CN104389044A - Preparation method of transparent anti-static high-performance enhanced polyamide yarns - Google Patents
Preparation method of transparent anti-static high-performance enhanced polyamide yarns Download PDFInfo
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Abstract
The invention provides a preparation method of transparent anti-static high-performance enhanced polyamide yarns. The preparation method comprises the following steps: (1) preparing the following raw materials in parts by weigh: 60-70 parts of PA6 slices, 15-25 parts of alkali-free glass fiber chopped strands, 3-5 parts of a nylon transparent reagent, 3-5 parts of an internal mixed antistatic agent and 1-3 parts of auxiliaries, adding the raw materials to a high-speed mixer and mixing evenly, wherein the auxiliaries include a coupling agent, an antioxidant and a lubricant in the weight ratio of 1 to 1 to 1; (2) drying the raw materials; (3) preparing a spinning fluid, namely accurately adding the various raw materials by use of a master batch injecting/releasing pump, mixing and melting; (4) spinning, namely pressing the spinning fluid into a spinning assembly quantitatively by use of a metering pump, jetting out the spinning fluid by a spinneret plate, and forming a tow in a spinning window; and (5) carrying out post-processing, namely orderly performing the steps of draw-twisting on prepared fibers, setting, balancing, dyeing-grading, checking and packaging. The transparent anti-static high-performance enhanced polyamide yarns prepared by use of the preparation method have the high strength, transparency and antistatic properties.
Description
Technical field
The high-performance that the present invention relates to a kind of transparent antistatic strengthens the preparation method of POLYAMIDE YARNS, belongs to chemical fiber field.
Background technology
Polyamide fibre is the trade name of polyamide fiber, polyamide fiber is commonly called as nylon (Nylon), English name Polyamide(is called for short PA), density 1.15g/cm3, be on molecular backbone containing recurring amide radical group-[NHCO]-thermoplastic resin general name, comprise aliphatic PA, fat-aromatic series PA and aromatic series PA.Wherein aliphatic PA is wide in variety, and output is large, and be widely used, its name is determined by the carbon number that synthon is concrete.
Polyamide is mainly used in synthetic fiber, its most outstanding advantage be ABRASION RESISTANCE higher than other all fibres, higher than cotton ABRASION RESISTANCE 10 times, higher than wool 20 times, in BLENDED FABRIC, enter some polyamide fibers a little, can greatly improve its ABRASION RESISTANCE; When being stretched to 3-6%, elastic recovery rate can reach 100%; Up to ten thousand foldings can be stood scratch and do not rupture.The strength ratio cotton height 1-2 of polyamide fiber doubly, than wool height 4-5 doubly, is 3 times of viscose.But the heat resistance of polyamide fiber and light resistance poor, retentivity is not good yet, the clothes made not as terylene well-pressed.In addition, the shortcoming of hygroscopicity and dyeability difference is all there is for the nylon-66 of wearing clothes and polyamide fibre-6, develop the new varieties of polyamide fiber for this reason---the novel polyamide fiber of poly-β-alanine and polyamide fibre-4, have that light weight, wrinkle resistance are excellent, the feature such as good permeability and good durability, dyeability and HEAT SETTING, be therefore considered to rising.
Because polyamide has nontoxic, light weight, excellent mechanical strength, ABRASION RESISTANCE and corrosion resistance preferably, therefore be widely used in replacing the metals such as copper to manufacture bearing, gear, pump leaf and other parts in the industry such as machinery, chemical industry, instrument, automobile, be applicable to make wear part, drive mechanism part, household appliance components, automobile making part, screw mandrel prevents machine components, chemical machinery part, chemical industry equipment.As turbine, gear, bearing, impeller, crank, instrument board, driving shaft, valve, blade, screw mandrel, high pressure packing ring, screw, nut, sealing ring, shuttle, cover letter, axle sleeve connector etc.Molten polyamide has very high intensity after being spun into silk, mainly makees synthetic fiber and can be used as medical suture.On civilian, can blending or be purely spun into various medical treatment and knitwear.Chinlon filament is used for knitting and silk textile industry, as knitted the polyamide fibre socks of the various wear-resisting explanation such as monofilament hose, elastic force silk stocking, polyamide fibre gauze kerchief, mosquito net, polyamide fibre lace, elastic force polyamide fibre coat, the silk product of various polyamide fibre silk fabric or intertexture.Polyamide staple fibre is mostly used for the wool type product blending with wool or other chemical fibre, makes the various wear-resisting dress material worn long.Industrially polyamide fibre is used for manufacturing cord fabric thread, industrial cloth, hawser, conveyer belt, tent, fishing net etc. in a large number.Main as parachute and other army fabrics in national defence.
Existing high-performance polyamide fibre, can only have in enhancing, the performance such as fire-retardant, weather-proof wherein one or both, lack the high-performance polyamide fibre simultaneously possessing multiple performance.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art part, provide a kind of high-performance of transparent antistatic to strengthen the preparation method of POLYAMIDE YARNS.
The high-performance of transparent antistatic of the present invention strengthens the preparation method of POLYAMIDE YARNS, comprises the following steps:
1) raw material: PA6 section 60-70 weight portion, alkali-free glass fibre short chopping 15-25 weight portion, nylon clarifier 3-5 weight portion, interior mixed type antistatic additive 3-5 weight portion and auxiliary agent 1-3 weight portion is prepared according to following proportioning, described auxiliary agent comprises coupling agent, anti-oxidant auxiliary agent and lubricant, the weight ratio of three is 1:1:1, adds in high-speed mixer and mixes;
2) drying process is carried out to raw material;
3) spin fluid is prepared: utilize master batch to annotate pump and accurately add each raw material, mixed melting;
4) spinning: above-mentioned spin fluid is quantitatively pressed into filament spinning component through measuring pump, is sprayed by spinnerets, forms tow in spinning window;
5) aft-loaded airfoil: the fiber made is carried out successively draw-teisting, sizing, balance, dyeing grades and test package operation.
Preferably,
Described raw material comprises following ingredients, and: PA6 cuts into slices 65 weight portions, alkali-free glass fibre short chopping 20 weight portion, nylon clarifier 4 weight portion, interior mixed type antistatic additive 4 weight portion, coupling agent 0.7 weight portion, anti-oxidant auxiliary agent 0.7 weight portion and lubricant 0.7 weight portion.
The high-performance of transparent antistatic of the present invention strengthens in the preparation method of POLYAMIDE YARNS, add the intensity of the short chopping of alkali-free glass fibre for increasing POLYAMIDE YARNS, add nylon clarifier for the formation of transparent POLYAMIDE YARNS, add the antistatic behaviour of interior mixed type antistatic additive for increasing POLYAMIDE YARNS, therefore obtained product possesses high strength, transparent and anlistatig performance simultaneously, can extensive use in automobile, electrical equipment, Machinery Ministry structure, transportation equipment, weaving, papermaking equipment etc.
Detailed description of the invention
embodiment 1
The high-performance of the transparent antistatic of the present embodiment strengthens the preparation method of POLYAMIDE YARNS, comprises the following steps:
1) prepare raw material: PA6 according to following proportioning to cut into slices 65 weight portions, alkali-free glass fibre short chopping 20 weight portion, nylon clarifier 4 weight portion, interior mixed type antistatic additive 4 weight portion, coupling agent 0.7 weight portion, anti-oxidant auxiliary agent 0.7 weight portion and lubricant 0.7 weight portion, add in high-speed mixer and mix;
2) drying process is carried out to raw material;
3) spin fluid is prepared: utilize master batch to annotate pump and accurately add each raw material, mixed melting;
4) spinning: above-mentioned spin fluid is quantitatively pressed into filament spinning component through measuring pump, is sprayed by spinnerets, forms tow in spinning window;
5) aft-loaded airfoil: the fiber made is carried out successively draw-teisting, sizing, balance, dyeing grades and test package operation.
embodiment 2
The high-performance of the transparent antistatic of the present embodiment strengthens the preparation method of POLYAMIDE YARNS, comprises the following steps:
1) prepare raw material: PA6 according to following proportioning to cut into slices 60 weight portions, alkali-free glass fibre short chopping 15 weight portion, nylon clarifier 3 weight portion, interior mixed type antistatic additive 3 weight portion, coupling agent 0.33 weight portion, anti-oxidant auxiliary agent 0.33 weight portion and lubricant 0.33 weight portion, add in high-speed mixer and mix;
2) drying process is carried out to raw material;
3) spin fluid is prepared: utilize master batch to annotate pump and accurately add each raw material, mixed melting;
4) spinning: above-mentioned spin fluid is quantitatively pressed into filament spinning component through measuring pump, is sprayed by spinnerets, forms tow in spinning window;
5) aft-loaded airfoil: the fiber made is carried out successively draw-teisting, sizing, balance, dyeing grades and test package operation.
embodiment 3
The high-performance of the transparent antistatic of the present embodiment strengthens the preparation method of POLYAMIDE YARNS, comprises the following steps:
1) prepare raw material: PA6 according to following proportioning to cut into slices 70 weight portions, alkali-free glass fibre short chopping 25 weight portion, nylon clarifier 5 weight portion, interior mixed type antistatic additive 5 weight portion, coupling agent 1 weight portion, anti-oxidant auxiliary agent 1 weight portion and lubricant 1 weight portion, add in high-speed mixer and mix;
2) drying process is carried out to raw material;
3) spin fluid is prepared: utilize master batch to annotate pump and accurately add each raw material, mixed melting;
4) spinning: above-mentioned spin fluid is quantitatively pressed into filament spinning component through measuring pump, is sprayed by spinnerets, forms tow in spinning window;
5) aft-loaded airfoil: the fiber made is carried out successively draw-teisting, sizing, balance, dyeing grades and test package operation.
Claims (2)
1. the high-performance of transparent antistatic strengthens a preparation method for POLYAMIDE YARNS, it is characterized in that, comprises the following steps:
1) raw material: PA6 section 60-70 weight portion, alkali-free glass fibre short chopping 15-25 weight portion, nylon clarifier 3-5 weight portion, interior mixed type antistatic additive 3-5 weight portion and auxiliary agent 1-3 weight portion is prepared according to following proportioning, described auxiliary agent comprises coupling agent, anti-oxidant auxiliary agent and lubricant, the weight ratio of three is 1:1:1, adds in high-speed mixer and mixes;
2) drying process is carried out to raw material;
3) spin fluid is prepared: utilize master batch to annotate pump and accurately add each raw material, mixed melting;
4) spinning: above-mentioned spin fluid is quantitatively pressed into filament spinning component through measuring pump, is sprayed by spinnerets, forms tow in spinning window;
5) aft-loaded airfoil: the fiber made is carried out successively draw-teisting, sizing, balance, dyeing grades and test package operation.
2. the high-performance of transparent antistatic according to claim 1 strengthens the preparation method of POLYAMIDE YARNS, it is characterized in that, described raw material comprises following ingredients, and: PA6 cuts into slices 65 weight portions, alkali-free glass fibre short chopping 20 weight portion, nylon clarifier 4 weight portion, interior mixed type antistatic additive 4 weight portion, coupling agent 0.7 weight portion, anti-oxidant auxiliary agent 0.7 weight portion and lubricant 0.7 weight portion.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108914243A (en) * | 2018-06-25 | 2018-11-30 | 南通美铭锦纶有限公司 | A kind of preparation method of enhanced chinlon 6 filament |
CN109770458A (en) * | 2018-12-28 | 2019-05-21 | 天长市东安防护用品有限公司 | Antistatic medical cleanness clothing of one kind and preparation method thereof |
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CN101469129A (en) * | 2007-12-24 | 2009-07-01 | 上海杰事杰新材料股份有限公司 | Flame-retardant antistatic reinforced nylon 6 composition and preparation |
CN101665986A (en) * | 2009-09-28 | 2010-03-10 | 海安县中山合成纤维有限公司 | Mica chinlon cool fiber filament and production method thereof |
CN101955656A (en) * | 2010-10-14 | 2011-01-26 | 苏州市科创聚合物有限公司 | Glass fiber enhanced nylon 6 material for improving transparency |
CN102108207A (en) * | 2009-12-28 | 2011-06-29 | 上海日之升新技术发展有限公司 | Compound filling material nylon 6 composition with high surface anti-static electricity and preparation method thereof |
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2014
- 2014-11-13 CN CN201410638049.XA patent/CN104389044A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN101469129A (en) * | 2007-12-24 | 2009-07-01 | 上海杰事杰新材料股份有限公司 | Flame-retardant antistatic reinforced nylon 6 composition and preparation |
CN101665986A (en) * | 2009-09-28 | 2010-03-10 | 海安县中山合成纤维有限公司 | Mica chinlon cool fiber filament and production method thereof |
CN102108207A (en) * | 2009-12-28 | 2011-06-29 | 上海日之升新技术发展有限公司 | Compound filling material nylon 6 composition with high surface anti-static electricity and preparation method thereof |
CN101955656A (en) * | 2010-10-14 | 2011-01-26 | 苏州市科创聚合物有限公司 | Glass fiber enhanced nylon 6 material for improving transparency |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108914243A (en) * | 2018-06-25 | 2018-11-30 | 南通美铭锦纶有限公司 | A kind of preparation method of enhanced chinlon 6 filament |
CN109770458A (en) * | 2018-12-28 | 2019-05-21 | 天长市东安防护用品有限公司 | Antistatic medical cleanness clothing of one kind and preparation method thereof |
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Application publication date: 20150304 |