CN104305511A - Application of spices made of green plums to cigarettes - Google Patents

Application of spices made of green plums to cigarettes Download PDF

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Publication number
CN104305511A
CN104305511A CN201410412799.5A CN201410412799A CN104305511A CN 104305511 A CN104305511 A CN 104305511A CN 201410412799 A CN201410412799 A CN 201410412799A CN 104305511 A CN104305511 A CN 104305511A
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CN
China
Prior art keywords
spices
cigarettes
cigarette
green plums
application
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410412799.5A
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Chinese (zh)
Inventor
党立志
冯洪涛
段焰青
徐若飞
廖头根
夏建军
王明锋
王文元
刘亚
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China Tobacco Yunnan Industrial Co Ltd
Original Assignee
China Tobacco Yunnan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Yunnan Industrial Co Ltd filed Critical China Tobacco Yunnan Industrial Co Ltd
Priority to CN201410412799.5A priority Critical patent/CN104305511A/en
Publication of CN104305511A publication Critical patent/CN104305511A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances

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  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention discloses application of spices made of green plums to cigarettes. The green plums are washed; kernels of the green plums are removed; the green plums are soaked with red wine; reflux extraction and filtering are carried out; and then the needed spices for the cigarettes are obtained. The spices serve as backing materials to be evenly sprinkled to cut tobaccos; and then constant temperature and constant humidity balancing is carried out for 24 h. After effective constituents in the green plums and special aroma of the green plums are compounded with the cut tobaccos, the quality of the cigarettes can be effectively improved and the aroma quality of the cigarettes can be improved. According to the application of the spices made of the green plums to the cigarettes, the technical process is simple; operation is easy; cost is low; the spices ate suitable for application and popularization and are of positive significance in improving the sound development of the cigarette industry.

Description

The application of green plum spices in cigarette
Technical field
The invention belongs to cigarette additive technical field, be specifically related to a kind of embody rule of spices in production of cigarettes taking green plum as raw material and prepare.
Background technology
Tobacco is one of mainstay of China's finance.State Tobacco Monopoly Bureau explicitly points out Eleventh Five-Year Plan Chinese cigarette development in science and technology outline the 7th article, " will capture the key technology affecting tobacco aroma quality, perfume quantity ", reduces and external quality of tobacco gap, to improve the competing power in domestic and international market.Existing tobacco aromatics, at rectification fragrance, is promoted and is inhaled taste, suppresses excitant and assorted taste aspect effect not to be very good, and the fragrance in cigarette is difficult to keep for a long time.
Green plum is the fruit of perennial deciduous fruit tree, green plum shape subcircular, and pericarp color is oyster, uniform color, and the pericarp color of seconds allows a small amount of blush; Domestic like product is generally that fruit shape is oval, the shallow dark green of pericarp, and mellow fruit is yellow, sunny slope has blush, and in light russet to peony, pulp is faint yellow, average 28 grams of single fruit weight, pulp is thick, core is little, edible rate >89%, and pulp is delicate, fragrance is mellow, unique flavor, is with sweet in acid, domestic like product mildly bitter flavor or micro-puckery.Green plum is containing soluble solid 7.0%, and total acid content >4.3%, is rich in various trace elements, amino acid, vitamins c, and has in acid with sweet fragrance.The one-tenth of green plum is grouped into has following characteristics: nutritious, low sugar peracid, and its T value (sugar-acid ratio) is only 0.2.Secondly, it has rational calcium-phosphorus ratio, its Ca/P ≈ 1:1, and in addition, containing VB up to 5.6mg/100g, and VB2 is in very stable peracidity environment.Modern medicine study shows, green plum has following effect: 1, dispelling fatigue, enhances vigour, 2, antitumor; remove blood rubbish, 3, significantly improve functions of intestines and stomach, 4, protection liver; 5, antibacterial, expelling parasite, anti-allergic effects, 6, delay senility, keep effect such as beauty treatment grade.At present, green plum because of its fresh fruit too sour, except a small amount of for except eating raw, most for being processed into preserved fruit, preserved fruit, medicinal material and health food, cosmetics etc.
Nutritional labeling in green plum particularly fragrance can promote the suction taste of cigarette, suppresses tobacco excitant and assorted taste, soft fine and smooth flue gas, and reducing throat stimulates, and improves throat's comfortableness.But in prior art, the nutriment of green plum and fragrance are extracted, and also there is no relevant report at present as the method that essence spice for cigarette is applied in cigarette.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide the embody rule of a kind of green plum spices in production of cigarettes, in order to promote the flavouring essence quality of cigarette product.
Object of the present invention is achieved by following technical proposals.
Except as otherwise noted, the percentage adopted in the present invention is mass percent.
The application of green plum spices in cigarette, is characterized in that: cleaned by green plum, weigh after stoning, soak, refluxing extraction 1 ~ 3 hour with the red wine of 5 ~ 10 times amount, and filtration gained clear liquid is required spices; At cigarette primary processing feeding stage, be sprayed at equably on pipe tobacco by described spices, addition is 5 ~ 20g/ case, and is 60% in humidity, and temperature is under 22 DEG C of conditions, constant temperature and humidity balance 24h.
Compared with prior art, the present invention has the following advantages:
1. the present invention utilizes green plum to prepare essence spice for cigarette initiatively, and adds in cigarette with bed material form, achieves good technique effect.
2. the active ingredient in green plum and its distinctive fragrance with pipe tobacco compound after, effectively can improve the quality of cigarette, improve the aroma quality of cigarette.
3. present invention process is simple, processing ease, and cost is low, is suitable for applying, and developing in a healthy way to promotion cigarette industry has positive effect.
Detailed description of the invention
By the following examples, the present invention is described in further detail.Should be appreciated that specific embodiment described herein only in order to explain the present invention, be not limited to the technical solution.
Embodiment 1
1. get green plum 100g, add the red wine of 5 times, refluxing extraction 1.0 hours, filters out impurity after having extracted, and namely gained clear liquid obtains the present invention.
2. pair aroma component of the present invention detects, testing result shows, the flavor matter that in this extract, content is higher mainly contains vanillic aldehyde, benzaldehyde, phenylacetaldehyde, 4-methylphenol, isoamyl alcohol, 2-methyl butanol, benzyl carbinol, ethanol, phenmethylol, 4-hydroxylphenylethyl alcohol, 4 hydroxybutyric acid ethyl ester, ethyl benzoate, ethyl acetate, palmitic acid, malic acid, β-dihydroionone, fumaric acid etc.
3. it can be used as bed material to be sprayed at equably on pipe tobacco, addition is 8g/ case, and not add spiced tobacco leaf for contrast.After the pipe tobacco of processed group and control group is put into climatic chamber inner equilibrium 24h, make cigarette, sample and the equal random number of contrast, the group of smokeing panel test be made up of the expert that smokes panel test carries out sensory evaluating smoking.Perfuming result of the test of smokeing panel test shows that this perfume additive and the comparatively harmony of cigarette perfume (or spice) can significantly improve cigarette perfume (or spice), fine and smooth alcohol and flue gas, reduction excitant, cover assorted gas, improve cigarette odor-absorbing, and produces a kind of pure and fresh special note.
Embodiment 2
1. get green plum sample 100g, add the red wine of 5 times, refluxing extraction 1.5 hours, filters out impurity after having extracted, and namely gained clear liquid obtains the present invention.
2. pair aroma component of the present invention detects, testing result shows, the flavor matter that in this extract, content is higher mainly contains vanillic aldehyde, benzaldehyde, phenylacetaldehyde, 4-methylphenol, isoamyl alcohol, 2-methyl butanol, benzyl carbinol, ethanol, phenmethylol, 4-hydroxylphenylethyl alcohol, 4 hydroxybutyric acid ethyl ester, ethyl benzoate, ethyl acetate, palmitic acid, malic acid, β-dihydroionone, fumaric acid etc.
3. it can be used as bed material to be sprayed at equably on pipe tobacco, addition is 10g/ case, and not add spiced tobacco leaf for contrast.After the pipe tobacco of processed group and control group is put into climatic chamber inner equilibrium 24h, make cigarette, sample and the equal random number of contrast, the group of smokeing panel test be made up of the expert that smokes panel test carries out sensory evaluating smoking.Perfuming result of the test of smokeing panel test shows, this perfume additive and the comparatively harmony of cigarette perfume (or spice), can improve cigarette quality, cover assorted gas, reduces excitant, soft fine and smooth flue gas, improves comfort level, increases cigarette flavor matter.
Embodiment 3
1. get green plum sample 100g, add the red wine of 5 times, refluxing extraction 2 hours, filters out impurity after having extracted, and namely gained clear liquid obtains the present invention.
2. pair aroma component of the present invention detects, testing result shows, the flavor matter that in this extract, content is higher mainly contains vanillic aldehyde, benzaldehyde, phenylacetaldehyde, 4-methylphenol, isoamyl alcohol, 2-methyl butanol, benzyl carbinol, ethanol, phenmethylol, 4-hydroxylphenylethyl alcohol, 4 hydroxybutyric acid ethyl ester, ethyl benzoate, ethyl acetate, palmitic acid, malic acid, β-dihydroionone, fumaric acid etc.
3. it can be used as bed material to be sprayed at equably on pipe tobacco, addition is 12g/ case, and not add spiced tobacco leaf for contrast.After the pipe tobacco of processed group and control group is put into climatic chamber inner equilibrium 24h, make cigarette, sample and the equal random number of contrast, the group of smokeing panel test be made up of the expert that smokes panel test carries out sensory evaluating smoking.Perfuming result of the test of smokeing panel test shows, this perfume additive and the comparatively harmony of cigarette perfume (or spice), can improve cigarette quality, cover assorted gas, reduces excitant, soft fine and smooth flue gas, improves comfort level, increases cigarette flavor matter.
Embodiment 4
1. get green plum sample 100g, add the red wine of 5 times, refluxing extraction 3 hours, filters out impurity after having extracted, and namely gained clear liquid obtains the present invention.
2. pair aroma component of the present invention detects, testing result shows, the flavor matter that in this extract, content is higher mainly contains vanillic aldehyde, benzaldehyde, phenylacetaldehyde, 4-methylphenol, isoamyl alcohol, 2-methyl butanol, benzyl carbinol, ethanol, phenmethylol, 4-hydroxylphenylethyl alcohol, 4 hydroxybutyric acid ethyl ester, ethyl benzoate, ethyl acetate, palmitic acid, malic acid, β-dihydroionone, fumaric acid etc.
3. it can be used as bed material to be sprayed at equably on pipe tobacco, addition is 15g/ case, and not add spiced tobacco leaf for contrast.After the pipe tobacco of processed group and control group is put into climatic chamber inner equilibrium 24h, make cigarette, sample and the equal random number of contrast, the group of smokeing panel test be made up of the expert that smokes panel test carries out sensory evaluating smoking.Perfuming result of the test of smokeing panel test shows, this perfume additive and the comparatively harmony of cigarette perfume (or spice), can improve cigarette quality, cover assorted gas, reduces excitant, soft fine and smooth flue gas, improves comfort level, increases cigarette flavor matter.
Embodiment 5
1. get green plum sample 100g, add the red wine of 10 times, refluxing extraction 1 hour, filters out impurity after having extracted, and namely gained clear liquid obtains the present invention.
2. pair aroma component of the present invention detects, testing result shows, the flavor matter that in this extract, content is higher mainly contains vanillic aldehyde, benzaldehyde, phenylacetaldehyde, 4-methylphenol, isoamyl alcohol, 2-methyl butanol, benzyl carbinol, ethanol, phenmethylol, 4-hydroxylphenylethyl alcohol, 4 hydroxybutyric acid ethyl ester, ethyl benzoate, ethyl acetate, palmitic acid, malic acid, β-dihydroionone, fumaric acid etc.
3. it can be used as bed material to be sprayed at equably on pipe tobacco, addition is 10g/ case, and not add spiced tobacco leaf for contrast.After the pipe tobacco of processed group and control group is put into climatic chamber inner equilibrium 24h, make cigarette, sample and the equal random number of contrast, the group of smokeing panel test be made up of the expert that smokes panel test carries out sensory evaluating smoking.Perfuming result of the test of smokeing panel test shows, this perfume additive and the comparatively harmony of cigarette perfume (or spice), can improve cigarette quality, cover assorted gas, reduces excitant, soft fine and smooth flue gas, improves comfort level, increases cigarette flavor matter.
Embodiment 6
1. get green plum sample 100g, add the red wine of 10 times, refluxing extraction 2 hours, filters out impurity after having extracted, and namely gained clear liquid obtains the present invention.
2. pair aroma component of the present invention detects, testing result shows, the flavor matter that in this extract, content is higher mainly contains vanillic aldehyde, benzaldehyde, phenylacetaldehyde, 4-methylphenol, isoamyl alcohol, 2-methyl butanol, benzyl carbinol, ethanol, phenmethylol, 4-hydroxylphenylethyl alcohol, 4 hydroxybutyric acid ethyl ester, ethyl benzoate, ethyl acetate, palmitic acid, malic acid, β-dihydroionone, fumaric acid etc.
3. it can be used as bed material to be sprayed at equably on pipe tobacco, addition is 12g/ case, and not add spiced tobacco leaf for contrast.After the pipe tobacco of processed group and control group is put into climatic chamber inner equilibrium 24h, make cigarette, sample and the equal random number of contrast, the group of smokeing panel test be made up of the expert that smokes panel test carries out sensory evaluating smoking.Perfuming result of the test of smokeing panel test shows, this perfume additive and the comparatively harmony of cigarette perfume (or spice), can improve cigarette quality, cover assorted gas, reduces excitant, soft fine and smooth flue gas, improves comfort level, increases cigarette flavor matter.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any amendments done within the spirit and principles in the present invention, equivalent replacement and improvement etc., all should be included within protection scope of the present invention.

Claims (1)

1. the application of green plum spices in cigarette, is characterized in that: cleaned by green plum, weigh after stoning, soak, refluxing extraction 1 ~ 3 hour with the red wine of 5 ~ 10 times amount, and filtration gained clear liquid is required spices; At cigarette primary processing feeding stage, be sprayed at equably on pipe tobacco by described spices, addition is 5 ~ 20g/ case, and is 60% in humidity, and temperature is under 22 DEG C of conditions, constant temperature and humidity balance 24h.
CN201410412799.5A 2014-08-20 2014-08-20 Application of spices made of green plums to cigarettes Pending CN104305511A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104939306A (en) * 2015-07-03 2015-09-30 广西中烟工业有限责任公司 New method for obtaining red date extractive and application in cigarettes
CN104974850A (en) * 2015-06-17 2015-10-14 云南中烟工业有限责任公司 Plum glyceryl triacetate extract and application thereof in cigarettes

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0620982A1 (en) * 1993-04-06 1994-10-26 British-American Tobacco Company Limited Flavouring smoking articles with vanillin glycoside
CN101215805A (en) * 2008-01-07 2008-07-09 红云烟草(集团)有限责任公司 Cigarette perfuming agent and its preparation method and application
CN103549640A (en) * 2013-11-20 2014-02-05 中国烟草总公司郑州烟草研究院 Application of hosta plantaginea flower water extract to cigarettes
CN103695173A (en) * 2012-09-27 2014-04-02 邢娜 Mango flavor tobacco essence
CN103740465A (en) * 2013-12-13 2014-04-23 浙江中烟工业有限责任公司 Waxberry extract used for cigarettes, preparation method thereof and use by being taken as tobacco additive
CN103865645A (en) * 2012-12-11 2014-06-18 爱普香料集团股份有限公司 Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming
CN103952236A (en) * 2014-05-22 2014-07-30 嘉兴市得百科新材料科技有限公司 Perfume composition for fenugreek tobacco and preparation method thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0620982A1 (en) * 1993-04-06 1994-10-26 British-American Tobacco Company Limited Flavouring smoking articles with vanillin glycoside
CN101215805A (en) * 2008-01-07 2008-07-09 红云烟草(集团)有限责任公司 Cigarette perfuming agent and its preparation method and application
CN103695173A (en) * 2012-09-27 2014-04-02 邢娜 Mango flavor tobacco essence
CN103865645A (en) * 2012-12-11 2014-06-18 爱普香料集团股份有限公司 Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming
CN103549640A (en) * 2013-11-20 2014-02-05 中国烟草总公司郑州烟草研究院 Application of hosta plantaginea flower water extract to cigarettes
CN103740465A (en) * 2013-12-13 2014-04-23 浙江中烟工业有限责任公司 Waxberry extract used for cigarettes, preparation method thereof and use by being taken as tobacco additive
CN103952236A (en) * 2014-05-22 2014-07-30 嘉兴市得百科新材料科技有限公司 Perfume composition for fenugreek tobacco and preparation method thereof

Non-Patent Citations (1)

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Title
于建军: "《卷烟工艺学》", 31 July 2003, 中国农业出版社 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104974850A (en) * 2015-06-17 2015-10-14 云南中烟工业有限责任公司 Plum glyceryl triacetate extract and application thereof in cigarettes
CN104939306A (en) * 2015-07-03 2015-09-30 广西中烟工业有限责任公司 New method for obtaining red date extractive and application in cigarettes

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Application publication date: 20150128