CN104288076A - Tablet for honey facial mask - Google Patents

Tablet for honey facial mask Download PDF

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Publication number
CN104288076A
CN104288076A CN201410503937.0A CN201410503937A CN104288076A CN 104288076 A CN104288076 A CN 104288076A CN 201410503937 A CN201410503937 A CN 201410503937A CN 104288076 A CN104288076 A CN 104288076A
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Prior art keywords
tabletting
honey
facial mask
folium nelumbinis
concentrated solution
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CN201410503937.0A
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CN104288076B (en
Inventor
赵上生
冯尔玺
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NANJING CHANGLI BEES PRODUCT Co Ltd
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NANJING CHANGLI BEES PRODUCT Co Ltd
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  • Jellies, Jams, And Syrups (AREA)
  • Medicinal Preparation (AREA)

Abstract

The invention relates to a tablet for a honey facial mask. The tablet is prepared by pressing the following raw materials: 20-25wt% of dried honey powder, 10-15wt% of a lotus leaf extracting concentrated solution, 1.0-1.2wt% of 2-hydroxysuccinic acid, 0.8-1.0wt% of potassium sorbate, 3-5wt% of cross-linked sodium carboxymethylcellulose, 5-10wt% of microcrystalline cellulose, 8-10wt% of carboxymethyl chitosan and the balance of carrageenan. The tablet for the honey facial mask disclosed by the invention is not only high in forming rate and easy to store, but also easy to dissolve and good in film forming performance; in addition, by virtue of a synergistic effect among the dried honey powder, the lotus leaf extracting concentrated solution and the 2-hydroxysuccinic acid, the tablet can better develop effects of resisting free radical and removing freckles.

Description

Honey facial mask tabletting
Technical field
The present invention relates to the technical field of cosmetics, more particularly, the present invention relates to a kind of honey facial mask tabletting.
Background technology
Mel is as natural health-care nutritional food and the product with multiple industrial use, it is a kind of saccharide saturated solution with the complexity of biological nature, containing compositions such as rich in protein, enzyme, aminoacid, vitamin, organic acid, trace element, hormones, be widely used in all many-sides such as medical science pharmacology, clinical treatment, health care of food, looks improving and the skin nourishing, be with a wide range of applications.
Because Mel has stronger moist property, the moisture in air can be absorbed, can prevent epidermal surface moisture from evaporating preferably and scatter and disappear; The nutritional labeling of Mel is natural nutrient substance, and the bioactive substances such as its monosaccharide, vitamin, enzyme are conducive to by the absorption of Skin Cell, effectively can improve the nutritional status of skin surface; Containing multiple acid in Mel, these materials have stronger bactericidal action, and the effects such as it is moist in addition, nutrition, can effectively remove or alleviate face's pimples, acne, help and eliminate black speck and some other facial speckle.Therefore Mel can be made honey facial mask to be used for carrying out moisturizing, whitening or speckle dispelling to facial skin as main material.But in the prior art, honey facial mask is all based on natural Mel, is made by adding other helper component such as component DIY such as milk, Ovum Gallus domesticus album, not only needs field fabrication, and being difficult to permanent preservation, there is obvious defect.
Summary of the invention
In order to solve above-mentioned technical problem of the prior art, the object of the present invention is to provide a kind of honey facial mask tabletting.
To achieve these goals, the present invention is by the following technical solutions:
A kind of honey facial mask tabletting, it is characterized in that: described tabletting is suppressed by following raw material and formed: the honey powder of 20 ~ 25wt%, the Folium Nelumbinis of 10 ~ 15wt% extracts concentrated solution, the 2-hydroxyl succinic acid of 1.0 ~ 1.2wt%, the potassium sorbate of 0.8 ~ 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 3 ~ 5wt%, the microcrystalline Cellulose of 5 ~ 10wt%, the carboxymethyl chitosan of 8 ~ 10wt%, and the carrageenan of surplus.
Wherein, described honey powder is prepared by following technique:
(1) vacuum lyophilization: Mel freezer dryer carried out precooling and freezingly obtain solids; Wherein, the time of precooling is 2 ~ 3 hours, and temperature is-30 ~-40 DEG C; The freezing time is 10 ~ 12 hours, and temperature is-25 ~-30 DEG C, and vacuum is below 1000Pa;
(2) pulverize at low temperature, solids step (1) obtained carries out pulverizing and obtaining the honey powder that particle diameter is less than 50 μm under the condition of-15 ~-20 DEG C.
Wherein, described Folium Nelumbinis is extracted concentrated solution and is prepared by following technique: the dry Folium Nelumbinis of pulverizing is placed in the water boiled and soaks 30 ~ 60 minutes, after removing slag, filtrate is concentrated 2.0 ~ 2.5 hours under the vacuum condition of 0.01 ~ 0.05MPa, obtain described Folium Nelumbinis and extract concentrated solution; Wherein, the mass ratio of dry Folium Nelumbinis and water is 1: 10.
Wherein, tabletting is prepared by the technique comprised the following steps:
(1) according to required mass percent, get Folium Nelumbinis and extract concentrated solution, add honey powder wherein, 2-hydroxyl succinic acid, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously;
(2) at the temperature of 50 ~ 70 DEG C, drying and processing is carried out 15 ~ 20 minutes, pulverize, cross 20 mesh sieves, then add microcrystalline Cellulose and carboxymethyl chitosan and mix homogeneously, be then cooled to-5 ~-15 DEG C, be carry out tabletting under the condition of 20 ~ 60KN at pressure.
Wherein, described technique also comprises step (3), and described step (3) refers to and refers to utilize wavelength to be that the ultraviolet of 100 ~ 120nm irradiates, and irradiation dose is 0.5 ~ 1.0mWcm -2.
Compared with prior art, honey facial mask tabletting of the present invention has following beneficial effect:
Not only ratio of briquetting is high for honey facial mask tabletting of the present invention, easily stores, and soluble, good film-forming property; In addition, extracted the synergism of concentrated solution and 2-hydroxyl succinic acid by honey powder, Folium Nelumbinis, better can play the effect of free radical resisting and speckle dispelling.
Detailed description of the invention
Below with reference to specific embodiment, honey facial mask tabletting of the present invention and preparation method thereof is further elaborated, has more complete, accurate and deep understanding to help those skilled in the art to inventive concept of the present invention, technical scheme.
the preparation of honey powder
The honey powder of embodiments of the invention and comparative example is prepared by following technique:
(1) vacuum lyophilization: Mel freezer dryer carried out precooling and freezingly obtain solids; Wherein, the time of precooling is 2 hours, and temperature is-35 DEG C; The freezing time is 10 hours, and temperature is-25 DEG C, and vacuum is below 1000Pa; (2) pulverize at low temperature, solids step (1) obtained carries out pulverizing and obtains the honey powder that particle diameter is less than 50 μm under the condition of-20 DEG C.
folium Nelumbinis extracts the preparation of concentrated solution
The Folium Nelumbinis of embodiments of the invention and comparative example is extracted concentrated solution and is prepared by following technique: the dry Folium Nelumbinis of pulverizing is placed in the water boiled and soaks 60 minutes, after removing slag, filtrate is concentrated 2.5 hours under the vacuum condition of 0.05MPa, obtain described Folium Nelumbinis and extract concentrated solution; Wherein, the mass ratio of dry Folium Nelumbinis and water is 1: 10.
Embodiment 1
The honey facial mask tabletting of the present embodiment, its raw material comprises: the honey powder of 20wt%, the Folium Nelumbinis of 10wt% extracts concentrated solution, the 2-hydroxyl succinic acid of 1.0wt%, the potassium sorbate of 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 3.0wt%, the microcrystalline Cellulose of 8wt%, the carboxymethyl chitosan of 10wt%, and the carrageenan of surplus; And described tabletting is prepared by following processing step: (1), according to required mass percent, is got Folium Nelumbinis and extracted concentrated solution, add honey powder wherein, 2-hydroxyl succinic acid, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously; (2) at the temperature of 60 DEG C, drying and processing is carried out 20 minutes, pulverize, cross 20 mesh sieves, then add product cellulose and carboxymethyl chitosan mix homogeneously in a subtle way, then be cooled to-10 DEG C, be carry out tabletting under the condition of 25KN at pressure, the weight of tabletting is 1.5 grams; (3) utilize the ultraviolet that wavelength is 100nm to irradiate, and irradiation dose is 0.5mWcm -2.
Embodiment 2
The honey facial mask tabletting of the present embodiment, its raw material comprises: the honey powder of 25wt%, the Folium Nelumbinis of 15wt% extracts concentrated solution, the 2-hydroxyl succinic acid of 1.2wt%, the potassium sorbate of 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 5wt%, the microcrystalline Cellulose of 10wt%, the carboxymethyl chitosan of 10wt%, and the carrageenan of surplus; And described tabletting is prepared by following processing step: (1), according to required mass percent, is got Folium Nelumbinis and extracted concentrated solution, add honey powder wherein, 2-hydroxyl succinic acid, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously; (2) at the temperature of 60 DEG C, drying and processing is carried out 20 minutes, pulverize, cross 20 mesh sieves, then add microcrystalline Cellulose and carboxymethyl chitosan and mix homogeneously, then be cooled to-10 DEG C, be carry out tabletting under the condition of 25KN at pressure, the weight of tabletting is 1.5 grams; (3) utilize the ultraviolet that wavelength is 100nm to irradiate, and irradiation dose is 0.5mWcm -2.
Comparative example 1
The honey facial mask tabletting of this comparative example, its raw material comprises: the honey powder of 25wt%, the 2-hydroxyl succinic acid of 1.2wt%, the potassium sorbate of 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 5wt%, the microcrystalline Cellulose of 10wt%, the carboxymethyl chitosan of 10wt%, and the carrageenan of surplus; And described tabletting is prepared by following processing step: according to required mass percent, by honey powder, 2-hydroxyl succinic acid, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously; At the temperature of 60 DEG C, carry out drying and processing 20 minutes, pulverize, cross 20 mesh sieves, then add microcrystalline Cellulose and carboxymethyl chitosan and mix homogeneously, be then cooled to-10 DEG C, be carry out tabletting under the condition of 25KN at pressure, the weight of tabletting is 1.5 grams; (3) utilize the ultraviolet that wavelength is 100nm to irradiate, and irradiation dose is 0.5mWcm -2.
Comparative example 2
The honey facial mask tabletting of this comparative example, its raw material comprises: the honey powder of 25wt%, and the Folium Nelumbinis of 15wt% extracts concentrated solution, the potassium sorbate of 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 5wt%, the microcrystalline Cellulose of 10wt%, the carboxymethyl chitosan of 10wt%, and the carrageenan of surplus; And described tabletting is prepared by following processing step: (1), according to required mass percent, is got Folium Nelumbinis and extracted concentrated solution, add honey powder wherein, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously; (2) at the temperature of 60 DEG C, drying and processing is carried out 20 minutes, pulverize, cross 20 mesh sieves, then add microcrystalline Cellulose and carboxymethyl chitosan and mix homogeneously, then be cooled to-10 DEG C, be carry out tabletting under the condition of 25KN at pressure, the weight of tabletting is 1.5 grams; (3) utilize the ultraviolet that wavelength is 100nm to irradiate, and irradiation dose is 0.5mWcm -2.
Comparative example 3
The honey facial mask tabletting of this comparative example, its raw material comprises: the honey powder of 25wt%, the potassium sorbate of 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 5wt%, the microcrystalline Cellulose of 10wt%, the carboxymethyl chitosan of 10wt%, and the carrageenan of surplus; And described tabletting is prepared by following processing step: according to required mass percent, by honey powder, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously; At the temperature of 60 DEG C, carry out drying and processing 20 minutes, pulverize, cross 20 mesh sieves, then add microcrystalline Cellulose and carboxymethyl chitosan and mix homogeneously, be then cooled to-10 DEG C, be carry out tabletting under the condition of 25KN at pressure, the weight of tabletting is 1.5 grams; (3) utilize the ultraviolet that wavelength is 100nm to irradiate, and irradiation dose is 0.5mWcm -2.
Comparative example 4
The honey facial mask tabletting of this comparative example, its raw material comprises: the honey powder of 25wt%, the Folium Nelumbinis of 15wt% extracts concentrated solution, the citric acid of 1.2wt%, the potassium sorbate of 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 5wt%, the microcrystalline Cellulose of 10wt%, the carboxymethyl chitosan of 10wt%, and the carrageenan of surplus; And described tabletting is prepared by following processing step: (1), according to required mass percent, is got Folium Nelumbinis and extracted concentrated solution, add honey powder wherein, citric acid, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously; (2) at the temperature of 60 DEG C, drying and processing is carried out 20 minutes, pulverize, cross 20 mesh sieves, then add microcrystalline Cellulose and carboxymethyl chitosan and mix homogeneously, then be cooled to-10 DEG C, be carry out tabletting under the condition of 25KN at pressure, the weight of tabletting is 1.5 grams; (3) utilize the ultraviolet that wavelength is 100nm to irradiate, and irradiation dose is 0.5mWcm -2.
facial film result of use
Subjects is face with the Asia women crowd of blackhead and/or skin dark stain, and the object on probation of investigation is 750 examples, and the age is 18 ~ 35 years old, each 150 examples of honey facial mask tabletting prepared by each embodiment and comparative example.Age distributing equilibrium in each group, eliminates the impact at age.Using method: adopt above-mentioned composition tablet to utilize facial mask machine to make sheet-type packs (each use tabletting a slice).Clean face, facial film is spread on the face, after 30 minutes, take facial film off, clean, apply once before sleeping every night, use 30 days continuously.Effect assessment standard is as follows: A is effective: skin is fine and smooth, and the color of macroscopic blackhead or skin dark stain is thin out (more than 30% color of the visible number of naked eyes is thin out).B is effective: the color of macroscopic blackhead or skin dark stain is thin out (10 ~ 30% colors of the visible number of naked eyes are thin out).DEG C without positive effect: the color of macroscopic blackhead or skin dark stain has no obviously thin out (less than 10% color of the visible number of naked eyes is thin out).Result of use is as shown in table 1:
Table 1
? Embodiment 1 Embodiment 2 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4
A 20 28 12 10 12 10
B 55 62 50 49 55 53
C 75 60 88 91 83 87
A+B 75 90 62 59 67 63
For the ordinary skill in the art; specific embodiment is just to invention has been exemplary description; obvious specific implementation of the present invention is not subject to the restrictions described above; as long as have employed the improvement of the various unsubstantialities that method of the present invention is conceived and technical scheme is carried out; or design of the present invention and technical scheme directly applied to other occasion, all within protection scope of the present invention without to improve.

Claims (5)

1. a honey facial mask tabletting, it is characterized in that: described tabletting is suppressed by following raw material and formed: the honey powder of 20 ~ 25wt%, the Folium Nelumbinis of 10 ~ 15wt% extracts concentrated solution, the 2-hydroxyl succinic acid of 1.0 ~ 1.2wt%, the potassium sorbate of 0.8 ~ 1.0wt%, the cross-linking sodium carboxymethyl cellulose of 3 ~ 5wt%, the microcrystalline Cellulose of 5 ~ 10wt%, the carboxymethyl chitosan of 8 ~ 10wt%, and the carrageenan of surplus.
2. honey facial mask tabletting according to claim 1, is characterized in that: described honey powder is prepared by following technique:
(1) vacuum lyophilization: Mel freezer dryer carried out precooling and freezingly obtain solids; Wherein, the time of precooling is 2 ~ 3 hours, and temperature is-30 ~-40 DEG C; The freezing time is 10 ~ 12 hours, and temperature is-25 ~-30 DEG C, and vacuum is below 1000Pa;
(2) pulverize at low temperature, solids step (1) obtained carries out pulverizing and obtaining the honey powder that particle diameter is less than 50 μm under the condition of-15 ~-20 DEG C.
3. honey facial mask tabletting according to claim 1, it is characterized in that: described Folium Nelumbinis is extracted concentrated solution and prepared by following technique: the dry Folium Nelumbinis of pulverizing is placed in the water boiled and soaks 30 ~ 60 minutes, after removing slag, filtrate is concentrated 2.0 ~ 2.5 hours under the vacuum condition of 0.01 ~ 0.05MPa, obtain described Folium Nelumbinis and extract concentrated solution; Wherein, the mass ratio of dry Folium Nelumbinis and water is 1: 10.
4. honey facial mask tabletting according to claim 1, is characterized in that: tabletting is prepared by the technique comprised the following steps:
(1) according to required mass percent, get Folium Nelumbinis and extract concentrated solution, add honey powder wherein, 2-hydroxyl succinic acid, potassium sorbate, cross-linking sodium carboxymethyl cellulose and carrageenan, mix homogeneously;
(2) at the temperature of 50 ~ 70 DEG C, drying and processing is carried out 15 ~ 20 minutes, pulverize, cross 20 mesh sieves, then add microcrystalline Cellulose and carboxymethyl chitosan and mix homogeneously, be then cooled to-5 ~-15 DEG C, be carry out tabletting under the condition of 20 ~ 60KN at pressure.
5. honey facial mask tabletting according to claim 4, it is characterized in that: described technique also comprises step (3), described step (3) refers to and refers to utilize wavelength to be that the ultraviolet of 100 ~ 120nm irradiates, and irradiation dose is 0.5 ~ 1.0mWcm -2.
CN201410503937.0A 2014-09-28 2014-09-28 Honey facial mask tabletting Active CN104288076B (en)

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2180837C1 (en) * 2001-03-27 2002-03-27 Сафонова Элианна Султановна Cosmetic cream-mask to take care of face and neck skin
CN101744758A (en) * 2008-12-12 2010-06-23 沈阳市和平区高新技术企业创业服务中心 Honey facial mask with moisturizing factor
CN103479559A (en) * 2013-09-12 2014-01-01 严洁 Skin compacting mask

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2180837C1 (en) * 2001-03-27 2002-03-27 Сафонова Элианна Султановна Cosmetic cream-mask to take care of face and neck skin
CN101744758A (en) * 2008-12-12 2010-06-23 沈阳市和平区高新技术企业创业服务中心 Honey facial mask with moisturizing factor
CN103479559A (en) * 2013-09-12 2014-01-01 严洁 Skin compacting mask

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Denomination of invention: Mask for honey mask

Effective date of registration: 20210125

Granted publication date: 20170922

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