CN104389201A - Silk dyeing auxiliary - Google Patents
Silk dyeing auxiliary Download PDFInfo
- Publication number
- CN104389201A CN104389201A CN201410647433.6A CN201410647433A CN104389201A CN 104389201 A CN104389201 A CN 104389201A CN 201410647433 A CN201410647433 A CN 201410647433A CN 104389201 A CN104389201 A CN 104389201A
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- China
- Prior art keywords
- silk
- dyeing
- agent
- color
- dye
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 55
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 29
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 27
- 239000002994 raw material Substances 0.000 claims abstract description 21
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims abstract description 14
- 239000006184 cosolvent Substances 0.000 claims abstract description 14
- 239000003431 cross linking reagent Substances 0.000 claims abstract description 14
- 239000008367 deionised water Substances 0.000 claims abstract description 14
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 14
- 239000002270 dispersing agent Substances 0.000 claims abstract description 14
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 14
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 14
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims abstract description 14
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims abstract description 14
- 150000008442 polyphenolic compounds Chemical class 0.000 claims abstract description 14
- 235000013824 polyphenols Nutrition 0.000 claims abstract description 14
- 229910052938 sodium sulfate Inorganic materials 0.000 claims abstract description 14
- 235000011152 sodium sulphate Nutrition 0.000 claims abstract description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000012752 auxiliary agent Substances 0.000 claims description 17
- PLDUPXSUYLZYBN-UHFFFAOYSA-N Fluphenazine Chemical compound C1CN(CCO)CCN1CCCN1C2=CC(C(F)(F)F)=CC=C2SC2=CC=CC=C21 PLDUPXSUYLZYBN-UHFFFAOYSA-N 0.000 claims description 13
- 230000000740 bleeding effect Effects 0.000 claims description 13
- 229960001374 fluphenazine decanoate Drugs 0.000 claims description 13
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 230000001965 increasing effect Effects 0.000 abstract 2
- 229920001661 Chitosan Polymers 0.000 abstract 1
- 241001122767 Theaceae Species 0.000 abstract 1
- 229910000365 copper sulfate Inorganic materials 0.000 abstract 1
- 230000002708 enhancing effect Effects 0.000 abstract 1
- 230000001737 promoting effect Effects 0.000 abstract 1
- 239000000975 dye Substances 0.000 description 31
- 238000005516 engineering process Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 3
- 239000005416 organic matter Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000009975 hank dyeing Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
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Abstract
The invention relates to the technical field of silk production and processing and discloses a silk dyeing auxiliary. The silk dyeing auxiliary is prepared from the following raw materials in percentage by weight: 5-10% of chitosan, 5-10% of tea polyphenol, 3-7% of ferrous sulfate, 3-7% of copper sulfate, 3-10% of sodium sulfate, 1-3% of a cross-linking agent DE, 1-3% of an accelerant, 1-3% of a levelling agent, 1-10% of a dispersant, 1-3% of a penetrant, 1-3% of a curing agent, 1-3% of a color fixing agent, 1-3% of a cosolvent and the balance being deionized water. The silk dyeing auxiliary is reasonable in formula, has the excellent promoting performance on silk dyeing and is capable of being used for increasing the dye-uptake and the color fastness, improving the dyeing quality and enhancing the dispersibility of a dye in a dye solution system; dyed silk has the tiny change in color before and after soaping, and the dyeing depth is increased by 15%; the silk dyeing auxiliary is wide in raw material source, and the pollution to the environment is reduced.
Description
Technical field
The present invention relates to silk production processing technique field, refer more particularly to a kind of dyeing silk auxiliary agent.
Background technology
China is silk ancient country, and after before 4,000 years, the imperial concubine Lei ancestral of Yellow Emperor, a legendary ruler has invented silk reeling technology, the silk goods of China just start well-known.Zhang Qian sends as an envoy to behind the Western Regions, and the trade of China's silk fabrics starts to be transmitted to Europe, they buying silk, wear silk and regards to be rich in and the symbol of identity as.Silk reeling equipment develops into automatic Silk Reeling from seat reel silk from cocoons, vertical reel silk from cocoons, but on silk reeling technology, remains and continue to use traditional production technology especially, and its technological process is substantially identical with the silk reeling technology that Lei ancestral invents.
The technological process control of current dyeing silk is still domestic textile enterprise particularly a kind of production method of adopting of silk weaving enterprise.In process of production, how controlling, reduce and overcome the uneven dyeing such as silk hank dyeing aberration, look flower, is urgent problem in production at present to obtain desirable Color.Existing dyeing silk auxiliary agent is generally organic matter, or rare earth element mixes with organic matter and forms, adopt existing dyeing assistant to print and dye, dyestuff dye-uptake and COLOR FASTNESS are all lower, and dyestuff is not strong in the dispersiveness of dye solution system, and dyestuff easily produces precipitation because of build-up of static charges, dye utilization rate is low, dyeing cost is high, and in dyeing and printing sewage, the content of organic dyestuff is high, large for environmental pollution.
Summary of the invention
The object of the present invention is to provide a kind of dyeing silk auxiliary agent, shorten dyeing time, reduce energy resource consumption, decreasing pollution.
For achieving the above object, the present invention is by the following technical solutions:
A kind of dyeing silk auxiliary agent, comprises the raw material of following percentage by weight: shitosan 5-10%, Tea Polyphenols 5-10%, ferrous sulfate 3-7%, copper sulphate 3-7%, sodium sulphate 3-10%, crosslinking agent DE 1-3%, accelerant 1-3%, Lyogen MF 1-3%, dispersant 1-10%, bleeding agent 1-3%, color-fixing agent 1-3%, cosolvent 1-3%, surplus is deionized water, and said components percentage composition summation is 100%.
Preferably, described dyeing silk auxiliary agent comprises the raw material of following percentage by weight: shitosan 8%, Tea Polyphenols 8%, ferrous sulfate 5%, copper sulphate 5%, sodium sulphate 7%, crosslinking agent DE 2%, accelerant 2%, Lyogen MF 2%, dispersant 5%, bleeding agent 2%, color-fixing agent 2%, cosolvent 2%, surplus is deionized water, and said components percentage composition summation is 100%.
Preferably, described dyeing silk auxiliary agent comprises the raw material of following percentage by weight: shitosan 9%, Tea Polyphenols 9%, ferrous sulfate 6%, copper sulphate 6%, sodium sulphate 8%, crosslinking agent DE 2.5%, accelerant 2.5%, Lyogen MF 2.5%, dispersant 8%, bleeding agent 2.5%, color-fixing agent 2.5%, cosolvent 2.5%, surplus is deionized water, and said components percentage composition summation is 100%.
Preferably, described dyeing silk auxiliary agent comprises the raw material of following percentage by weight: shitosan 6%, Tea Polyphenols 6%, ferrous sulfate 4%, copper sulphate 4%, sodium sulphate 9%, crosslinking agent DE 1.5%, accelerant 1.5%, Lyogen MF 1.5%, dispersant 9%, bleeding agent 1.5%, color-fixing agent 1.5%, cosolvent 1.5%, surplus is deionized water, and said components percentage composition summation is 100%.
Compared with prior art, the present invention has the following advantages:
Dyeing assistant formula of the present invention is reasonable, to dyeing silk, there is good improving performance, improve dyestuff dye-uptake and COLOR FASTNESS, improve dyeing quality, increase the dispersiveness of dyestuff in dye solution system, very little through front and back change color of soaping after dyeing silk, dye level improves 15%, raw material sources of the present invention are extensive, decrease the pollution to environment.
Detailed description of the invention
Below in conjunction with detailed description of the invention, technical scheme of the present invention is further described in detail.
Embodiment one:
A kind of dyeing silk auxiliary agent, comprises the raw material of following percentage by weight: shitosan 10%, Tea Polyphenols 10%, ferrous sulfate 7%, copper sulphate 7%, sodium sulphate 10%, crosslinking agent DE 3%, accelerant 3%, Lyogen MF 3%, dispersant 10%, bleeding agent 3%, color-fixing agent 3%, cosolvent 3%, surplus is deionized water, and said components percentage composition summation is 100%.The present embodiment dyeing assistant formula is reasonable, to dyeing silk, there is good improving performance, improve dyestuff dye-uptake and COLOR FASTNESS, improve dyeing quality, increase the dispersiveness of dyestuff in dye solution system, very little through front and back change color of soaping after dyeing silk, dye level improves 15%, the present embodiment raw material sources are extensive, decrease the pollution to environment.
Embodiment two:
A kind of dyeing silk auxiliary agent, comprises the raw material of following percentage by weight: shitosan 5%, Tea Polyphenols 5%, ferrous sulfate 3%, copper sulphate 3%, sodium sulphate 3%, crosslinking agent DE 1%, accelerant 1%, Lyogen MF 1%, dispersant 1%, bleeding agent 1%, color-fixing agent 1%, cosolvent 1%, surplus is deionized water, and said components percentage composition summation is 100%.The present embodiment dyeing assistant formula is reasonable, to dyeing silk, there is good improving performance, improve dyestuff dye-uptake and COLOR FASTNESS, improve dyeing quality, increase the dispersiveness of dyestuff in dye solution system, very little through front and back change color of soaping after dyeing silk, dye level improves 15%, the present embodiment raw material sources are extensive, decrease the pollution to environment.
Embodiment three:
A kind of dyeing silk auxiliary agent, comprises the raw material of following percentage by weight: shitosan 8%, Tea Polyphenols 8%, ferrous sulfate 5%, copper sulphate 5%, sodium sulphate 7%, crosslinking agent DE 2%, accelerant 2%, Lyogen MF 2%, dispersant 5%, bleeding agent 2%, color-fixing agent 2%, cosolvent 2%, surplus is deionized water, and said components percentage composition summation is 100%.The present embodiment dyeing assistant formula is reasonable, to dyeing silk, there is good improving performance, improve dyestuff dye-uptake and COLOR FASTNESS, improve dyeing quality, increase the dispersiveness of dyestuff in dye solution system, very little through front and back change color of soaping after dyeing silk, dye level improves 15%, the present embodiment raw material sources are extensive, decrease the pollution to environment.
Embodiment four:
A kind of dyeing silk auxiliary agent, comprises the raw material of following percentage by weight: shitosan 9%, Tea Polyphenols 9%, ferrous sulfate 6%, copper sulphate 6%, sodium sulphate 8%, crosslinking agent DE 2.5%, accelerant 2.5%, Lyogen MF 2.5%, dispersant 8%, bleeding agent 2.5%, color-fixing agent 2.5%, cosolvent 2.5%, surplus is deionized water, and said components percentage composition summation is 100%.The present embodiment dyeing assistant formula is reasonable, to dyeing silk, there is good improving performance, improve dyestuff dye-uptake and COLOR FASTNESS, improve dyeing quality, increase the dispersiveness of dyestuff in dye solution system, very little through front and back change color of soaping after dyeing silk, dye level improves 15%, the present embodiment raw material sources are extensive, decrease the pollution to environment.
Embodiment five:
A kind of dyeing silk auxiliary agent, comprises the raw material of following percentage by weight: shitosan 6%, Tea Polyphenols 6%, ferrous sulfate 4%, copper sulphate 4%, sodium sulphate 9%, crosslinking agent DE 1.5%, accelerant 1.5%, Lyogen MF 1.5%, dispersant 9%, bleeding agent 1.5%, color-fixing agent 1.5%, cosolvent 1.5%, surplus is deionized water, and said components percentage composition summation is 100%.The present embodiment dyeing assistant formula is reasonable, to dyeing silk, there is good improving performance, improve dyestuff dye-uptake and COLOR FASTNESS, improve dyeing quality, increase the dispersiveness of dyestuff in dye solution system, very little through front and back change color of soaping after dyeing silk, dye level improves 15%, the present embodiment raw material sources are extensive, decrease the pollution to environment.
It should be noted last that, above detailed description of the invention is only in order to illustrate technical scheme of the present invention and unrestricted, although with reference to preferred embodiment to invention has been detailed description, those of ordinary skill in the art is to be understood that, can modify to technical scheme of the present invention or equivalent replacement, and not departing from the spirit and scope of technical solution of the present invention, it all should be encompassed in the middle of right of the present invention.
Claims (4)
1. a dyeing silk auxiliary agent, is characterized in that, comprises the raw material of following percentage by weight: shitosan 5-10%, Tea Polyphenols 5-10%, ferrous sulfate 3-7%, copper sulphate 3-7%, sodium sulphate 3-10%, crosslinking agent DE 1-3%, accelerant 1-3%, Lyogen MF 1-3%, dispersant 1-10%, bleeding agent 1-3%, color-fixing agent 1-3%, cosolvent 1-3%, surplus is deionized water, and said components percentage composition summation is 100%.
2. dyeing silk auxiliary agent according to claim 1, is characterized in that, comprises the raw material of following percentage by weight: shitosan 8%, Tea Polyphenols 8%, ferrous sulfate 5%, copper sulphate 5%, sodium sulphate 7%, crosslinking agent DE 2%, accelerant 2%, Lyogen MF 2%, dispersant 5%, bleeding agent 2%, color-fixing agent 2%, cosolvent 2%, surplus is deionized water, and said components percentage composition summation is 100%.
3. dyeing silk auxiliary agent according to claim 1, is characterized in that, comprises the raw material of following percentage by weight: shitosan 9%, Tea Polyphenols 9%, ferrous sulfate 6%, copper sulphate 6%, sodium sulphate 8%, crosslinking agent DE 2.5%, accelerant 2.5%, Lyogen MF 2.5%, dispersant 8%, bleeding agent 2.5%, color-fixing agent 2.5%, cosolvent 2.5%, surplus is deionized water, and said components percentage composition summation is 100%.
4. dyeing silk auxiliary agent according to claim 1, is characterized in that, comprises the raw material of following percentage by weight: shitosan 6%, Tea Polyphenols 6%, ferrous sulfate 4%, copper sulphate 4%, sodium sulphate 9%, crosslinking agent DE 1.5%, accelerant 1.5%, Lyogen MF 1.5%, dispersant 9%, bleeding agent 1.5%, color-fixing agent 1.5%, cosolvent 1.5%, surplus is deionized water, and said components percentage composition summation is 100%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410647433.6A CN104389201B (en) | 2014-11-14 | 2014-11-14 | A kind of silk dyeing auxiliary |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410647433.6A CN104389201B (en) | 2014-11-14 | 2014-11-14 | A kind of silk dyeing auxiliary |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104389201A true CN104389201A (en) | 2015-03-04 |
| CN104389201B CN104389201B (en) | 2016-06-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410647433.6A Active CN104389201B (en) | 2014-11-14 | 2014-11-14 | A kind of silk dyeing auxiliary |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104389201B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106498774A (en) * | 2016-11-29 | 2017-03-15 | 潍坊百禾工艺品有限公司 | A kind of dyeing assistant and preparation method thereof |
| CN107034700A (en) * | 2016-11-03 | 2017-08-11 | 江苏海云花新材料有限公司 | A kind of dyeing nylon acid-releasing agent and preparation method thereof |
| CN109098018A (en) * | 2018-06-08 | 2018-12-28 | 姜永达 | A kind of dyeing used additives and preparation method thereof |
| CN109778565A (en) * | 2017-11-10 | 2019-05-21 | 丹阳市易通安全技术服务有限公司 | A kind of printing assistant |
| CN112301765A (en) * | 2020-11-03 | 2021-02-02 | 上海锐鲨高新材料有限公司 | Textile auxiliary for improving color fastness and preparation method thereof |
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| JP2002004182A (en) * | 2000-06-22 | 2002-01-09 | Ito En Ltd | Method for producing dyed fiber |
| CN101168928A (en) * | 2007-08-20 | 2008-04-30 | 罗海航 | Reactive dyestuff dyeing and fixing technique and printing and dyeing auxiliary agent used for the same |
| CN101280525A (en) * | 2008-06-05 | 2008-10-08 | 重庆市农业科学院 | Natural staining agent, preparation thereof and application thereof to silk dyeing |
| CN101956334A (en) * | 2010-09-10 | 2011-01-26 | 中国农业科学院茶叶研究所 | Method for dying cotton fiber by utilizing tea vegetable dye |
| CN102911517A (en) * | 2012-10-30 | 2013-02-06 | 中国农业科学院茶叶研究所 | Preparation method and usage of special tea dye for silk |
| CN103710999A (en) * | 2013-12-05 | 2014-04-09 | 安徽三喜针织有限公司 | Novel environmental protection composite dye and preparation method therefor |
| CN104099788A (en) * | 2014-07-04 | 2014-10-15 | 无锡市信达染整机械厂 | Environmental-friendly cotton fabric dyeing |
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2014
- 2014-11-14 CN CN201410647433.6A patent/CN104389201B/en active Active
Patent Citations (8)
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| JP2000355877A (en) * | 1999-06-11 | 2000-12-26 | Ito En Ltd | Antifungal use of tea saponin-fixed fiber |
| JP2002004182A (en) * | 2000-06-22 | 2002-01-09 | Ito En Ltd | Method for producing dyed fiber |
| CN101168928A (en) * | 2007-08-20 | 2008-04-30 | 罗海航 | Reactive dyestuff dyeing and fixing technique and printing and dyeing auxiliary agent used for the same |
| CN101280525A (en) * | 2008-06-05 | 2008-10-08 | 重庆市农业科学院 | Natural staining agent, preparation thereof and application thereof to silk dyeing |
| CN101956334A (en) * | 2010-09-10 | 2011-01-26 | 中国农业科学院茶叶研究所 | Method for dying cotton fiber by utilizing tea vegetable dye |
| CN102911517A (en) * | 2012-10-30 | 2013-02-06 | 中国农业科学院茶叶研究所 | Preparation method and usage of special tea dye for silk |
| CN103710999A (en) * | 2013-12-05 | 2014-04-09 | 安徽三喜针织有限公司 | Novel environmental protection composite dye and preparation method therefor |
| CN104099788A (en) * | 2014-07-04 | 2014-10-15 | 无锡市信达染整机械厂 | Environmental-friendly cotton fabric dyeing |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107034700A (en) * | 2016-11-03 | 2017-08-11 | 江苏海云花新材料有限公司 | A kind of dyeing nylon acid-releasing agent and preparation method thereof |
| CN106498774A (en) * | 2016-11-29 | 2017-03-15 | 潍坊百禾工艺品有限公司 | A kind of dyeing assistant and preparation method thereof |
| CN109778565A (en) * | 2017-11-10 | 2019-05-21 | 丹阳市易通安全技术服务有限公司 | A kind of printing assistant |
| CN109098018A (en) * | 2018-06-08 | 2018-12-28 | 姜永达 | A kind of dyeing used additives and preparation method thereof |
| CN112301765A (en) * | 2020-11-03 | 2021-02-02 | 上海锐鲨高新材料有限公司 | Textile auxiliary for improving color fastness and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104389201B (en) | 2016-06-08 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
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Denomination of invention: A silk dyeing auxiliary Effective date of registration: 20201230 Granted publication date: 20160608 Pledgee: Anhui Guangde Rural Commercial Bank Co.,Ltd. Pledgor: ANHUI HONGXIANG SILK WEAVING Co.,Ltd. Registration number: Y2020990001524 |
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Date of cancellation: 20220221 Granted publication date: 20160608 Pledgee: Anhui Guangde Rural Commercial Bank Co.,Ltd. Pledgor: ANHUI HONGXIANG SILK WEAVING Co.,Ltd. Registration number: Y2020990001524 |
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Denomination of invention: Silk dyeing assistant Effective date of registration: 20220221 Granted publication date: 20160608 Pledgee: Anhui Guangde Rural Commercial Bank Co.,Ltd. Pledgor: ANHUI HONGXIANG SILK WEAVING Co.,Ltd. Registration number: Y2022990000093 |
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| PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
| PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20230608 Granted publication date: 20160608 Pledgee: Anhui Guangde Rural Commercial Bank Co.,Ltd. Pledgor: ANHUI HONGXIANG SILK WEAVING Co.,Ltd. Registration number: Y2022990000093 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A Silk Dyeing Assistant Effective date of registration: 20230613 Granted publication date: 20160608 Pledgee: Anhui Guangde Rural Commercial Bank Co.,Ltd. Pledgor: ANHUI HONGXIANG SILK WEAVING Co.,Ltd. Registration number: Y2023980043707 |