CN104356830B - A kind of construction waterproof coating and preparation method thereof - Google Patents
A kind of construction waterproof coating and preparation method thereof Download PDFInfo
- Publication number
- CN104356830B CN104356830B CN201410679262.5A CN201410679262A CN104356830B CN 104356830 B CN104356830 B CN 104356830B CN 201410679262 A CN201410679262 A CN 201410679262A CN 104356830 B CN104356830 B CN 104356830B
- Authority
- CN
- China
- Prior art keywords
- parts
- weight
- acid
- paligorskite
- epoxychloropropane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
Abstract
This construction waterproof coating, is made up of the raw material of following parts by weight: base fluid 100 parts, Paligorskite 30 parts, vanadic anhydride 12 parts, polyaluminium chloride 8 parts, 2 ethyl imidazol(e) 1 part, hydroxypropyl methyl cellulose 5 parts, epoxychloropropane 4 parts, dioctyl succinate disulfonate acid 1 part, sulfamic acid 0.3 part；Defoamer 1 part.The present invention utilizes Tao Shi pure-acrylic emulsion UCAR H 371,2 ethyl imidazol(e), hydroxypropyl methyl cellulose, epoxychloropropane；Add the auxiliary agents such as dioctyl succinate disulfonate acid, sulfamic acid, defoamer to be blended；Especially add Paligorskite, vanadic anhydride, the active filler of polyaluminium chloride composition；Not only increase the combination properties such as the mechanics of waterproof material, heatproof, acid and alkali-resistance, and be easy to constructing operation.
Description
Technical field
The invention belongs to construction engineering technical field, be specially a kind of construction waterproof coating its preparation method.
Background technology
Waterproof material on market has two big classes: one is polyurethanes water-repellent paint.This kind of material is usually and is made up as raw material with coal tar of polyurethane.The tar gas toxicity that it is volatilized is big, and is not easy to remove, and is therefore prohibited from using in China in 2000.Still at the polyurethane waterproofing coating sold, it is to replace coal tar as raw material with Colophonium.But when using this coating, general employing dilutes containing the organic solvent such as toluene, dimethylbenzene, thus also containing toxic；Another kind of for polymer cement-base waterproof coating.The emulsion that it is synthesized by multiple waterborne polymeric forms with the high grade cement mixed with various additives, and the flexibility of polymer (resin) becames one with the rigidity of cement so that it shows excellence impervious in terms of stability.Its advantage is that easy construction, comprehensive cost are low, and the duration is short, and asepsis environment-protecting.Therefore, polyalcohol cement basis has become as the leading role in water-repellent paint market.
Publication No. CN 1935930A discloses " preparation method of a kind of ethylene-ethylene acetate copolymer asphalt water-proof coiled material ".After utilizing master batch of bitumen and ethylene-acetate ethylene copolymer mixing and stirring, directly extrusion is made, and the coiled material more all kinds of coiled material performance made all increases, but waterproof coiled material construction process is complicated, and stickiness relatively coating is poor.
Publication No. CN 101113276A discloses " a kind of coating composition containing acetate ethylene copolymer ".Two kinds of bases as coating with ethylene-vinyl acetate copolymer fluid and ethylene bottom oil, add various filler and auxiliary agent, prepared coating has the advantages such as good water-fast weatherability, flexibility, wet viscosity, this method requires higher for ambient temperature, being not suitable for operation in winter, human body can be damaged by the ethylene bottom oil Long Term Contact in product.
Summary of the invention
Present invention aim to overcome that deficiency of the prior art, it is provided that a kind of construction waterproof coating its preparation method, use the method to prepare coating and there is good mechanical property, high temperature resistant low temperature properties and excellent anticorrosive.
Construction waterproof coating of the present invention, it is characterised in that be made up of the raw material of following parts by weight:
Base fluid 94～106 parts, active filler 45～54 parts, thickening agent 8～11 parts,
Surfactant 1～2 parts, PH regulator 0.2～0.5 part, defoamer 1～1.5 parts；
Described base fluid is Tao Shi pure-acrylic emulsion UCAR H-371；
Described active filler is made up of Paligorskite, vanadic anhydride, polyaluminium chloride；
Described thickening agent is made up of 2-ethyl imidazol(e), hydroxypropyl methyl cellulose, epoxychloropropane；
Described surfactant is dioctyl succinate disulfonate acid；
Described PH regulator is sulfamic acid；
Described defoamer is BYK-019.
As optimization, this construction waterproof coating, is made up of the raw material of following parts by weight: base fluid 100 parts, Paligorskite 30 parts, vanadic anhydride 12 parts, polyaluminium chloride 8 parts, 2-ethyl imidazol(e) 1 part, hydroxypropyl methyl cellulose 5 parts, epoxychloropropane 4 parts, dioctyl succinate disulfonate acid 1 part, sulfamic acid 0.3 part；Defoamer 1 part.
The method preparing this construction waterproof coating, comprises the following steps:
A, the Paligorskite by described parts by weight, vanadic anhydride, polyaluminium chloride are respectively prepared the powder of 800～1000 mesh, are then added to stirrer for mixing uniform；
B, described parts by weight 2-ethyl imidazol(e), hydroxypropyl methyl cellulose, epoxychloropropane are joined in the mixture in step a under the conditions of 80～90 DEG C the speed with 600～800 turns/min stir 40 minutes；
C, described parts by weight Tao Shi pure-acrylic emulsion UCAR H-371, dioctyl succinate disulfonate acid are joined in the mixture in step b the speed with 1000～1200 turns/min stir 60 minutes；
D, described parts by weight sulfamic acid, BYK-019 are joined in the mixture in step c with the speed of 400～500 turns/min stir 30 minutes both finished product.
The present invention utilizes Tao Shi pure-acrylic emulsion UCAR H-371,2-ethyl imidazol(e), hydroxypropyl methyl cellulose, epoxychloropropane；Add the auxiliary agents such as dioctyl succinate disulfonate acid, sulfamic acid, defoamer to be blended；Especially add Paligorskite, vanadic anhydride, the active filler of polyaluminium chloride composition；Not only increase the combination properties such as the mechanics of waterproof material, heatproof, acid and alkali-resistance, and be easy to constructing operation.
The present invention prepares construction waterproof coating, and not only preparation technology is simple, high comprehensive performance, thus realizes various construction；Meanwhile, the membrane waterproofing formed has excellent mechanical property, chemical stability and a corrosion resistance, and nontoxic, harmless, pollution-free, odorlessness, it is a kind of environment-friendly type building water-repellent paint.
In blade coating embodiment 1, embodiment 2, embodiment 3, waterproof material is according to standard testings such as GB/T16777-2008 building water-proof paint method of testings, and its properties is as shown in table 1:
Detailed description of the invention
Example given below intends that the invention will be further described, but is not to be construed as limiting the scope of the invention, and those skilled in the art, according to some nonessential improvement and adjustment to the present invention of present invention, still fall within protection scope of the present invention.
Embodiment 1:a, take Paligorskite 30 grams, vanadic anhydride 12 grams, polyaluminium chloride 8 grams are respectively prepared the powder of 800～1000 mesh, are then added to stirrer for mixing uniform；
B, take in 2-ethyl imidazol(e) 1 gram, hydroxypropyl methyl cellulose 5 grams, 4 grams of mixture joining in step a of epoxychloropropane under the conditions of 80～90 DEG C the speed with 600～800 turns/min and stir 40 minutes；
C, take Tao Shi pure-acrylic emulsion UCAR H-371,100 grams, 1 gram of mixture joining in step b of dioctyl succinate disulfonate acid stirs 60 minutes with the speed of 1000～1200 turns/min；
D, take sulfamic acid 0.3 gram, BYK-019, in 1 gram of mixture joining in step c with the speed of 400～500 turns/min stir 30 minutes both finished product.
Embodiment 2:a, take Paligorskite 27 grams, vanadic anhydride 11 grams, polyaluminium chloride 7 grams are respectively prepared the powder of 800～1000 mesh, are then added to stirrer for mixing uniform；
B, take in 2-ethyl imidazol(e) 0.8 gram, hydroxypropyl methyl cellulose 4 grams, 3.2 grams of mixture joining in step a of epoxychloropropane under the conditions of 80～90 DEG C the speed with 600～800 turns/min and stir 40 minutes；
C, take Tao Shi pure-acrylic emulsion UCAR H-371,94 grams, 1 gram of mixture joining in step b of dioctyl succinate disulfonate acid stirs 60 minutes with the speed of 1000～1200 turns/min；
D, take sulfamic acid 0.2 gram, BYK-019, in 1 gram of mixture joining in step c with the speed of 400～500 turns/min stir 30 minutes both finished product.
Embodiment 3:a, take Paligorskite 32 grams, vanadic anhydride 13 grams, polyaluminium chloride 9 grams are respectively prepared the powder of 800～1000 mesh, are then added to stirrer for mixing uniform；
B, take in 2-ethyl imidazol(e) 1.2 grams, hydroxypropyl methyl cellulose 5.5 grams, 4.3 grams of mixture joining in step a of epoxychloropropane under the conditions of 80～90 DEG C the speed with 600～800 turns/min and stir 40 minutes；
C, take Tao Shi pure-acrylic emulsion UCAR H-371,106 grams, 1 gram of mixture joining in step b of dioctyl succinate disulfonate acid stirs 60 minutes with the speed of 1000～1200 turns/min；
D, take sulfamic acid 0.5 gram, BYK-019, in 1.5 grams of mixture joining in step c with the speed of 400～500 turns/min stir 30 minutes both finished product.
Claims (3)
1. a construction waterproof coating, it is characterised in that be made up of the raw material of following parts by weight:
Base fluid 94～106 parts, active filler 45～54 parts, thickening agent 8～11 parts,
Surfactant 1～2 parts, pH adjusting agent 0.2～0.5 part, defoamer 1～1.5 parts；
Described base fluid is Tao Shi pure-acrylic emulsion UCAR H-371；
Described active filler is made up of Paligorskite, vanadic anhydride, polyaluminium chloride；
Described thickening agent is made up of 2-ethyl imidazol(e), hydroxypropyl methyl cellulose, epoxychloropropane；
Described surfactant is dioctyl succinate disulfonate acid；
Described PH regulator is sulfamic acid；
Described defoamer is BYK-019.
Construction waterproof coating the most according to claim 1, it is characterised in that be made up of the raw material of following parts by weight: base fluid 100 parts, Paligorskite 30 parts, vanadic anhydride 12 parts, polyaluminium chloride 8 parts, 2-ethyl imidazol(e) 1 part, hydroxypropyl methyl cellulose 5 parts, epoxychloropropane 4 parts, dioctyl succinate disulfonate acid 1 part, sulfamic acid 0.3 part, defoamer 1 part.
3. the method preparing construction waterproof coating described in claim 2, it is characterised in that comprise the following steps:
A, the Paligorskite by described parts by weight, vanadic anhydride, polyaluminium chloride are respectively prepared the powder of 800～1000 mesh, are then added to stirrer for mixing uniform；
B, described parts by weight 2-ethyl imidazol(e), hydroxypropyl methyl cellulose, epoxychloropropane are joined in the mixture in step a under the conditions of 80～90 DEG C the speed with 600～800 turns/min stir 40 minutes；
C, described parts by weight Tao Shi pure-acrylic emulsion UCAR H-371, dioctyl succinate disulfonate acid are joined in the mixture in step b the speed with 1000～1200 turns/min stir 60 minutes；
D, join described weight number sulfamic acid, BYK-019 the mixture of step c stirs with the speed of 400～500 turns/min and get product for 30 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410679262.5A CN104356830B (en) | 2014-11-24 | 2014-11-24 | A kind of construction waterproof coating and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410679262.5A CN104356830B (en) | 2014-11-24 | 2014-11-24 | A kind of construction waterproof coating and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104356830A CN104356830A (en) | 2015-02-18 |
| CN104356830B true CN104356830B (en) | 2016-08-24 |
Family
ID=52524152
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410679262.5A Active CN104356830B (en) | 2014-11-24 | 2014-11-24 | A kind of construction waterproof coating and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104356830B (en) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106966683A (en) * | 2017-03-29 | 2017-07-21 | 合肥天沃能源科技有限公司 | It is a kind of for energy-saving coatings of glass and preparation method thereof |
| CN106928779A (en) * | 2017-03-29 | 2017-07-07 | 合肥天沃能源科技有限公司 | A kind of energy-saving wall coating and preparation method thereof |
| CN113122096A (en) * | 2021-04-21 | 2021-07-16 | 湖南加美乐素新材料股份有限公司 | Transparent water-based waterproof coating for buildings and preparation method thereof |
| CN113185884A (en) * | 2021-06-22 | 2021-07-30 | 陆安怡 | Low-cost environment-friendly waterproof building coating and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101486868A (en) * | 2009-02-23 | 2009-07-22 | 长沙凯德防水涂料有限公司 | Sheet metal roofing waterproof coating material and preparation thereof |
| CN103897526A (en) * | 2012-12-26 | 2014-07-02 | 郑红 | Waterproof coating used for external walls |
-
2014
- 2014-11-24 CN CN201410679262.5A patent/CN104356830B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101486868A (en) * | 2009-02-23 | 2009-07-22 | 长沙凯德防水涂料有限公司 | Sheet metal roofing waterproof coating material and preparation thereof |
| CN103897526A (en) * | 2012-12-26 | 2014-07-02 | 郑红 | Waterproof coating used for external walls |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104356830A (en) | 2015-02-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104356830B (en) | A kind of construction waterproof coating and preparation method thereof | |
| CN103113777B (en) | A kind of environment-friendly type aqueous high cohesive strength putty paste and preparation method thereof | |
| CN104140231A (en) | Environment-friendly waterproof mortar | |
| CN102604561A (en) | Aqueous adhesive and preparation method thereof | |
| CN101244913A (en) | Polyalcohol concrete base rigidity water-proofing material | |
| CN104250495A (en) | Preparation process of natural color sand really stone paint | |
| CN104513561A (en) | Waterproof paint | |
| CN104194630A (en) | Novel waterproof bonding coating and preparation method thereof | |
| CN102911602B (en) | Single-component polymer modified asphalt waterproofing paint and preparation method thereof | |
| CN102675999B (en) | Water-based fluorocarbon paint for silicate concrete curbs and preparation method thereof | |
| CN106221506A (en) | A kind of epoxy emulsion and preparation method thereof | |
| CN1986653A (en) | Outer wall putty | |
| CN104371466A (en) | Water-based colourful slice coating and preparation method thereof | |
| CN103468136B (en) | A kind of Environmental-protecwaterproof waterproof paint | |
| CN103694855B (en) | Water-base epoxy waterproof paint and preparation method thereof | |
| CN102391756B (en) | Weather-resistant liquid-state granite coating | |
| CN104403534A (en) | Aqueous primer matched with UV finish on electronic product plastic shell, and preparation method thereof | |
| CN104263122A (en) | Stable paint | |
| CN106243815A (en) | A kind of have the additive improving metope alignment material workability | |
| CN102220069A (en) | Aqueous epoxy coal tar paint and preparation method thereof | |
| CN104087139A (en) | Preparation method for composite waterproof coating | |
| CN103805091A (en) | Waterproof adhesive for building | |
| CN104292999A (en) | Anti-cracking waterproof coating for automobile | |
| CN109135454A (en) | A kind of colorful noctilucent emulsion glue and preparation method thereof | |
| CN108047869A (en) | A kind of no-solvent type polyurethane gravity flow self-leveling floor paint and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| CB03 | Change of inventor or designer information |
Inventor after: Peng Tianbin Inventor after: Luo Hong Inventor after: Peng Yonghui Inventor after: Bao Lvping Inventor after: Luo Diening Inventor after: Fang Zhen Inventor after: Dai Jinzhu Inventor after: Hu Jianfeng Inventor after: Huang Xinyuan Inventor after: Wang Xuebo Inventor before: Zhang Qiaomu |
|
| COR | Change of bibliographic data | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160601 Address after: 315100, Nanjing Road, Zhejiang, Ningbo, No. 1688 Applicant after: The deep blue sea, Zhejiang municipal administration gardens construction Co., Ltd Address before: 030001, room 122, 9225 Xuefu street, Xiaodian District, Shanxi, Taiyuan Applicant before: Zhang Qiaomu |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information |
Inventor after: Peng Tianbin Inventor after: Luo Hong Inventor after: Peng Yonghui Inventor after: Bao Lvping Inventor after: Luo Diening Inventor after: Fang Zhen Inventor after: Dai Jinzhu Inventor after: Hu Jianfeng Inventor after: Huang Xinyuan Inventor after: Wang Xuebo Inventor before: Peng Tianbin Inventor before: Luo Hong Inventor before: Peng Yonghui Inventor before: Bao Lvping Inventor before: Luo Diening Inventor before: Fang Zhen Inventor before: Dai Jinzhu Inventor before: Hu Jianfeng Inventor before: Huang Xinyuan Inventor before: Wang Xuebo |
|
| COR | Change of bibliographic data | ||
| CP03 | Change of name, title or address | ||
| CP03 | Change of name, title or address |
Address after: No. 3388, Yinzhou District Cang Hai Road, Yinzhou District, Ningbo, Zhejiang Patentee after: Zhejiang sea Construction Co., Ltd. Address before: No. 1688 ningheng Road, Ningbo, Zhejiang Province, Zhejiang Patentee before: The deep blue sea, Zhejiang municipal administration gardens construction Co., Ltd |