CN104294399A - Down feather composite fibers with jasmine fragrance and preparation method thereof - Google Patents
Down feather composite fibers with jasmine fragrance and preparation method thereof Download PDFInfo
- Publication number
- CN104294399A CN104294399A CN201410454658.XA CN201410454658A CN104294399A CN 104294399 A CN104294399 A CN 104294399A CN 201410454658 A CN201410454658 A CN 201410454658A CN 104294399 A CN104294399 A CN 104294399A
- Authority
- CN
- China
- Prior art keywords
- parts
- jasmine
- add
- hour
- butyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Cosmetics (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Artificial Filaments (AREA)
Abstract
The invention discloses down feather composite fibers with a jasmine fragrance, and is characterized in that the down feather composite fibers comprise the following raw materials in parts by weight: 13-16 parts of goose down, 16-21 parts of ox hair, 8-10 parts of glass fibers, 5-8 parts of polynosic, 3-6 parts of conductive fibers, 3-6 parts of jasmine, 1-3 parts of fructus toosendan, 2-4 parts of radix paeoniae rubra, 6-9 parts of mineral wool fibers, 18-22 parts of tobacco straws, 1.2-3.1 parts of triethyl acetyl citrate, 2.1-3.2 parts of propyl acetate, 0.2-0.5 parts of triethyl citrate, 0.6-1.4 parts of a nano pearl powder, 100-110 parts of 1-butyl-3-methylimidazolium acetate, 110-130 parts of 1-butyl-3-methylimidazolium dibutyl phosphate, 3-5 parts of an auxiliary agent, and a proper amount of water. With addition of jasmine, fructus toosendan, radix paeoniae rubra and other components, the down feather composite fibers not only have the jasmine fragrance, but also can effectively remove dirt on the feather composite fibers, and have better conditioning and nursing effects on down feather; and the prepared down feather composite fibers have the advantages of static electricity resistance, large elasticity, good filling power, bacteria resistance, bacteriostasis, wash durability and the like.
Description
Technical field
The present invention relates to nonwoven material technical field, be specifically related to a kind of eider down composite fibre with jasmine aroma and preparation method thereof.
Background technology
Eider down is the long belly goose, duck, becomes the fine hair of a reed catkins shape, slabbing be feather.Because eider down is a kind of animal protein fiber, higher than cotton (vegetative fiber element) heat insulating ability, and ten million leg-of-mutton tiny pore that eider down nodular fibrous gathers, can the convergent-divergent with temperature Change, produce temperature adjustment function, Absorbable rod human body distributes the hot gas of flowing, the invasion of isolated cool ambient air, because eider down has the superperformance that the softly warming of this uniqueness and moisture absorption disperse, determine the health care that eider down is good, eiderdown quilt be widely used in clothes, wadded a quilt with cotton, the fields such as filler of weaving.
Natural down is used to there is many defects in prior art: one, because eider down content in feather is little, usually only to account for 20-25%, thus make the use cost of eider down too high; Two, eider down makes moist because of the humidity of environment, preserves the improper raw mite that easily goes mouldy; Three, intensity is poor, can make eider down pulverizing, conglomeration, reduce warmth retention property, affect attractive in appearance more than washed; Four, the frequent static electrification of eider down in prior art, brings inconvenience; Five, existing eider down does not have the characteristics such as fire-retardant, antibacterial, water-fastness, there is the hidden danger such as safety, so develop a kind of existing environmental protection, health care, the warmth retention property being conducive to again the health of people is strong, high strength, fire-retardant, antibacterial, laundry-resistant eider down composite fibre can solve the deficiencies in the prior art smoothly.
Summary of the invention
Object of the present invention is just to provide a kind of eider down composite fibre with jasmine aroma and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of eider down composite fibre with jasmine aroma, it is characterized in that, be made up of the raw material of following weight portion: goose down 13-16, ox hair 16-21, glass fibre 8-10, polynosic 5-8, conductive fiber 3-6, Jasmine 3-6, Fructus meliae toosendan 1-3, radix paeoniae rubrathe 2-4, mineral wool fiber 6-9, tabacco straw 18-22, acetyl triethyl citrate 1.2-3.1, propyl acetate 2.1-3.2, triethyl citrate 0.2-0.5, Nano pearl powder 0.6-1.4, 1-butyl-3-N-Methylimidazoleacetic salt 100-110, 1-butyl-3-methylimidazole dibutylphosphoric acid ester 110-130, auxiliary agent 3-5, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: polymer dispersion powder 1-2, even bubble silicone oil 3-4, Benzotriazole Ultraviolet Stabilizer 0.03-0.05, polyvinylpyrrolidone 0.2-0.4, trihydroxy ethylamine oleate soap 1.2-3.4, kuh-seng 1-3, erythrina bark 2-4, camphor 0.1-0.3, water 100, its preparation method is by kuh-seng, erythrina bark, camphor boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, in filtrate, add other residual componentss be heated to 45-55 DEG C of agitation grinding 20-30 minute, to obtain final product.
The preparation method of described a kind of eider down composite fibre with jasmine aroma, is characterized in that comprising the following steps:
(1) by Jasmine, Fructus meliae toosendan, radix paeoniae rubrathe boiling 1-2 hour, add tabacco straw and soak 8-10 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, then add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality, filter, with clear water washing to clean, dry and add Nano pearl powder grinding 30-40 minute;
(2) goose down, ox hair, chicken feather are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray into vaporific triethyl citrate;
(3) take 1-butyl-3-N-Methylimidazoleacetic salt, 1-butyl-3-methylimidazole dibutylphosphoric acid ester drops in reactor and stirs and evenly mixs, add step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The present invention has following beneficial effect: the present invention adds the compositions such as Jasmine, Fructus meliae toosendan, the radix paeoniae rubrathe, the fragrance not only with Jasmine effectively can also remove the dirt on eider down composite fibre, have good conditioning, nursing role to eider down, obtained eider down composite fibre have antistatic, elasticity is large, bulking intensity good, antibacterial bacteriostatic, the advantage such as water-fastness.
Detailed description of the invention
Described a kind of eider down composite fibre with jasmine aroma, it is characterized in that, be made up of the raw material of following weight portion: goose down 15, ox hair 17, glass fibre 8, polynosic 5, conductive fiber 3, Jasmine 4, Fructus meliae toosendan 1, the radix paeoniae rubrathe 4, mineral wool fiber 6, tabacco straw 22, acetyl triethyl citrate 1.2, propyl acetate 2.6, triethyl citrate 0.2, Nano pearl powder 0.6,1-butyl-3-N-Methylimidazoleacetic salt 100,1-butyl-3-methylimidazole dibutylphosphoric acid ester 110, auxiliary agent 3, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: polymer dispersion powder 1, even bubble silicone oil 3, Benzotriazole Ultraviolet Stabilizer 0.04, polyvinylpyrrolidone 0.2, trihydroxy ethylamine oleate soap 1.7, kuh-seng 1, erythrina bark 2, camphor 0.1, water 100, its preparation method is by kuh-seng, erythrina bark, camphor boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, in filtrate, add other residual componentss be heated to 45-55 DEG C of agitation grinding 20-30 minute, to obtain final product.
Preparation method comprises the following steps:
(1) by Jasmine, Fructus meliae toosendan, radix paeoniae rubrathe boiling 1-2 hour, add tabacco straw and soak 8-10 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, then add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality, filter, with clear water washing to clean, dry and add Nano pearl powder grinding 30-40 minute;
(2) goose down, ox hair, chicken feather are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray into vaporific triethyl citrate;
(3) take 1-butyl-3-N-Methylimidazoleacetic salt, 1-butyl-3-methylimidazole dibutylphosphoric acid ester drops in reactor and stirs and evenly mixs, add step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
The technical parameter index of the eider down composite fibre using the present invention to produce is as follows:
(1) light weight, warming, environmental protection;
(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 99.9%;
(3) water-fastness, flame retardant effect is excellent.
Claims (2)
1. the eider down composite fibre with jasmine aroma, it is characterized in that, be made up of the raw material of following weight portion: goose down 13-16, ox hair 16-21, glass fibre 8-10, polynosic 5-8, conductive fiber 3-6, Jasmine 3-6, Fructus meliae toosendan 1-3, radix paeoniae rubrathe 2-4, mineral wool fiber 6-9, tabacco straw 18-22, acetyl triethyl citrate 1.2-3.1, propyl acetate 2.1-3.2, triethyl citrate 0.2-0.5, Nano pearl powder 0.6-1.4, 1-butyl-3-N-Methylimidazoleacetic salt 100-110, 1-butyl-3-methylimidazole dibutylphosphoric acid ester 110-130, auxiliary agent 3-5, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: polymer dispersion powder 1-2, even bubble silicone oil 3-4, Benzotriazole Ultraviolet Stabilizer 0.03-0.05, polyvinylpyrrolidone 0.2-0.4, trihydroxy ethylamine oleate soap 1.2-3.4, kuh-seng 1-3, erythrina bark 2-4, camphor 0.1-0.3, water 100, its preparation method is by kuh-seng, erythrina bark, camphor boiling 3-5 hour obtained the concentrated liquid of tradition Chinese medicine, filter, in filtrate, add other residual componentss be heated to 45-55 DEG C of agitation grinding 20-30 minute, to obtain final product.
2. the preparation method of a kind of eider down composite fibre with jasmine aroma according to claim 1, is characterized in that comprising the following steps:
(1) by Jasmine, Fructus meliae toosendan, radix paeoniae rubrathe boiling 1-2 hour, add tabacco straw and soak 8-10 hour, filter, get filter residue and dry pulverizing, add 10% sulfuric acid heating stirring reaction 1-2 hour of filter residue powder 20 times of quality in mass ratio, then add the NaOH heating stirring reaction 1-2 hour of filter residue powder 2 times of quality, filter, with clear water washing to clean, dry and add Nano pearl powder grinding 30-40 minute;
(2) goose down, ox hair, chicken feather are dropped in above-mentioned filtrate and soak 10-13 hour, after pulling oven dry, degreasing, ultra-fine grinding out, spray into vaporific triethyl citrate;
(3) take 1-butyl-3-N-Methylimidazoleacetic salt, 1-butyl-3-methylimidazole dibutylphosphoric acid ester drops in reactor and stirs and evenly mixs, add step (1), (2) product grinding 20-40 minute, be heated to 100-120 DEG C, add other residual components stirring reaction 50-70 minute, obtained spinning solution;
(4) finally obtained spinning solution carried out spinning, winding, boundling, stretching and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410454658.XA CN104294399A (en) | 2014-09-09 | 2014-09-09 | Down feather composite fibers with jasmine fragrance and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410454658.XA CN104294399A (en) | 2014-09-09 | 2014-09-09 | Down feather composite fibers with jasmine fragrance and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104294399A true CN104294399A (en) | 2015-01-21 |
Family
ID=52314340
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410454658.XA Pending CN104294399A (en) | 2014-09-09 | 2014-09-09 | Down feather composite fibers with jasmine fragrance and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104294399A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104831413A (en) * | 2015-03-30 | 2015-08-12 | 安徽省三森纺织有限公司 | Camellia nitidissima down feather composite fiber and producing method thereof |
| CN105821517A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Multilayer composite setting down feather composite fibers and manufacture method thereof |
| CN105821516A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Anti-static down feather composite fibers compounded by nanometer goose down powder/ultrafine chicken feather powder and manufacture method thereof |
| CN105862163A (en) * | 2016-04-28 | 2016-08-17 | 陈后前 | Cotton straw/bamboo fiber compounded down feather composite fibers and manufacturing method thereof |
| CN106929932A (en) * | 2017-03-22 | 2017-07-07 | 安徽三祥羽毛股份有限公司 | Anti-static down composite fibre is used in a kind of down products processing |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20030051112A (en) * | 2001-12-18 | 2003-06-25 | 최명부 | The Manufacture Metal to Shide Cotten |
| CN101536852A (en) * | 2009-04-23 | 2009-09-23 | 江苏丝乡丝绸股份有限公司 | Method for producing cocoon fiber quilt for dermatitis prevention |
| CN102433654A (en) * | 2011-09-30 | 2012-05-02 | 江苏月龙服饰有限公司 | Perfumed down jacket fabric preparation method |
| CN102440448A (en) * | 2011-09-30 | 2012-05-09 | 江苏月龙服饰有限公司 | Fragrant down jacket |
| CN102561046A (en) * | 2011-12-23 | 2012-07-11 | 浙江阿思家居室用品有限公司 | Method for manufacturing fragrance down |
| CN103055534A (en) * | 2012-12-20 | 2013-04-24 | 华南理工大学 | Method of extracting of essential oil in Chinese medicinal herb and cellulose comprehensive utilization |
| CN103710775A (en) * | 2013-12-18 | 2014-04-09 | 中国科学院过程工程研究所 | Preparation method of ionic liquid keratin spinning solutions |
-
2014
- 2014-09-09 CN CN201410454658.XA patent/CN104294399A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20030051112A (en) * | 2001-12-18 | 2003-06-25 | 최명부 | The Manufacture Metal to Shide Cotten |
| CN101536852A (en) * | 2009-04-23 | 2009-09-23 | 江苏丝乡丝绸股份有限公司 | Method for producing cocoon fiber quilt for dermatitis prevention |
| CN102433654A (en) * | 2011-09-30 | 2012-05-02 | 江苏月龙服饰有限公司 | Perfumed down jacket fabric preparation method |
| CN102440448A (en) * | 2011-09-30 | 2012-05-09 | 江苏月龙服饰有限公司 | Fragrant down jacket |
| CN102561046A (en) * | 2011-12-23 | 2012-07-11 | 浙江阿思家居室用品有限公司 | Method for manufacturing fragrance down |
| CN103055534A (en) * | 2012-12-20 | 2013-04-24 | 华南理工大学 | Method of extracting of essential oil in Chinese medicinal herb and cellulose comprehensive utilization |
| CN103710775A (en) * | 2013-12-18 | 2014-04-09 | 中国科学院过程工程研究所 | Preparation method of ionic liquid keratin spinning solutions |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104831413A (en) * | 2015-03-30 | 2015-08-12 | 安徽省三森纺织有限公司 | Camellia nitidissima down feather composite fiber and producing method thereof |
| CN105821517A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Multilayer composite setting down feather composite fibers and manufacture method thereof |
| CN105821516A (en) * | 2016-04-28 | 2016-08-03 | 安徽华强羽绒有限公司 | Anti-static down feather composite fibers compounded by nanometer goose down powder/ultrafine chicken feather powder and manufacture method thereof |
| CN105862163A (en) * | 2016-04-28 | 2016-08-17 | 陈后前 | Cotton straw/bamboo fiber compounded down feather composite fibers and manufacturing method thereof |
| CN106929932A (en) * | 2017-03-22 | 2017-07-07 | 安徽三祥羽毛股份有限公司 | Anti-static down composite fibre is used in a kind of down products processing |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104264276A (en) | Mildew-proof down feather composite fiber and preparation method thereof | |
| CN104762691A (en) | Antimicrobial deodorizing down composite fiber and manufacturing method thereof | |
| CN104762692A (en) | Moisture-absorbing thermal-insulation down composite fiber and manufacturing method thereof | |
| CN104195665B (en) | Eider down composite fibre that a kind of waste and old down fiber/acrylic staple fibre is compound and preparation method thereof | |
| CN104264277A (en) | Mothproof down feather composite fiber and preparation method thereof | |
| CN104294399A (en) | Down feather composite fibers with jasmine fragrance and preparation method thereof | |
| CN104213247A (en) | Water-washable silk composite fiber and preparation method thereof | |
| CN104195664A (en) | Down feather composite fiber modified by polypropylene fiber and preparation method of down feather composite fiber | |
| CN104264275A (en) | Waterproof down feather composite fiber and preparation method thereof | |
| CN104233509A (en) | Down feather composite fibers with anion polyester staple fibers and production method thereof | |
| CN104233505A (en) | Antibacterial and mothproof silk composite fibers and manufacturing method thereof | |
| CN104831407A (en) | Compound warm down feather composite fiber and producing method thereof | |
| CN103668999A (en) | Production method of aromatic home textile fabric | |
| CN103276530B (en) | Feather cotton that fire-retardant eider down, feather fiber combine and preparation method thereof | |
| CN104762694A (en) | Bactericidal mildewproof down composite fibers and manufacturing method thereof | |
| CN104213245A (en) | Long-acting slow-release fragrant silk composite fiber and preparation method thereof | |
| CN104762693A (en) | Regenerated down composite fiber and manufacturing method thereof | |
| CN104831411A (en) | Multifunctional mothproof down feather composite fiber and producing method thereof | |
| CN104233508A (en) | Puffed silk composite fibers with high elasticity and manufacturing method thereof | |
| CN104790063A (en) | Odor-removing down feather composite fiber and preparation method thereof | |
| CN104894865A (en) | Deodorant and breathable feather-down composite heat-insulating material and making method thereof | |
| CN104278355A (en) | Washable light down feather composite fiber and preparation method thereof | |
| CN104357933A (en) | Ultraviolet-proof cotton fiber and preparation method thereof | |
| CN104233506A (en) | Silk composite fibers applicable to allergic constitution and manufacturing method thereof | |
| CN106835676A (en) | A kind of fabric being made by macromolecular material |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150121 |
|
| RJ01 | Rejection of invention patent application after publication |