CN104403451A - Environment-friendly fireproof floor paint and preparation method thereof - Google Patents
Environment-friendly fireproof floor paint and preparation method thereof Download PDFInfo
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- CN104403451A CN104403451A CN201410624453.1A CN201410624453A CN104403451A CN 104403451 A CN104403451 A CN 104403451A CN 201410624453 A CN201410624453 A CN 201410624453A CN 104403451 A CN104403451 A CN 104403451A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- Chemical & Material Sciences (AREA)
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
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Abstract
The invention discloses an environment-friendly fireproof floor paint, which comprises the following main components: acrylic acid emulsion, a wetting agent, a surfactant, a filling material, vermiculite powder, deionized water, nano-level silicon dioxide powder, superfine dolomite, alumina fine powder, and color paste. Through the components mentioned above and combination with a specific ratio, the floor paint has a better fireproof performance and is more environment-friendly, compared to the conventional floor paints in the market. At the same time, the preparation process is controlled so as to ensure the application performance of the paint.
Description
Technical field
The present invention relates to a kind of manufacture method of coating, belong to building material field, particularly relate to a kind of environment-friendly fireproof Floor paint and preparation method thereof.
Background technology
In repairs profession, the fire prevention of timber floor is the content that human consumer is concerned about always.Frie retardant coating in the market is generally divided into expanded polystyrene veneer and non-expansion type two class, Non-expansive fireproof paint is that the mode by adding fire retardant reaches fp effect, it is very thick that the flameproof effect wanting to have reached must be coated with, and add a large amount of containing fire retardants such as halogen, nitrogen, phosphorus, produce a large amount of toxic gases; Expanding fire-proof paint is exactly that film expanded by heating forms cellular carburization zone, flame heat regulating is isolated and reduces or slow down the transmission to ground, when high temperature, coating decomposites not so gas simultaneously, isolated also diluent air, the series of physical that occurs when preventing fires of coating and chemical reaction absorb a large amount of heats thus play fire-retardant and delay flame spread, spread in addition, for people provide the time of fire extinguishing, but expanding fire-proof paint, mainly based on the solvent based coating of high VOC, cannot meet the demand of the low VOC in market.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes a kind of environment-friendly fireproof Floor paint, additionally provide the preparation method of this coating simultaneously.
Technical scheme of the present invention is as follows:
A kind of environment-friendly fireproof Floor paint, comprises the component of following weight percent,
The ACRYLIC EMULSION of described ACRYLIC EMULSION to be solid content be 55-60%, the solid content as used is on the low side, suitably can regulate the content of deionized water.
Described wetting agent is the wetting agent A337 of Kening Co., Ltd, adds this wetting agent and effectively can strengthen fluency in coating use procedure.
Described tensio-active agent is Sodium dodecylbenzene sulfonate, and what add tensio-active agent act as the solubility property strengthening ACRYLIC EMULSION.
Described filler is one or more the mixing in titanium dioxide, light calcium carbonate, china clay, silica powder.
Vermiculite power is clay mineral like a kind of smectites, for the silicate of laminate structure, vermiculite through its volume of high-temperature roasting can undergoes rapid expansion 6-20 doubly, the effect adding vermiculite power is in order under the high temperature that is heated, vermiculite power expands, isolation heat slows down the transmission to ground, simultaneously for the reaction of super fine bitter spar and alumina powder provides room and time.
The effect adding nanometer grade silica powder body is when envrionment temperature raises rapidly, is attached on the vermiculite power of expansion, and of short duration auxiliary vermiculite power resists high temperature.
Super fine bitter spar and alumina powder can react very soon under high temperature action, can generate on high temperature resistant species distribution vermiculite upon inflation, can play good flameproof effect.
The fire prevention principle of environment-friendly fireproof Floor paint of the present invention is as follows: when being subject to the temperatures involved of flame on floor, vermiculite power meeting undergoes rapid expansion, form sealing coat, thus slow down the impact of flame heat regulating on floor, nanometer grade silica powder has good dispersity simultaneously, the advantage that resistance to elevated temperatures is good, high temperature attack can be resisted, but because nanometer grade silica powder price is higher, in order to reduce costs, the present invention only adds a small amount of nanometer grade silica powder, of short durationly resist high temperature, add super fine bitter spar and alumina powder simultaneously, under the high temperature conditions, super fine bitter spar and alumina powder can generate the high temperature resistant material based on magnesia-alumina spinel structure by fast response very much, thus reach long-time fp effect.
Following table lists the impact of the weight percent comparison coating flameproof effect added of nanometer grade silica powder, super fine bitter spar and alumina powder.
1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 | 12 | 13 | |
A | 5 | 3 | 3 | 3 | 1 | 1 | 1 | 0.5 | 0.5 | 0.5 | 0.1 | 0.1 | 0.1 |
B | 0 | 0 | 2 | 5 | 0 | 2 | 5 | 0 | 2 | 5 | 0 | 2 | 5 |
C | 0 | 0 | 5 | 8 | 0 | 5 | 8 | 0 | 5 | 8 | 0 | 5 | 8 |
Result | Nothing | Slightly | Nothing | Nothing | Seriously | Slightly | Nothing | Seriously | Slightly | Nothing | Seriously | Seriously | Slightly |
A: nanometer grade silica powder; B: super fine bitter spar (325 order) C: alumina powder (700 order), the unit of A, B, C is g.
Other materials in coating and content are respectively:
Described detection method is: by above-mentioned coating uniform application in timber floor, carries out fire resistance test, when build is 0.5mm, and alcohol baking 30min, the base material carbonization result (nothing: base material Non-carbonized of gained; Slight: the slight carbonization of base material; Serious: the serious carbonization of base material).
Obtained by above table, in the present invention, the add-on be applicable to of nanometer grade silica powder, super fine bitter spar and alumina powder is
Nanometer grade silica powder 0.5-1%
Super fine bitter spar (325 order) 2-5%
Alumina powder (700 order) 5-8%.
A preparation method for environment-friendly fireproof Floor paint, comprises the following steps:
Add deionized water, wetting agent, filler, nanometer grade silica powder, super fine bitter spar, alumina powder in a reservoir, high-speed stirring (1000-1500 rev/min) evenly after, enter sand mill and be ground to fineness and be less than 50 microns;
After adding tensio-active agent middling speed (600-800 rev/min) stirring 2-3min, then add ACRYLIC EMULSION, stir 4-6min.
Finally add vermiculite, stirring at low speed (100-300 rev/min) evenly rear filtration gets product.
Finished product the tap water of additional 10-20% can be diluted to suitable viscosity in use.
Preferably, if used under 0-10 DEG C of environment, glycerol can also be added in use.
Beneficial effect of the present invention is: by the combination of each component and the specific proportioning of each component, compare the existing product on market, have fire performance and environmental-protecting performance better, simultaneously by the control to dope preparing process, ensure that the use properties of coating.
Embodiment
Embodiment 1:
A kind of environment-friendly fireproof Floor paint, comprising: by weight percentage,
Described ACRYLIC EMULSION to be solid content be 55% ACRYLIC EMULSION.
Described wetting agent is the wetting agent A337 of Kening Co., Ltd.
Described tensio-active agent is Sodium dodecylbenzene sulfonate.
Described filler is titanium dioxide.
Painting color in this embodiment is white, and filler titanium dioxide has played the effect of mill base, therefore does not add other mill base.
A preparation method for environment-friendly fireproof Floor paint, comprises the following steps:
Add deionized water, wetting agent, titanium dioxide, nanometer grade silica powder, super fine bitter spar, alumina powder in a reservoir, high-speed stirring (1500 revs/min) evenly after, enter sand mill and be ground to fineness and be less than 50 microns;
After adding tensio-active agent middling speed (800 revs/min) stirring 3min, then add ACRYLIC EMULSION, stir 5min.
Finally add vermiculite, stirring at low speed (100 revs/min) evenly rear filtration gets product.
Finished product in use can additional 10% tap water be diluted to suitable viscosity.
Embodiment 2:
A kind of environment-friendly fireproof Floor paint, comprising: by weight percentage,
Described ACRYLIC EMULSION to be solid content be 60% ACRYLIC EMULSION.
Described wetting agent is the wetting agent A337 of Kening Co., Ltd.
Described tensio-active agent is Sodium dodecylbenzene sulfonate.
Described filler is the mixture of light calcium carbonate and silica powder, and its blending ratio is 1:1.
Described mill base is ultramarine.
A preparation method for environment-friendly fireproof Floor paint, comprises the following steps:
Add deionized water, wetting agent, filler, nanometer grade silica powder, super fine bitter spar, alumina powder in a reservoir, high-speed stirring (1000 revs/min) evenly after, enter sand mill and be ground to fineness and be less than 50 microns;
After adding tensio-active agent middling speed (600 revs/min) stirring 2min, then add ACRYLIC EMULSION, stir 6min.
Regulate PH to 8-9, add ultramarine, continue to stir 3min.
Finally add vermiculite, stirring at low speed (300 revs/min) evenly rear filtration gets product.
Finished product in use can additional 15% tap water be diluted to suitable viscosity.
Embodiment 3:
A kind of environment-friendly fireproof Floor paint, comprising: by weight percentage,
Described ACRYLIC EMULSION to be solid content be 56.5% ACRYLIC EMULSION.
Described wetting agent is the wetting agent A337 of Kening Co., Ltd.
Described tensio-active agent is Sodium dodecylbenzene sulfonate.
Described filler is the mixture of china clay, light calcium carbonate and silica powder, and its blending ratio is 1:3:3.
Described mill base is carbon black.
A preparation method for environment-friendly fireproof Floor paint, comprises the following steps:
Add deionized water, wetting agent, filler, nanometer grade silica powder, super fine bitter spar, alumina powder, carbon black in a reservoir, high-speed stirring (1200 revs/min) evenly after, enter sand mill and be ground to fineness and be less than 50 microns;
After adding tensio-active agent middling speed (650 revs/min) stirring 2.5min, then add ACRYLIC EMULSION, stir 4min.
Finally add vermiculite, stirring at low speed (200 revs/min) evenly rear filtration gets product.
Finished product is when using for 5 DEG C, and the tap water of additional 20% and the glycerol dilution of coating quality 5% are stirred to suitable viscosity.
The environment-friendly fireproof Floor paint prepared embodiment 1-3 below carries out every objectionable impurities test.
In addition the sample of embodiment 1-3 is through tuerculoderma, does not find anaphylaxis, through respiratory tract test for sample is to respiratory tract nonirritant.
By the coating uniform application of embodiment 1-3 in timber floor, carry out fire resistance test, when build is 0.5mm, detected result is as follows:
Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 |
Alcohol baking 30min | Base material Non-carbonized | Base material Non-carbonized | Base material Non-carbonized |
Alcohol baking 45min | Base material Non-carbonized | The slight carbonization of base material | Base material Non-carbonized |
Alcohol baking 60min | Base material Non-carbonized | The slight carbonization of base material | The slight carbonization of base material |
This detects data only for above-mentioned detection sample.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (9)
1. an environment-friendly fireproof Floor paint, is characterized in that, comprises the component of following weight percent:
ACRYLIC EMULSION 30-50%
Wetting agent 0.2-0.5%
Tensio-active agent 1.5-4%
Filler 15-25%
Vermiculite power (80-120 order) 0.5-2%
Deionized water 30-40%
Nanometer grade silica powder 0.5-1%
Super fine bitter spar (325 order) 0.2-0.5%
Alumina powder (700 order) 0.5-0.8%
Mill base 0-2%.
2. environment-friendly fireproof Floor paint as claimed in claim 1, is characterized in that, the ACRYLIC EMULSION of described ACRYLIC EMULSION to be solid content be 55-60%, the solid content as used is on the low side, suitably can regulate the content of deionized water in formula.
3. environment-friendly fireproof Floor paint as claimed in claim 1, it is characterized in that, described wetting agent is the wetting agent A337 of Kening Co., Ltd.
4. environment-friendly fireproof Floor paint as claimed in claim 1, it is characterized in that, described tensio-active agent is Sodium dodecylbenzene sulfonate.
5. environment-friendly fireproof Floor paint as claimed in claim 1, it is characterized in that, described filler is one or more the mixing in titanium dioxide, light calcium carbonate, china clay, silica powder.
6. a preparation method for environment-friendly fireproof Floor paint, is characterized in that, its preparation method comprises the following steps:
Add deionized water, wetting agent, filler, nanometer grade silica powder, super fine bitter spar, alumina powder in a reservoir, high-speed stirring (1000-1500 rev/min) evenly after, enter sand mill and be ground to fineness and be less than 50 microns;
After adding tensio-active agent middling speed (600-800 rev/min) stirring 2-3min, then add ACRYLIC EMULSION, stir 4-6min;
Finally add vermiculite power, stirring at low speed (100-300 rev/min) evenly rear filtration gets product.
7. the preparation method of environment-friendly fireproof Floor paint as claimed in claim 6, is characterized in that, the tap water of described coating additional 10-20% is in use diluted to suitable viscosity.
8. the preparation method of environment-friendly fireproof Floor paint as claimed in claims 6 or 7, is characterized in that, when described coating uses under 0-10 DEG C of environment, separately add appropriate glycerol.
9. the preparation method of environment-friendly fireproof Floor paint as claimed in claim 6, is characterized in that, its preparation method comprises the following steps:
Add deionized water, wetting agent, filler, nanometer grade silica powder, super fine bitter spar, alumina powder in a reservoir, high-speed stirring (1000 revs/min) evenly after, enter sand mill and be ground to fineness and be less than 50 microns;
After adding tensio-active agent middling speed (600 revs/min) stirring 2-3min, then add ACRYLIC EMULSION, stir 4-6min;
Finally add vermiculite power, stirring at low speed (300 revs/min) evenly rear filtration gets product;
Described environment-friendly fireproof Floor paint comprises the component of following weight percent:
ACRYLIC EMULSION (solid content 55%) 30%
Wetting agent 0.2%
Sodium dodecylbenzene sulfonate 2%
Titanium dioxide 25%
Vermiculite power (80-120 order) 2%
Deionized water 39%
Nanometer grade silica powder 0.5%
Super fine bitter spar (325 order) 0.5%
Alumina powder (700 order) 0.8%
Described wetting agent is the wetting agent A337 of Kening Co., Ltd.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106930505A (en) * | 2017-03-06 | 2017-07-07 | 张家港市星泰防火保温材料有限公司 | A kind of fireproof floorboard and its manufacture method |
CN108546473A (en) * | 2018-05-29 | 2018-09-18 | 芜湖市元奎新材料科技有限公司 | Floor fireproof coating |
CN108753081A (en) * | 2018-05-29 | 2018-11-06 | 芜湖市元奎新材料科技有限公司 | Floor anti-flaming dope |
CN112282261A (en) * | 2020-10-29 | 2021-01-29 | 安徽扬子地板股份有限公司 | Spliced fireproof wallboard and preparation method thereof |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106930505A (en) * | 2017-03-06 | 2017-07-07 | 张家港市星泰防火保温材料有限公司 | A kind of fireproof floorboard and its manufacture method |
CN108546473A (en) * | 2018-05-29 | 2018-09-18 | 芜湖市元奎新材料科技有限公司 | Floor fireproof coating |
CN108753081A (en) * | 2018-05-29 | 2018-11-06 | 芜湖市元奎新材料科技有限公司 | Floor anti-flaming dope |
CN112282261A (en) * | 2020-10-29 | 2021-01-29 | 安徽扬子地板股份有限公司 | Spliced fireproof wallboard and preparation method thereof |
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