CN104368290A - Method for preparing aqueous solution of titanium tetrachloride, and apparatus thereof - Google Patents
Method for preparing aqueous solution of titanium tetrachloride, and apparatus thereof Download PDFInfo
- Publication number
- CN104368290A CN104368290A CN201310357522.2A CN201310357522A CN104368290A CN 104368290 A CN104368290 A CN 104368290A CN 201310357522 A CN201310357522 A CN 201310357522A CN 104368290 A CN104368290 A CN 104368290A
- Authority
- CN
- China
- Prior art keywords
- titanium tetrachloride
- reactor
- aqueous solution
- valve
- water
- Prior art date
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- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 title claims abstract description 96
- 239000007864 aqueous solution Substances 0.000 title claims abstract description 65
- 238000000034 method Methods 0.000 title claims abstract description 29
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 81
- 239000008367 deionised water Substances 0.000 claims abstract description 42
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 33
- 238000006243 chemical reaction Methods 0.000 claims abstract description 24
- 238000010521 absorption reaction Methods 0.000 claims abstract description 12
- 239000007788 liquid Substances 0.000 claims description 26
- JEGUKCSWCFPDGT-UHFFFAOYSA-N h2o hydrate Chemical compound O.O JEGUKCSWCFPDGT-UHFFFAOYSA-N 0.000 claims description 10
- 238000002242 deionisation method Methods 0.000 claims description 9
- 230000001105 regulatory effect Effects 0.000 claims description 8
- 238000003860 storage Methods 0.000 claims description 7
- 239000000376 reactant Substances 0.000 claims description 5
- 238000004891 communication Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 230000007062 hydrolysis Effects 0.000 abstract description 5
- 238000006460 hydrolysis reaction Methods 0.000 abstract description 5
- 238000002360 preparation method Methods 0.000 description 24
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 15
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 15
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 15
- 239000007789 gas Substances 0.000 description 13
- 239000000243 solution Substances 0.000 description 10
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 9
- 235000010215 titanium dioxide Nutrition 0.000 description 6
- 238000012360 testing method Methods 0.000 description 5
- 229910003074 TiCl4 Inorganic materials 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 239000004408 titanium dioxide Substances 0.000 description 3
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 2
- 239000005977 Ethylene Substances 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 230000001276 controlling effect Effects 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000006096 absorbing agent Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- UFNOKFQJIDUZIU-UHFFFAOYSA-J ethene titanium(4+) tetrachloride Chemical group C=C.[Cl-].[Cl-].[Cl-].[Cl-].[Ti+4] UFNOKFQJIDUZIU-UHFFFAOYSA-J 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000011941 photocatalyst Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 230000007306 turnover Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00099—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00177—Controlling or regulating processes controlling the pH
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310357522.2A CN104368290B (en) | 2013-08-16 | 2013-08-16 | The preparation method of titanium tetrachloride aqueous solution and device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201310357522.2A CN104368290B (en) | 2013-08-16 | 2013-08-16 | The preparation method of titanium tetrachloride aqueous solution and device |
Publications (2)
Publication Number | Publication Date |
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CN104368290A true CN104368290A (en) | 2015-02-25 |
CN104368290B CN104368290B (en) | 2016-08-24 |
Family
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Family Applications (1)
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CN201310357522.2A Active CN104368290B (en) | 2013-08-16 | 2013-08-16 | The preparation method of titanium tetrachloride aqueous solution and device |
Country Status (1)
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CN (1) | CN104368290B (en) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107469753A (en) * | 2017-09-25 | 2017-12-15 | 河南师范大学 | A kind of new chemical experimental robot |
CN108183141A (en) * | 2017-12-28 | 2018-06-19 | 成都中建材光电材料有限公司 | A kind of cadmium telluride thin-film battery of new structure and preparation method thereof |
CN108795105A (en) * | 2018-07-18 | 2018-11-13 | 黄山幻彩颜料科技有限公司 | A kind of stable quality, efficiently, the hydrolysis process of the production pearlescent pigment of environmental protection |
CN108854617A (en) * | 2018-06-06 | 2018-11-23 | 杭州弗沃德精细化工有限公司 | A kind of titanium tetrachloride aqueous solution device for formulating and method |
CN109111340A (en) * | 2018-10-26 | 2019-01-01 | 浙江众成包装材料股份有限公司 | Serialization prepares the high pressure reaction assembly of 1- (1- bromoethyl) -4- chloromethylbenzene |
CN109364787A (en) * | 2018-11-19 | 2019-02-22 | 云南昆船环保技术有限公司 | A kind of alcohol concentration auto-scheduling system and its concocting method |
CN111253795A (en) * | 2020-01-17 | 2020-06-09 | 营口盼盼硅藻材料集团有限公司 | Production process and device of purifying material |
CN113731329A (en) * | 2021-08-31 | 2021-12-03 | 沈阳工程学院 | Titanium tetrachloride aqueous solution preparation device |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2870071A (en) * | 1953-10-30 | 1959-01-20 | Ionics | Electrolytic production of titanium tetrahalides |
CN201151738Y (en) * | 2007-12-17 | 2008-11-19 | 贵阳铝镁设计研究院 | Reducing distillation reactor |
CN203469964U (en) * | 2013-08-16 | 2014-03-12 | 河南龙兴钛业有限公司 | Device for preparing titanium tetrachloride water solution |
-
2013
- 2013-08-16 CN CN201310357522.2A patent/CN104368290B/en active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2870071A (en) * | 1953-10-30 | 1959-01-20 | Ionics | Electrolytic production of titanium tetrahalides |
CN201151738Y (en) * | 2007-12-17 | 2008-11-19 | 贵阳铝镁设计研究院 | Reducing distillation reactor |
CN203469964U (en) * | 2013-08-16 | 2014-03-12 | 河南龙兴钛业有限公司 | Device for preparing titanium tetrachloride water solution |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107469753A (en) * | 2017-09-25 | 2017-12-15 | 河南师范大学 | A kind of new chemical experimental robot |
CN108183141A (en) * | 2017-12-28 | 2018-06-19 | 成都中建材光电材料有限公司 | A kind of cadmium telluride thin-film battery of new structure and preparation method thereof |
CN108854617A (en) * | 2018-06-06 | 2018-11-23 | 杭州弗沃德精细化工有限公司 | A kind of titanium tetrachloride aqueous solution device for formulating and method |
CN108854617B (en) * | 2018-06-06 | 2020-09-15 | 杭州弗沃德精细化工有限公司 | Titanium tetrachloride aqueous solution preparation device and method |
CN108795105A (en) * | 2018-07-18 | 2018-11-13 | 黄山幻彩颜料科技有限公司 | A kind of stable quality, efficiently, the hydrolysis process of the production pearlescent pigment of environmental protection |
CN109111340A (en) * | 2018-10-26 | 2019-01-01 | 浙江众成包装材料股份有限公司 | Serialization prepares the high pressure reaction assembly of 1- (1- bromoethyl) -4- chloromethylbenzene |
CN109364787A (en) * | 2018-11-19 | 2019-02-22 | 云南昆船环保技术有限公司 | A kind of alcohol concentration auto-scheduling system and its concocting method |
CN111253795A (en) * | 2020-01-17 | 2020-06-09 | 营口盼盼硅藻材料集团有限公司 | Production process and device of purifying material |
CN113731329A (en) * | 2021-08-31 | 2021-12-03 | 沈阳工程学院 | Titanium tetrachloride aqueous solution preparation device |
Also Published As
Publication number | Publication date |
---|---|
CN104368290B (en) | 2016-08-24 |
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SE01 | Entry into force of request for substantive examination | ||
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CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 459000 Jiyuan City, Henan Province, tiger Ridge Industrial Cluster Spring Village Patentee after: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY CO.,LTD. Address before: 459000 Jiyuan City, Henan Province, tiger Ridge Industrial Cluster Spring Village Patentee before: HENAN LONGXING TITANIUM Co.,Ltd. |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Method for preparing aqueous solution of titanium tetrachloride, and apparatus thereof Effective date of registration: 20181024 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY CO.,LTD. Registration number: 2018990000988 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
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Date of cancellation: 20191220 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY CO.,LTD. Registration number: 2018990000988 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Method for preparing aqueous solution of titanium tetrachloride, and apparatus thereof Effective date of registration: 20191220 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY CO.,LTD. Registration number: Y2019990000777 |
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Date of cancellation: 20201023 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY Co.,Ltd. Registration number: Y2019990000777 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method and device of titanium tetrachloride aqueous solution Effective date of registration: 20201104 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY Co.,Ltd. Registration number: Y2020980007498 |
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Date of cancellation: 20210901 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY Co.,Ltd. Registration number: Y2020980007498 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation method and device of titanium tetrachloride aqueous solution Effective date of registration: 20210903 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY Co.,Ltd. Registration number: Y2021980008781 |
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Date of cancellation: 20221009 Granted publication date: 20160824 Pledgee: Bank of China Limited by Share Ltd. Jiyuan branch Pledgor: HENAN LONGXING TITANIUM INDUSTRY TECHNOLOGY CO.,LTD. Registration number: Y2021980008781 |