp preparation, spraying dry, wind to send aging and packaging.Liquid washing agent manufactures easy, only need by tensio-active agent, auxiliary agent and other additives, and treated water, sends into mixing machine and carries out mixing.
Half aq. type clean-out system is also accurate aq. type clean-out system, forms as alcohols, organic hydrocarbon etc. by high boiling solvent and promoting agent etc.Usually containing 5% one 20% moisture, generally nonflammable, but heat cleaning time water-content control improper, may combustion phenomena be produced.Half aq. type cleaning has washed with solvent that some are different, and its Cleaning principle peels off to remove, instead of dissolving.In order to prevent the greasy dirt peeled off to be attached in cleaned material, scavenging solution will circulate continuously, and increases water-and-oil separator again.Partly wash usual cleaning performance fine, but running cost is higher, waste liquid can not regenerate recovery, reuses, containing COD(chemical oxygen demand) higher, need to carry out wastewater treatment.Half aq. type clean-out system adsorbs the novel detergent product of the medicament that various auxiliary agent synthesizes by fine particulate weakly alkaline, the active abrasive particle of natural interface is adopted to be raw material, coordinating multiple actives and sterilant, rumbling compound, that the green technology such as agent and unique bright factor high-tech is seen through in import is formulated, is a kind of multi-functional, efficient comprehensive Environment protection cleaning care products.Be the decontamination product of Modern New, clean effect is unique, and purposes is wide, is free from side effects to human body skin.By active abrasive particle be help with abrasive particle in pollute containing all kinds of serious tough stains more thoroughly can be removed fast with slight soft friction during unique cleaning agent matching purge.The dirt such as black dirt, heavy oil dirt, cement scale, spackling dirt, coin marking, rust deposite, gluing matter, tea stain, drink stain, glue hammering, leather shoes scratch, obstinate wax stain, aluminium trace, wooden trace, grid trace, watermark, footwear print, ink print, environmental protection, do not damage brick face, do not hinder hand.
Leaning solvent refers to water-fast organic solvent.Leaning solvent is made up of varsol, halogenated hydrocarbon solvent, alcoholic solvent, ether solvent, ketones solvent, esters solvent, phenol solvent, mixed solvent.
The clean-out system of electronic component in the market, mostly cleaning performance is bad, and some clean-out systems also have nitrites objectionable impurities, harm environment and people healthy; Because it is higher to the requirement of scavenging solution, there is higher requirement to its corrodibility and cleaning speed, can not should cause damage to electronics again to electronic component Rapid Cleaning.Therefore, develop and a kind ofly novel have environmental hazard low, cleaning performance is excellent, and the clean-out system less to electronic component infringement, has become the problem of those skilled in the art's solution too impatient to wait.
Chinese invention patent specification sheets CN 103571640 A is so a kind of water base LED chip clean-out system and preparation method thereof openly.This water base LED chip clean-out system, be made up of the raw material of following weight part: isomery fatty alcohol-polyoxyethylene ether 3-4, single stearic acid glycerine lipoprotein 1-2, sodium salicylate 2-3, propylene glycol 20-25,1,3-dioxolane 10-12, rosin 3-4, ethanol 30-35, the tertiary butyl-4-hydroxyanisol 6-8, tripropylene glycol methyl ether 4-5, auxiliary agent 4-5, deionized water 100-120.This invention can form protective membrane at chip surface, isolated air, prevents water and other molecules corrosion chip in air, anti-oxidant, facilitates next step manufacture craft to carry out.But this clean-out system for chip cleaning performance be not fine.
Chinese invention patent specification sheets CN 101368132 A openly so a kind of low-surface tensity circuit chip detergent.This low-surface tensity circuit chip detergent, comprise permeate agent, PH conditioning agent, tensio-active agent, solubilizing agent and pure water, wherein the weight percent of oxygenant is 1% to 5%, the weight percent of PH conditioning agent is 2% to 10%, the weight percent of solubilizing agent is 5% to 10%, the weight percent of tensio-active agent is 1% to 10%, and all the other are pure water; It is alkaline aqueous solution clean-out system, and good to the inhibition of circuit chip surface cleaning tension force, corrodibility is little, not etching apparatus, and not fragile circuit chip is surperficial, is convenient to the treatment and discharge of discarded scavenging solution, meets the requirement of environment protection.But this flocculation agent is not fine for the treatment effect of sewage.But this clean-out system for chip cleaning performance be not fine.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of electronic component clean-out system and preparation method's skill, and this electronic component clean-out system cleaning efficiency is high, and soil removability is strong; Safety performance is good, free from environmental pollution; Save energy, washing cost is low; Washing process is to electronic component not damaged.
In order to solve the problems of the technologies described above, a kind of electronic component clean-out system of the present invention, by weight percentage, comprises following component: Oleum Cocois ethylene glycol acid amides 25%-35%, diethanolamine 5%-10%, water glass 3%-6%, citric acid 1%-5%, tripropylene glycol methyl ether 3%-8%, rust-preventive agent 3%-5%, permeate agent 1%-3%, stablizer 0.3%-1%, all the other compositions are deionized water.
Described rust-preventive agent is organic carboxylate.
Described permeate agent is selected from the one in lauryl alcohol, oleic acid, mentha camphor.
Described stablizer is sodium oxalate.
The preparation method of described electronic component clean-out system, according to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
This electronic component clean-out system is adopted to have the following advantages: this clean-out system cleaning efficiency is high, and soil removability is strong; Safety performance is good, free from environmental pollution; Save energy, washing cost is low; Washing process is to electronic component not damaged.Add rust-preventive agent can permeate rust cleaning, loosen lubrication, prevent electronical elements surface by corrosion; Add the osmotic efficiency that permeate agent can strengthen Oleum Cocois ethylene glycol acid amides, the two synergy; Add stablizer and can keep chemical equilibrium, reduce surface tension, prevent light, thermolysis or oxygenolysis.
Embodiment
Electronic component clean-out system, by weight percentage, comprise following component: Oleum Cocois ethylene glycol acid amides 25%-35%, diethanolamine 5%-10%, water glass 3%-6%, citric acid 1%-5%, tripropylene glycol methyl ether 3%-8%, rust-preventive agent 3%-5%, permeate agent 1%-3%, stablizer 0.3%-1%, all the other compositions are deionized water.
Described rust-preventive agent is organic carboxylate.
Described permeate agent is selected from the one in lauryl alcohol, oleic acid, mentha camphor.
Described stablizer is sodium oxalate.
The preparation method of described electronic component clean-out system, according to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
Embodiment 1:
According to weight percent, take 25% Oleum Cocois ethylene glycol acid amides respectively, 5% diethanolamine, 3% water glass, 1% citric acid, 3% tripropylene glycol methyl ether, 3% rust-preventive agent, 1% permeate agent, 0.3% stablizer, all the other compositions are deionized water.
According to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
Embodiment 2:
According to weight percent, take 28% Oleum Cocois ethylene glycol acid amides respectively, 7% diethanolamine, 4% water glass, 2% citric acid, 4% tripropylene glycol methyl ether, 4% rust-preventive agent, 2% permeate agent, 0.5% stablizer, all the other compositions are deionized water.
According to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
Embodiment 3:
According to weight percent, take 30% Oleum Cocois ethylene glycol acid amides respectively, 8% diethanolamine, 4% water glass, 3% citric acid, 5% tripropylene glycol methyl ether, 4% rust-preventive agent, 2% permeate agent, 0.6% stablizer, all the other compositions are deionized water.
According to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
Embodiment 4:
According to weight percent, take 32% Oleum Cocois ethylene glycol acid amides respectively, 9% diethanolamine, 5% water glass, 4% citric acid, 6% tripropylene glycol methyl ether, 4% rust-preventive agent, 2% permeate agent, 0.8% stablizer, all the other compositions are deionized water.
According to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
Embodiment 5:
According to weight percent, take 35% Oleum Cocois ethylene glycol acid amides respectively, 10% diethanolamine, 6% water glass, 5% citric acid, 8% tripropylene glycol methyl ether, 5% rust-preventive agent, 3% permeate agent, 1% stablizer, all the other compositions are deionized water.
According to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
Cleaning performance test is carried out to embodiment 1-5 and comparative example 1-2 gained electronic component clean-out system, the results are shown in Table 1:
Table 1
Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Example 1 relatively | Example 2 relatively | |
Cleaning rate | 88.1% | 91.2% | 93.5% | 94.7% | 96.1% | 85.1% | 82.5% |
As seen from the above table, cleaning efficiency of the present invention is high, and soil removability is strong; Safety performance is good, free from environmental pollution; Save energy, washing cost is low; Washing process is to electronic component not damaged.
The technical characteristic described in detail is not had to be prior art in the application.Above-described embodiment is the principle of illustrative the application and effect thereof only, but not for limiting the application.Any person skilled in the art scholar all under the spirit and category of the application, can modify above-described embodiment or changes.Therefore, have in art and usually know that the knowledgeable modifies or changes not departing from all equivalences completed under the spirit and technological thought that the application discloses, must be contained by the claim of the application.
Claims (5)
1. an electronic component clean-out system, it is characterized in that: by weight percentage, comprise following component: Oleum Cocois ethylene glycol acid amides 25%-35%, diethanolamine 5%-10%, water glass 3%-6%, citric acid 1%-5%, tripropylene glycol methyl ether 3%-8%, rust-preventive agent 3%-5%, permeate agent 1%-3%, stablizer 0.3%-1%, all the other compositions are deionized water.
2. according to electronic component clean-out system according to claim 1, it is characterized in that: described rust-preventive agent is organic carboxylate.
3. according to electronic component clean-out system according to claim 1, it is characterized in that: described permeate agent is selected from the one in lauryl alcohol, oleic acid, mentha camphor.
4. according to electronic component clean-out system according to claim 1, it is characterized in that: described stablizer is sodium oxalate.
5. the preparation method of an electronic component clean-out system as claimed in claim 1, it is characterized in that: according to weight proportion, each composition is configured, by Oleum Cocois ethylene glycol acid amides, diethanolamine, water glass, citric acid, tripropylene glycol methyl ether, deionized water mixing, under stirring at 800-1000 rev/min, be heated to 40-50 DEG C, add rust-preventive agent, permeate agent, stablizer, continue to stir 10-15 minute.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105018252A (en) * | 2015-07-02 | 2015-11-04 | 苏州永创达电子有限公司 | Electronic product cleaning compound |
CN111363632A (en) * | 2018-12-25 | 2020-07-03 | 山东浪潮华光光电子股份有限公司 | Normal-temperature dewaxing cleaning agent and use method thereof |
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CN102660752A (en) * | 2012-05-09 | 2012-09-12 | 上海福岛化工科技发展有限公司 | Environment-friendly efficient bubble-free cleaning agent |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105018252A (en) * | 2015-07-02 | 2015-11-04 | 苏州永创达电子有限公司 | Electronic product cleaning compound |
CN111363632A (en) * | 2018-12-25 | 2020-07-03 | 山东浪潮华光光电子股份有限公司 | Normal-temperature dewaxing cleaning agent and use method thereof |
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Application publication date: 20150325 |