CN104449997A - Dilutable easy-to-clean antirust grease and preparation method thereof - Google Patents
Dilutable easy-to-clean antirust grease and preparation method thereof Download PDFInfo
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- CN104449997A CN104449997A CN201410626858.9A CN201410626858A CN104449997A CN 104449997 A CN104449997 A CN 104449997A CN 201410626858 A CN201410626858 A CN 201410626858A CN 104449997 A CN104449997 A CN 104449997A
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Abstract
The invention discloses dilutable easy-to-clean antirust grease. The dilutable easy-to-clean antirust grease is characterized by being prepared from the following raw materials in parts by weight: 12-16 parts of lanonol, 35-40 parts of vaseline, 2-4 parts of carnauba wax, 6-8 parts of petroleum sodium sulfonate, 9-11 parts of 0# light diesel oil, 13-15 parts of spindle oil, 1-2 parts of sorbitol monoleate, 1.5-2 parts of cocoanut fatty acid diethanolamide, 2.5-3 parts of zinc naphthenate, 0.6-1 part of benzotriazole and 2.5-4 parts of a protective agent. By adopting a dilutable formula, the dilutable easy-to-clean antirust grease can be used after being diluted with 10-fold kerosene, and can be applied to rust protection during metal processing; through addition of the protective agent, the antirust grease can be resistant to ultraviolet radiation, can be antibacterial and antiseptic, and can form a firm protective film on a metal surface so as to prevent rusting caused by corrosion of water and oxygen; an oil film of the dilutable easy-to-clean antirust grease is high in strength, easy to clean and long in antirust cycle; the oil change period is prolonged; and the production cost is effectively lowered.
Description
Technical field
The present invention relates to rust protection liquid field, particularly a kind of rust preventing grease diluting easy cleaning and preparation method thereof.
Background technology
Slushing oil and rust preventing grease have different uses to divide the work respectively in intermetallic composite coating.When applying preventive by dipping oil, still there is large gauging namely to pack because oil does not drain, make the place that oil is many produce corrosion; Also the uneven or drain spray of oil film can be caused when spraying.So easy to operate, the rust preventing grease that cost is low is a kind of desirable antirust product.But most rust preventing grease is thick and heavy paste substance, and use range has certain restriction.
The present invention is directed to the characteristic of rust preventing grease, according to demand, make a kind of dilutable rust preventing grease, serve many purposes.In use, can dilute with coal Water Oil Or Gas, can be used in when not diluting and outdoor etc. antirustly require high environment, may be used for intermetallic composite coating or metallic weapon etc. after after diluting 10 times and seal up for safekeeping for a long time.May be used for intermetallic composite coating etc., and rust preventing grease rust-preventing characteristic after dilution, oilness are excellent, and easily clean, be especially suitable for use as the antirust of cutting fluid or polishing fluid; Add protective material, uvioresistant is irradiated, Antimicrobial preservative, and can form firmly protective membrane in metallic surface, and the erosion of anti-sealing and oxygen causes getting rusty.
Summary of the invention
The object of this invention is to provide a kind of rust preventing grease diluting easy cleaning and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
Dilute a rust preventing grease for easy cleaning, be made up of the raw material of following weight part: lanosterol 12-16, Vaseline 35-40, carnauba wax 2-4, petroleum sodium sulfonate 6-8,0# solar oil 9-11, spindle oil 13-15, sorbitol monooleate 1-2, cocoanut fatty acid diethanolamide 1.5-2, zinc naphthenate 2.5-3, benzotriazole 0.6-1, protective material 2.5-4;
Described protective material is prepared from by the raw material of following weight part: bakelite 10-12, urethane 13-15, ethylene glycol diglycidylether 2-3, butyleneglycol 4.5-6, tween 80 1-2, myristyl benzyl dimethyl ammonium chloride 0.1-0.2, red iron oxide 3-4, nano titanium oxide 2-4, Viscotrol C 5-7, Zinic stearas 2-3, silicon dioxide gel 3-5, sec.-propyl three isophthaloyl titanic acid ester 0.3-0.5; First preparation method adds Viscotrol C, silicon dioxide gel, agitation grinding 50-60 minute by after red iron oxide, nano titanium oxide mixing, forms dispersion; Then by bakelite, urethane, the mixing of sec.-propyl three isophthaloyl titanic acid ester, be heated to 90 DEG C-115 DEG C stirring reaction 2-3 hour, be cooled to 45 DEG C-60 DEG C again, add all the other remaining components except tween 80, myristyl benzyl dimethyl ammonium chloride, stir 30-40 minute with the speed of 400-500 rev/min; Finally be cooled to room temperature, add dispersion and tween 80, myristyl benzyl dimethyl ammonium chloride, stir and obtain protective material.
A kind of rust preventing grease diluting easy cleaning of the present invention, be made up of following concrete steps:
(1) add lanosterol by spindle oil, stir, gradation adds Vaseline, fully grinding 1-2 hour;
(2) by carnauba wax, petroleum sodium sulfonate, zinc naphthenate mixing, be heated to 80 DEG C-100 DEG C while stirring, insulation 60-90 minute, is then cooled to 45 DEG C-55 DEG C, adds sorbitol monooleate, insulation reaction 30-40 minute;
(3) step (1) is mixed with step (2), add protective material, stir 20-30 minute with the speed of 300-350 rev/min; then all the other remaining components are added; be heated to 60 DEG C-65 DEG C, continue to stir 1.5-2 hour, then namely cold going obtain rust preventing grease of the present invention to room temperature.
Excellent effect of the present invention is: the present invention adopts can diluted formulations, can use with after the kerosene cutback of 10 times, antirust for during intermetallic composite coating, add protective material, can not only uvioresistant irradiate, Antimicrobial preservative, and firmly protective membrane can be formed in metallic surface, the erosion of anti-sealing and oxygen causes getting rusty; Oil film strength of the present invention is large, but is easy to cleaning, and the antirust cycle is long, and the drain period extends, and effectively reduces production cost.
Embodiment
Below by specific examples, the present invention is described in detail.
Dilute a rust preventing grease for easy cleaning, be made up of the raw material of following weight part (kilogram): lanosterol 12, Vaseline 35, carnauba wax 2, petroleum sodium sulfonate 6,0# solar oil 9, spindle oil 13, sorbitol monooleate 1, cocoanut fatty acid diethanolamide 1.5, zinc naphthenate 2.5, benzotriazole 0.6, protective material 2.5;
Described protective material is prepared from by the raw material of following weight part (kilogram): bakelite 10, urethane 13, ethylene glycol diglycidylether 2, butyleneglycol 4.5, tween 80 1, myristyl benzyl dimethyl ammonium chloride 0.1, red iron oxide 3, nano titanium oxide 2, Viscotrol C 5, Zinic stearas 2, silicon dioxide gel 3, sec.-propyl three isophthaloyl titanic acid ester 0.3; First preparation method adds Viscotrol C, silicon dioxide gel, agitation grinding 50-60 minute by after red iron oxide, nano titanium oxide mixing, forms dispersion; Then by bakelite, urethane, the mixing of sec.-propyl three isophthaloyl titanic acid ester, be heated to 90 DEG C-115 DEG C stirring reaction 2-3 hour, be cooled to 45 DEG C-60 DEG C again, add all the other remaining components except tween 80, myristyl benzyl dimethyl ammonium chloride, stir 30-40 minute with the speed of 400-500 rev/min; Finally be cooled to room temperature, add dispersion and tween 80, myristyl benzyl dimethyl ammonium chloride, stir and obtain protective material.
A kind of rust preventing grease diluting easy cleaning of the present invention, be made up of following concrete steps:
(1) add lanosterol by spindle oil, stir, gradation adds Vaseline, fully grinding 1-2 hour;
(2) by carnauba wax, petroleum sodium sulfonate, zinc naphthenate mixing, be heated to 80 DEG C-100 DEG C while stirring, insulation 60-90 minute, is then cooled to 45 DEG C-55 DEG C, adds sorbitol monooleate, insulation reaction 30-40 minute;
(3) step (1) is mixed with step (2), add protective material, stir 20-30 minute with the speed of 300-350 rev/min; then all the other remaining components are added; be heated to 60 DEG C-65 DEG C, continue to stir 1.5-2 hour, then namely cold going obtain rust preventing grease of the present invention to room temperature.
The rust preventing grease outward appearance that the present invention makes is the ointment of smooth even, room temperature directly can use or spray with after kerosene cutback 10 times, and salt spray resistance is tested: be 35 DEG C in temperature, and through 150 hours, 45# steel was corrosion-free; Wet-heat resisting is tested: be 50 DEG C in temperature, and through 700 hours, 45# steel was corrosion-free.
Claims (2)
1. one kind can be diluted the rust preventing grease of easy cleaning, it is characterized in that, be made up of the raw material of following weight part: lanosterol 12-16, Vaseline 35-40, carnauba wax 2-4, petroleum sodium sulfonate 6-8,0# solar oil 9-11, spindle oil 13-15, sorbitol monooleate 1-2, cocoanut fatty acid diethanolamide 1.5-2, zinc naphthenate 2.5-3, benzotriazole 0.6-1, protective material 2.5-4;
Described protective material is prepared from by the raw material of following weight part: bakelite 10-12, urethane 13-15, ethylene glycol diglycidylether 2-3, butyleneglycol 4.5-6, tween 80 1-2, myristyl benzyl dimethyl ammonium chloride 0.1-0.2, red iron oxide 3-4, nano titanium oxide 2-4, Viscotrol C 5-7, Zinic stearas 2-3, silicon dioxide gel 3-5, sec.-propyl three isophthaloyl titanic acid ester 0.3-0.5; First preparation method adds Viscotrol C, silicon dioxide gel, agitation grinding 50-60 minute by after red iron oxide, nano titanium oxide mixing, forms dispersion; Then by bakelite, urethane, the mixing of sec.-propyl three isophthaloyl titanic acid ester, be heated to 90 DEG C-115 DEG C stirring reaction 2-3 hour, be cooled to 45 DEG C-60 DEG C again, add all the other remaining components except tween 80, myristyl benzyl dimethyl ammonium chloride, stir 30-40 minute with the speed of 400-500 rev/min; Finally be cooled to room temperature, add dispersion and tween 80, myristyl benzyl dimethyl ammonium chloride, stir and obtain protective material.
2. a kind of rust preventing grease diluting easy cleaning according to claim 1, is characterized in that, be made up of following concrete steps:
(1) add lanosterol by spindle oil, stir, gradation adds Vaseline, fully grinding 1-2 hour;
(2) by carnauba wax, petroleum sodium sulfonate, zinc naphthenate mixing, be heated to 80 DEG C-100 DEG C while stirring, insulation 60-90 minute, is then cooled to 45 DEG C-55 DEG C, adds sorbitol monooleate, insulation reaction 30-40 minute;
(3) step (1) is mixed with step (2), add protective material, stir 20-30 minute with the speed of 300-350 rev/min; then all the other remaining components are added; be heated to 60 DEG C-65 DEG C, continue to stir 1.5-2 hour, then namely cold going obtain rust preventing grease of the present invention to room temperature.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105670756A (en) * | 2016-03-01 | 2016-06-15 | 安徽振海重工机械有限公司 | Valve lubricating grease and preparation method thereof |
CN108003789A (en) * | 2017-12-23 | 2018-05-08 | 海麟文博(厦门)文物预防性保护技术有限公司 | Historical relic's protection wax and preparation method thereof |
Citations (6)
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CN101139541A (en) * | 2006-09-08 | 2008-03-12 | 刘延鹏 | Tail sealing grease for shield tunneller |
CN101768499A (en) * | 2010-01-25 | 2010-07-07 | 蓝星环境工程有限公司 | Lipid type antirust oil with gaseous phase antirust function |
CN101921652A (en) * | 2010-08-18 | 2010-12-22 | 中国石油化工股份有限公司 | Oil-air lubricating grease and production method thereof |
CN102229845A (en) * | 2011-05-20 | 2011-11-02 | 麻城市天安纳米化工材料有限公司 | Long-acting antirust grease and preparation method thereof |
CN103013623A (en) * | 2011-09-27 | 2013-04-03 | 比亚迪股份有限公司 | Anti-rust oil and preparation method thereof |
CN103725386A (en) * | 2013-12-31 | 2014-04-16 | 刘守亮 | Main bearing sealing grease for heading equipment shield tunneling machine in tunnel engineering and preparation method of grease |
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2014
- 2014-11-10 CN CN201410626858.9A patent/CN104449997A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101139541A (en) * | 2006-09-08 | 2008-03-12 | 刘延鹏 | Tail sealing grease for shield tunneller |
CN101768499A (en) * | 2010-01-25 | 2010-07-07 | 蓝星环境工程有限公司 | Lipid type antirust oil with gaseous phase antirust function |
CN101921652A (en) * | 2010-08-18 | 2010-12-22 | 中国石油化工股份有限公司 | Oil-air lubricating grease and production method thereof |
CN102229845A (en) * | 2011-05-20 | 2011-11-02 | 麻城市天安纳米化工材料有限公司 | Long-acting antirust grease and preparation method thereof |
CN103013623A (en) * | 2011-09-27 | 2013-04-03 | 比亚迪股份有限公司 | Anti-rust oil and preparation method thereof |
CN103725386A (en) * | 2013-12-31 | 2014-04-16 | 刘守亮 | Main bearing sealing grease for heading equipment shield tunneling machine in tunnel engineering and preparation method of grease |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105670756A (en) * | 2016-03-01 | 2016-06-15 | 安徽振海重工机械有限公司 | Valve lubricating grease and preparation method thereof |
CN108003789A (en) * | 2017-12-23 | 2018-05-08 | 海麟文博(厦门)文物预防性保护技术有限公司 | Historical relic's protection wax and preparation method thereof |
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