CN104370542A - 一种氧化锆基陶瓷刀具材料及其制备方法 - Google Patents
一种氧化锆基陶瓷刀具材料及其制备方法 Download PDFInfo
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- CN104370542A CN104370542A CN201410580896.5A CN201410580896A CN104370542A CN 104370542 A CN104370542 A CN 104370542A CN 201410580896 A CN201410580896 A CN 201410580896A CN 104370542 A CN104370542 A CN 104370542A
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- 239000000463 material Substances 0.000 title claims abstract description 22
- 239000000919 ceramic Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims description 10
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 title abstract 3
- 229910001928 zirconium oxide Inorganic materials 0.000 title abstract 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 43
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 11
- 239000008367 deionised water Substances 0.000 claims abstract description 10
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 10
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims abstract description 7
- 229910012519 LiSbO3 Inorganic materials 0.000 claims abstract description 7
- 229920002125 Sokalan® Polymers 0.000 claims abstract description 7
- 229910021538 borax Inorganic materials 0.000 claims abstract description 7
- 239000001768 carboxy methyl cellulose Substances 0.000 claims abstract description 7
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims abstract description 7
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims abstract description 7
- 229910000420 cerium oxide Inorganic materials 0.000 claims abstract description 7
- FYDKNKUEBJQCCN-UHFFFAOYSA-N lanthanum(3+);trinitrate Chemical compound [La+3].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O FYDKNKUEBJQCCN-UHFFFAOYSA-N 0.000 claims abstract description 7
- BMMGVYCKOGBVEV-UHFFFAOYSA-N oxo(oxoceriooxy)cerium Chemical compound [Ce]=O.O=[Ce]=O BMMGVYCKOGBVEV-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004584 polyacrylic acid Substances 0.000 claims abstract description 7
- BITYAPCSNKJESK-UHFFFAOYSA-N potassiosodium Chemical compound [Na].[K] BITYAPCSNKJESK-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 7
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 7
- AYJRCSIUFZENHW-DEQYMQKBSA-L barium(2+);oxomethanediolate Chemical compound [Ba+2].[O-][14C]([O-])=O AYJRCSIUFZENHW-DEQYMQKBSA-L 0.000 claims abstract description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims description 24
- 239000002245 particle Substances 0.000 claims description 15
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 12
- 238000000498 ball milling Methods 0.000 claims description 12
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 claims description 12
- -1 polyoxyethylene Polymers 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 238000007731 hot pressing Methods 0.000 claims description 9
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 6
- 239000005995 Aluminium silicate Substances 0.000 claims description 6
- 239000004160 Ammonium persulphate Substances 0.000 claims description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
- 235000012211 aluminium silicate Nutrition 0.000 claims description 6
- ROOXNKNUYICQNP-UHFFFAOYSA-N ammonium persulfate Chemical compound [NH4+].[NH4+].[O-]S(=O)(=O)OOS([O-])(=O)=O ROOXNKNUYICQNP-UHFFFAOYSA-N 0.000 claims description 6
- 235000019395 ammonium persulphate Nutrition 0.000 claims description 6
- AYJRCSIUFZENHW-UHFFFAOYSA-L barium carbonate Chemical compound [Ba+2].[O-]C([O-])=O AYJRCSIUFZENHW-UHFFFAOYSA-L 0.000 claims description 6
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 6
- 239000000292 calcium oxide Substances 0.000 claims description 6
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 239000004021 humic acid Substances 0.000 claims description 6
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 6
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 6
- 239000000347 magnesium hydroxide Substances 0.000 claims description 6
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 6
- 159000000000 sodium salts Chemical class 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 102000004160 Phosphoric Monoester Hydrolases Human genes 0.000 claims description 3
- 108090000608 Phosphoric Monoester Hydrolases Proteins 0.000 claims description 3
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
- 238000001354 calcination Methods 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000010439 graphite Substances 0.000 claims description 3
- 229910002804 graphite Inorganic materials 0.000 claims description 3
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims description 3
- 239000002105 nanoparticle Substances 0.000 claims description 3
- 239000012299 nitrogen atmosphere Substances 0.000 claims description 3
- 229910000166 zirconium phosphate Inorganic materials 0.000 claims description 3
- LEHFSLREWWMLPU-UHFFFAOYSA-B zirconium(4+);tetraphosphate Chemical compound [Zr+4].[Zr+4].[Zr+4].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LEHFSLREWWMLPU-UHFFFAOYSA-B 0.000 claims description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 3
- 238000005299 abrasion Methods 0.000 abstract 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 239000002202 Polyethylene glycol Substances 0.000 abstract 1
- 238000013021 overheating Methods 0.000 abstract 1
- 229920001223 polyethylene glycol Polymers 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Compositions Of Oxide Ceramics (AREA)
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105568202A (zh) * | 2015-12-18 | 2016-05-11 | 合肥中澜新材料科技有限公司 | 一种耐腐蚀发动机汽缸内壁耐磨涂层及其制备方法 |
CN106278254A (zh) * | 2016-08-09 | 2017-01-04 | 东莞市晶谷新材料技术有限公司 | 一种高强高韧陶瓷复合材料及其在制造刀具中的应用 |
CN106588061A (zh) * | 2016-12-07 | 2017-04-26 | 苏州洛特兰新材料科技有限公司 | 一种添加有羰基镍粉的陶瓷复合材料及其制备方法 |
CN106747433A (zh) * | 2017-02-28 | 2017-05-31 | 安徽拓吉泰新型陶瓷科技有限公司 | 氧化锆基纳米陶瓷工模具材料及其制备方法 |
CN108751988A (zh) * | 2018-07-03 | 2018-11-06 | 贵州大学 | 一种磷石膏和粉煤灰制酸联产陶瓷刀具材料的工艺 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH04503329A (ja) * | 1988-11-03 | 1992-06-18 | ケンナメタル インコーポレイテッド | アルミナージルコニアーカーバイド ホイスカーにより強化された切削工具 |
CN1418849A (zh) * | 2002-12-25 | 2003-05-21 | 天津大学 | 可用wc刀具加工的氧化锆基陶瓷材料 |
CN101121971A (zh) * | 2007-09-10 | 2008-02-13 | 山东大学 | 一种碳化钨-氧化锆-氧化铝复合刀具材料的制备方法 |
CN101602111A (zh) * | 2009-06-23 | 2009-12-16 | 邓湘凌 | 超强超韧陶瓷刀具及其制作方法 |
CN101798216A (zh) * | 2010-03-23 | 2010-08-11 | 山东轻工业学院 | 添加硼化钛的氧化锆基纳米陶瓷工模具材料及其制备方法 |
-
2014
- 2014-10-27 CN CN201410580896.5A patent/CN104370542B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH04503329A (ja) * | 1988-11-03 | 1992-06-18 | ケンナメタル インコーポレイテッド | アルミナージルコニアーカーバイド ホイスカーにより強化された切削工具 |
CN1418849A (zh) * | 2002-12-25 | 2003-05-21 | 天津大学 | 可用wc刀具加工的氧化锆基陶瓷材料 |
CN101121971A (zh) * | 2007-09-10 | 2008-02-13 | 山东大学 | 一种碳化钨-氧化锆-氧化铝复合刀具材料的制备方法 |
CN101602111A (zh) * | 2009-06-23 | 2009-12-16 | 邓湘凌 | 超强超韧陶瓷刀具及其制作方法 |
CN101798216A (zh) * | 2010-03-23 | 2010-08-11 | 山东轻工业学院 | 添加硼化钛的氧化锆基纳米陶瓷工模具材料及其制备方法 |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105568202A (zh) * | 2015-12-18 | 2016-05-11 | 合肥中澜新材料科技有限公司 | 一种耐腐蚀发动机汽缸内壁耐磨涂层及其制备方法 |
CN106278254A (zh) * | 2016-08-09 | 2017-01-04 | 东莞市晶谷新材料技术有限公司 | 一种高强高韧陶瓷复合材料及其在制造刀具中的应用 |
CN106278254B (zh) * | 2016-08-09 | 2019-04-12 | 东莞市晶谷新材料技术有限公司 | 一种高强高韧陶瓷复合材料及其在制造刀具中的应用 |
CN106588061A (zh) * | 2016-12-07 | 2017-04-26 | 苏州洛特兰新材料科技有限公司 | 一种添加有羰基镍粉的陶瓷复合材料及其制备方法 |
CN106747433A (zh) * | 2017-02-28 | 2017-05-31 | 安徽拓吉泰新型陶瓷科技有限公司 | 氧化锆基纳米陶瓷工模具材料及其制备方法 |
CN106747433B (zh) * | 2017-02-28 | 2020-05-08 | 安徽拓吉泰新型陶瓷科技有限公司 | 氧化锆基纳米陶瓷工模具材料及其制备方法 |
CN108751988A (zh) * | 2018-07-03 | 2018-11-06 | 贵州大学 | 一种磷石膏和粉煤灰制酸联产陶瓷刀具材料的工艺 |
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