CN104277666A - Root-blocking type epoxy amino waterproof paint and preparation method thereof - Google Patents

Root-blocking type epoxy amino waterproof paint and preparation method thereof Download PDF

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Publication number
CN104277666A
CN104277666A CN201410590391.7A CN201410590391A CN104277666A CN 104277666 A CN104277666 A CN 104277666A CN 201410590391 A CN201410590391 A CN 201410590391A CN 104277666 A CN104277666 A CN 104277666A
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China
Prior art keywords
parts
root
powder
type epoxy
waterproof paint
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CN201410590391.7A
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Chinese (zh)
Inventor
朱厚信
张军
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ANHUI LANGKAIQI BUILDING MATERIALS Co Ltd
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ANHUI LANGKAIQI BUILDING MATERIALS Co Ltd
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Priority to CN201410590391.7A priority Critical patent/CN104277666A/en
Publication of CN104277666A publication Critical patent/CN104277666A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses root-blocking type epoxy amino waterproof paint. The root-blocking type epoxy amino waterproof paint is characterized by being prepared from the following raw materials in parts by weight: 0.4-0.6 part of defoaming agent BYK-392, 0.2-0.4 part of dispersing agent BYK-333, 55-65 parts of epoxy resin, 2-3 parts of wax powder, 1-3 parts of triethylamine, 3-5 parts of melamine urea-formaldehyde resin, 3-5 parts of methylated melamine resin, 1-2 parts of fumed silica, 2-3 parts of shellac, 4-6 parts of anatase titanium powder, 5-6 parts of calcium carbonate, 4-5 parts of carbon black, 0.7-1.4 parts of adhesion promoter, 6-8 parts of S-100, 3-5 parts of cyclohexanone, 10-13 parts of butyl acetate, 1-2 parts of metolachlor and 5-7 parts of root-blocking auxiliary. The root-blocking type epoxy amino waterproof paint has the advantages that adhesion of priming paint is good, the root-blocking type epoxy amino waterproof paint is smooth after being smeared, hardness is high, the root-blocking type epoxy amino waterproof paint also has excellent ageing resistance, weather resistance and deformability, and the added metolachlor and root-blocking auxiliary can be used for enhancing a function, namely resistance to puncture of plant root systems, of the root-blocking type epoxy amino waterproof paint and do not influence growth of plants.

Description

A kind of root-resistant type epoxy amino waterproof paint and preparation method thereof
Technical field
The present invention relates to a kind of coating and preparation method thereof, particularly a kind of root-resistant type epoxy amino waterproof paint and preparation method thereof.
Background technology
Along with the fast development of economy and the raising gradually of people's living standard, energy dilemma and ecocrisis more and more severeer, very serious to environmental influence.Along with the raising gradually of people's environmental consciousness; planting technique engineering becomes the main contents of urban construction gradually; and buildings is social maximum comsumption of natural resources person; so people can cover the views such as green vegetation, artificial hillock, pond at positions such as the roof of building or basement roofs usually, build the ecosystem of making us pleasing, beautifying the environment.And green roof is generally made up of planted plant, waterproof stopping area, water draining and accumulating device, heat insulation layer etc., wherein waterproof stopping area is particularly important.Any planting technique engineering all can face the problem of water leakage, because the plant of plantation has flourishing root system, they can penetrate roof construction layer and cause serious percolating water phenomenon, therefore architecture greening planting engineering requires that waterproof paint has good resistance to roots of plants and wears performance, ensures plant normal growth simultaneously.But waterproof paint exist overlap joint loosely have gap, can not topical application and bonding effect difference and go wrong in actual applications, good waterproof root resistance effect can not be reached.The present invention is directed to root resistance auxiliary agent prepared by this situation, add in coating as auxiliary agent, there is production cost low, root system of plant is not almost affected, play the effect of good anti-root system of plant puncture.
Summary of the invention
The object of this invention is to provide a kind of root-resistant type epoxy amino waterproof paint and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of root-resistant type epoxy amino waterproof paint, is made up of the raw material of following weight part: defoamer BYK-3920.4-0.6, dispersant B YK-3330.2-0.4, epoxy resin 55-65, wax powder 2-3, triethylamine 1-3, melamine urea-formaldehyde resin 3-5, methyl-etherified melamine resin 3-5, aerosil 1-2, shellac 2-3, anatase titanium dioxide titanium valve 4-6, calcium carbonate 5-6, carbon black 4-5, adhesion promoter 0.7-1.4, S-1006-8, pimelinketone 3-5, N-BUTYL ACETATE 10-13, metolachlor 1-2, root resistance auxiliary agent 5-7;
Described nanometer root resistance auxiliary agent is made up of the raw material of following weight part: root resistance agent B23-5, petroleum pitch AH-8030-34, petroleum resin 13-16, gum resin 4-6, nano titanium oxide 2-3, turps 12-14, ethyl acetate 6-8, epoxy soybean oil 2-3, copper nanoparticle 5-8, calcined kaolin powder 15-17, calcining calcite in powder 14-16, silicon carbide whisker powder 6-8, sodium lauryl sulphate 1-2, silane coupling agent KH5600.5-1.0, Ethylene glycol dimethacrylate 1-2, dilaurate dibutyl tin 0.4-0.8, preparation method is by silane coupling agent KH560, calcined kaolin powder, calcining calcite in powder, copper nanoparticle and silicon carbide whisker powder mixed grinding be uniformly dispersed formed mixed powder for subsequent use, again petroleum pitch AH-80 is heated to 120-130 ° of C, the solution making 0.5-1.5% that sodium lauryl sulphate is dissolved in water is heated to 60-80 ° of C formation emulsion, emulsion is added in petroleum pitch AH-80 and carries out high shear agitation 30-45 minute, temperature is controlled after 70-90 ° of C, add petroleum resin, gum resin, turps, ethyl acetate and epoxy soybean oil mixing and stirring, meanwhile add root resistance agent B2 again, mixed powder, dilaurate dibutyl tin and Ethylene glycol dimethacrylate stir.
A kind of root-resistant type epoxy amino waterproof paint of the present invention, comprises following concrete steps:
(1) by pimelinketone, S-100, N-BUTYL ACETATE mixing, add calcium carbonate, anatase titanium dioxide titanium valve, carbon black, aerosil ultrasonic disperse 10-20 minute, root resistance auxiliary agent, adhesion promoter, metolachlor and dispersant B YK-333 are added to grinding in sand mill by control temperature when 20-50 ° of C even;
(2) material of step (1) is transferred in the reactor with stirring rake, under 2000-4000 rev/min, add defoamer BYK-392, epoxy resin, shellac, wax powder stirring 1-2 hour;
(3) all the other surplus materialss are mixed, add the material in step (2), stir under 1200-1500 rev/min.
Advantage of the present invention is: paint adhesion of the present invention is strong, smear smooth, hardness is high, also there is excellent ageing-resistant, weathering resistance and deformability, the carbon black that the present invention adds absorbs ultraviolet, and strengthen the ageing-resistant performance of film, the adhesion promoter of interpolation further enhancing the adhesion property of film, the metolachlor added and root resistance auxiliary agent synergy further promote the function of the resistance to root system of plant puncture of coating, and unaffected to the growth of plant.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of root-resistant type epoxy amino waterproof paint, is made up of the raw material of following weight part (kilogram): defoamer BYK-3920.5, dispersant B YK-3330.3, epoxy resin 62, wax powder 2, triethylamine 2, melamine urea-formaldehyde resin 3, methyl-etherified melamine resin 4, aerosil 1, shellac 2, anatase titanium dioxide titanium valve 5, calcium carbonate 5, carbon black 4, adhesion promoter 0.9, S-1007, pimelinketone 4, N-BUTYL ACETATE 11, metolachlor 1, root resistance auxiliary agent 7;
Described nanometer root resistance auxiliary agent is made up of the raw material of following weight part (kilogram): root resistance agent B24, petroleum pitch AH-8033, petroleum resin 14, gum resin 5, nano titanium oxide 3, turps 12, ethyl acetate 7, epoxy soybean oil 3, copper nanoparticle 7, calcined kaolin powder 16, calcining calcite in powder 15, silicon carbide whisker powder 7, sodium lauryl sulphate 1, silane coupling agent KH5600.9, Ethylene glycol dimethacrylate 1, dilaurate dibutyl tin 0.6, preparation method is by silane coupling agent KH560, calcined kaolin powder, calcining calcite in powder, copper nanoparticle and silicon carbide whisker powder mixed grinding be uniformly dispersed formed mixed powder for subsequent use, again petroleum pitch AH-80 is heated to 120-130 ° of C, the solution making 0.5-1.5% that sodium lauryl sulphate is dissolved in water is heated to 60-80 ° of C formation emulsion, emulsion is added in petroleum pitch AH-80 and carries out high shear agitation 30-45 minute, temperature is controlled after 70-90 ° of C, add petroleum resin, gum resin, turps, ethyl acetate and epoxy soybean oil mixing and stirring, meanwhile add root resistance agent B2 again, mixed powder, dilaurate dibutyl tin and Ethylene glycol dimethacrylate stir.
A kind of root-resistant type epoxy amino waterproof paint of the present invention, comprises following concrete steps:
(1) by pimelinketone, S-100, N-BUTYL ACETATE mixing, add calcium carbonate, anatase titanium dioxide titanium valve, carbon black, aerosil ultrasonic disperse 10-20 minute, root resistance auxiliary agent, adhesion promoter, metolachlor and dispersant B YK-333 are added to grinding in sand mill by control temperature when 20-50 ° of C even;
(2) material of step (1) is transferred in the reactor with stirring rake, under 2000-4000 rev/min, add defoamer BYK-392, epoxy resin, shellac, wax powder stirring 1-2 hour;
(3) all the other surplus materialss are mixed, add the material in step (2), stir under 1200-1500 rev/min.
Paint adhesion experiment (cross-hatching) of the present invention: 1 grade, experiment of hardness: 3H, T curved experiment: 2T, resistance to impact shock is tested: 10J, artificial ageing resistance experiment (2000H): film is unchanged, resistance to boiling water experiment (2H): unchanged, root puncture resistant capacity experimental: without penetration phenomenon.

Claims (2)

1. a root-resistant type epoxy amino waterproof paint, it is characterized in that, be made up of the raw material of following weight part: defoamer BYK-3920.4-0.6, dispersant B YK-3330.2-0.4, epoxy resin 55-65, wax powder 2-3, triethylamine 1-3, melamine urea-formaldehyde resin 3-5, methyl-etherified melamine resin 3-5, aerosil 1-2, shellac 2-3, anatase titanium dioxide titanium valve 4-6, calcium carbonate 5-6, carbon black 4-5, adhesion promoter 0.7-1.4, S-1006-8, pimelinketone 3-5, N-BUTYL ACETATE 10-13, metolachlor 1-2, root resistance auxiliary agent 5-7;
Described nanometer root resistance auxiliary agent is made up of the raw material of following weight part: root resistance agent B23-5, petroleum pitch AH-8030-34, petroleum resin 13-16, gum resin 4-6, nano titanium oxide 2-3, turps 12-14, ethyl acetate 6-8, epoxy soybean oil 2-3, copper nanoparticle 5-8, calcined kaolin powder 15-17, calcining calcite in powder 14-16, silicon carbide whisker powder 6-8, sodium lauryl sulphate 1-2, silane coupling agent KH5600.5-1.0, Ethylene glycol dimethacrylate 1-2, dilaurate dibutyl tin 0.4-0.8, preparation method is by silane coupling agent KH560, calcined kaolin powder, calcining calcite in powder, copper nanoparticle and silicon carbide whisker powder mixed grinding be uniformly dispersed formed mixed powder for subsequent use, again petroleum pitch AH-80 is heated to 120-130 ° of C, the solution making 0.5-1.5% that sodium lauryl sulphate is dissolved in water is heated to 60-80 ° of C formation emulsion, emulsion is added in petroleum pitch AH-80 and carries out high shear agitation 30-45 minute, temperature is controlled after 70-90 ° of C, add petroleum resin, gum resin, turps, ethyl acetate and epoxy soybean oil mixing and stirring, meanwhile add root resistance agent B2 again, mixed powder, dilaurate dibutyl tin and Ethylene glycol dimethacrylate stir.
2. a kind of root-resistant type epoxy amino waterproof paint according to claims 1, is characterized in that, comprise following concrete steps:
(1) by pimelinketone, S-100, N-BUTYL ACETATE mixing, add calcium carbonate, anatase titanium dioxide titanium valve, carbon black, aerosil ultrasonic disperse 10-20 minute, root resistance auxiliary agent, adhesion promoter, metolachlor and dispersant B YK-333 are added to grinding in sand mill by control temperature when 20-50 ° of C even;
(2) material of step (1) is transferred in the reactor with stirring rake, under 2000-4000 rev/min, add defoamer BYK-392, epoxy resin, shellac, wax powder stirring 1-2 hour;
(3) all the other surplus materialss are mixed, add the material in step (2), stir under 1200-1500 rev/min.
CN201410590391.7A 2014-10-29 2014-10-29 Root-blocking type epoxy amino waterproof paint and preparation method thereof Pending CN104277666A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108912580A (en) * 2018-07-10 2018-11-30 湖北工业大学 The preparation method of copper nanometer rods enhancing pitch planted roof root resistance material

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1962782A (en) * 2005-11-10 2007-05-16 沈阳蓝光新型防水材料有限公司 Aqueous asphalt-based root-protecting waterproof coating and method for preparing same
CN101935488A (en) * 2010-09-30 2011-01-05 北京立高科技股份有限公司 Plant root resistant waterproof coating and preparation method thereof
CN102850903A (en) * 2012-08-31 2013-01-02 青岛康泰鑫环保科技有限公司 Improved high-efficiency anticorrosive coating
CN102863891A (en) * 2012-09-12 2013-01-09 常熟市三恒建材有限责任公司 Plant-root-piercing-resistant waterproof coating
CN102965020A (en) * 2012-11-30 2013-03-13 山东北方创信防水技术有限公司 Root-resistance spraying rapid-hardening rubber asphalt water-proofing material for planting
CN103275611A (en) * 2013-04-28 2013-09-04 北京立高防水工程有限公司 Environmentally-friendly root-resistant waterproof polyurethane paint and preparation method thereof
CN103468124A (en) * 2013-09-06 2013-12-25 安徽朗凯奇建材有限公司 Waterproof and root-resistant polyurethane coating for planting roof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1962782A (en) * 2005-11-10 2007-05-16 沈阳蓝光新型防水材料有限公司 Aqueous asphalt-based root-protecting waterproof coating and method for preparing same
CN101935488A (en) * 2010-09-30 2011-01-05 北京立高科技股份有限公司 Plant root resistant waterproof coating and preparation method thereof
CN102850903A (en) * 2012-08-31 2013-01-02 青岛康泰鑫环保科技有限公司 Improved high-efficiency anticorrosive coating
CN102863891A (en) * 2012-09-12 2013-01-09 常熟市三恒建材有限责任公司 Plant-root-piercing-resistant waterproof coating
CN102965020A (en) * 2012-11-30 2013-03-13 山东北方创信防水技术有限公司 Root-resistance spraying rapid-hardening rubber asphalt water-proofing material for planting
CN103275611A (en) * 2013-04-28 2013-09-04 北京立高防水工程有限公司 Environmentally-friendly root-resistant waterproof polyurethane paint and preparation method thereof
CN103468124A (en) * 2013-09-06 2013-12-25 安徽朗凯奇建材有限公司 Waterproof and root-resistant polyurethane coating for planting roof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108912580A (en) * 2018-07-10 2018-11-30 湖北工业大学 The preparation method of copper nanometer rods enhancing pitch planted roof root resistance material
CN108912580B (en) * 2018-07-10 2020-10-02 湖北工业大学 Preparation method of copper nanorod reinforced asphalt planting roof root-blocking material

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