It is a kind of to refresh the mind and the compound plant essential oil of repellent antipruritic and preparation method thereof
Technical field
The present invention relates to a kind of plants essential oil, more particularly to it is a kind of refresh the mind and the compound plant essential oil of repellent antipruritic and
Its preparation method.
Background technology
Modern life rhythm is fast, and work and study pressure is big, especially business people, white collar and student, often feels tired
It is exhausted, have one's head in the clouds.Some people easily feel sleepy in spring, torridity summer, autumn, particularly human pilot, with greater need for tired tired
Refreshed the mind when tired, avoid danger.At present on the market for the main externally applied product of this market demand be essential wind oil, white flower oil,
The medicines such as cooling ointment, although can play a role, mostly containing chemical synthesis, securities such as gaultherolin, camphors
Relatively low composition, smell are pungent, and mostly low side consumer products, it is difficult to meet that middle and high end crowd pursues natural, safe psychology.
A kind of compound essential oil to refresh the mind of the disclosure of the invention of application number 200710303708.4, it is mainly by rosemary
Essential oil, clove oil, oil of Cymbopogon winterianus, tea tree ethereal oil, Peppermint essential oil, Patchouli essential oil are mixed according to certain ratio.Should
Though compound essential oil can refresh the mind without repellent antipruritic function, and the compound essential oil using when be easy and fast to volatilize, lead
Cause a large amount of wastes of active ingredient.
The content of the invention
Refresh the mind and the compound plant essential oil of repellent antipruritic, have refrigerant, happy it is an object of the invention to provide a kind of
The fragrance of people, safety is gentle, can refresh the mind, quick repellent antipruritic, for non-defective unit of aestivating.
Refreshed the mind and the preparation method of the compound plant essential oil of repellent antipruritic present invention also offers a kind of, it is simple easily
OK, it is adapted to industrialized production.
The technical solution adopted for the present invention to solve the technical problems is:
It is a kind of to refresh the mind and the compound plant essential oil of repellent antipruritic, it is mixed by the component of following parts by weight meter:Suddenly
Bar seed oil 30-80 parts suddenly, peppermint leaf oil 10-20 parts, blue gum leaf oil 1-10 parts, lavender oil 1-10 parts, bergamot fruit oil 1-10
Part, hypericum perforatum oil 1-10 parts, patchouli oil 1-10 parts, natural menthol 5-20 parts, natural borneol 1-10 parts, tocopherol 0.5-
5 parts, natural bisabolol 0.5-5 parts, aloe gel freeze-dried powder 0.1-2 parts.
Sachet is Chinese earliest for the mode refreshed oneself, its volatility being namely based in these medical substances that plays a role
Composition.The present invention gives full play to motherland's TCM Features and combines modern pharmacology research achievement, match somebody with somebody using sachet as exploitation basis
With natural, refrigerant, inducing resuscitation of having one's ideas straightened out composition, compound essential oil product is formed, product has refrigerant, pleasant herbal aromatic, and can be fast
Fast sterilizing and itch-relieving, another selection is provided to pursue the personage of natural health.
Peppermint leaf oil:Dispelling wind and heat from the body, head clearing.Blue gum leaf oil:Expelling wind to resolve the exterior, clearing heat and detoxicating, desinsection is antipruritic.Pass through leaf company
Stick up oil:Clearing heat and detoxicating, dispersing swelling and dissipating binds, dispelling wind and heat from the body.Patchouli oil:Eliminate dampness with aromatics, deliver relieving summer-heat.Menthol:It is refrigerant antipruritic.It is raw
Educating phenol and reducing cell needs oxygen amount, the power that sustains life, endurance, endurance, while tocopherol has good oxidation resistance, energy
Extend the shelf life.Bisabolol has good anti-inflammatory, bactericidal action, can subside a swelling.Borneol:Inducing resuscitation of having one's ideas straightened out, priming are up.Smoke
Clothing grass oil and bergamot fruit oil can releive pressure, alleviate headache, anti-inflammation and sterilization, novel aroma helps to improve spirit, plays
The effect of Synergistic.Jojoba oil contains abundant vitamin, is easily merged with skin, has the effect for nourishing softening skin
Fruit, based on oil.Aloe gel freeze-dried powder can make essential oil volatility reduction while repellent antipruritic, play slow release,
The lasting effect of lasting.
Modern pharmacology research proves:Hypericum perforatum oil has obvious inhibitory action to gram-positive bacteria.In Pogostemon cablin
Pogostone is main antimicrobial component, is had to salmonella, Escherichia coli, Shigella, staphylococcus aureus etc. necessarily
Inhibitory action, to staphylococcus aureus effect be significantly stronger than enteric bacilli.Menthol has obvious itching-relieving action, and it is made
With with the effect to antihistamine and suppress histamine release it is relevant.Natural borneol is safe, and drug effect is stronger, disappears with antibacterial
Scorching, analgesic, protection nervous centralis, the effect for promoting medicine to pass through blood-brain barrier.Aloe gel can with desinsection antipruritic, detoxification sore treatment
Tinea, anti-inflammation and sterilization.
The problem of volatile in order to solve essential oil class product, retention time is short, and fragrance is not lasting enough, present invention invention are special
Aloe gel freeze-dried powder is added, while repellent antipruritic effect is strengthened, essential oil volatility can be reduced well, product works
More preferably, the fragrant breath of book on Chinese herbal medicine is substantially more longlasting, and pro-skin experience effect is more preferable.The compound plant essential oil each component collaboration hair of the present invention
Synergistic effect is waved, there is refrigerant, pleasant fragrance, safety is gentle, can refresh the mind, quick repellent antipruritic, for non-defective unit of aestivating.
Preferably, the peppermint leaf oil is obtained, CO 2 supercritical using carbon dioxide supercritical extraction dried peppermint leaf
The state modulator of extraction is:Extracting pressure 8-10Mpa, 50-55 DEG C of extraction temperature, carbon dioxide flow 25-30L/h, during extraction
Between 1-1.5h.
Preferably, the hypericum perforatum oil is obtained using carbon dioxide supercritical extraction hypericum perforatum, carbon dioxide surpasses
The state modulator of critical extraction is:Extracting pressure 20-22Mpa, 40-45 DEG C of extraction temperature, carbon dioxide flow 25-30L/h, extraction
Take time 1-1.5h.
Preferably, the patchouli oil is obtained, CO 2 supercritical using carbon dioxide supercritical extraction Pogostemon cablin
The state modulator of extraction is:Extracting pressure 15-16Mpa, 40-42 DEG C of extraction temperature, carbon dioxide flow 20-25L/h, quality are dense
The ethanol spent for 90-95% is entrainer, extraction time 2-2.5h.
Peppermint leaf oil of the present invention, hypericum perforatum oil, patchouli oil are extracted using carbon dioxide supercritical extraction technology, are operated
Temperature is low, and thermal instability composition and oxidizable component are survivable in volatile oil, and the active ingredient of acquisition is more comprehensively, closer
Natural component ratio.
It is a kind of to refresh the mind and the preparation method of the compound plant essential oil of repellent antipruritic, comprise the following steps:
(1)Natural menthol, natural borneol and jojoba seed oil are weighed in proportion, control 20-25 DEG C of temperature, ultrasound is to admittedly
Phased soln, then draw liquid into closed container;
(2)Into closed container, addition peppermint leaf oil, blue gum leaf oil, lavender oil, bergamot fruit are oily, hypericum perforatum is oily,
Patchouli oil, tocopherol and natural bisabolol, it is well mixed to obtain primary essential oil;
(3)Take the primary essential oil for accounting for primary essential oil cumulative volume 15-25% and aloe gel freeze-dried powder ground and mixed uniform, so
Remaining primary essential oil is added afterwards to be well mixed, it is filling into Ethereal oil bottle after homogenizer homogeneous.
In production process of the present invention, low temperature ultrasonic dissolving technology is employed, avoids menthol, borneol uses conventional heating
Caused by dissolution mechanism the problem of oils quality decline, the operating time is shortened, effectively reduces the volatilization of component, is lifted
Product quality.
The beneficial effects of the invention are as follows:
1st, raw materials used is natural plant extraction, no chemical raw material, and safety is gentle, can be long-term use of, more meets day
So, healthy consumption demand.
2nd, essential oil main component is micromolecular compound, easily permeates in skin, is easily absorbed by cell, is worked rapid.
Product fragrance walks string, inducing resuscitation of having one's ideas straightened out, by the position such as massaging after forehead, temple, ear, can be refreshed oneself with fast wake-up brain cell
Restoring consciouness.Through thousand personnel that go beyond what is acceptable or necessary(User is mainly driving personnel, stay up late overtime work personnel, student etc.)Experience, refreshes the mind, pin
Repellent antipruritic after bite by mosquitos is acted on, total effective rate is more than 96%.
3rd, product odour is refrigerant, fresh and clean, has draft breath, can adjust brain centres sense by inhaling the modes such as news
Should, human body is produced the refrigerant sensation soothed the spirit.
4th, because steam distillation is simple to operate, cost is relatively low, and the extraction to essential oil both at home and abroad at present uses the party more
Formula.But steam distillation operation temperature is higher, thermally labile component and oxidizable component are easily destroyed in volatile oil, and then are influenceed
Product quality.It is main to investigate active ingredient component and ratio in oil yield and volatile oil by contrast test, using carbon dioxide
Supercritical extract peppermint leaf oil, oil yield 2.43%, for 2.1 times of steam distillation oil yield 1.15%.Hypericum perforatum oil is adopted
With carbon dioxide supercritical extraction peppermint oil, oil yield 3.39%, for 1.6 times of steam distillation oil yield 2.11%.The wide leaves of pulse plants
Sesame oil is using carbon dioxide supercritical extraction technology extraction oil yield 2.46%, for 1.6 times of steam distillation 1.56%.Dioxy
Change three kinds of plant extractions that carbon supercritical extract is applied in prescription, it is with the obvious advantage, in the absence of dissolvent residual, with steam distillation
Compare, because operation temperature is low, terpenes constituents are not easy to lose, and part higher boiling composition can also extract, product entirety product
Matter is more excellent.
5th, the present invention use low temperature ultrasonic dissolving technology, avoid menthol, borneol it is conventional use heating for dissolving method and
Caused oils quality decline, shortens the operating time, effectively reduces the volatilization of component, improves product quality.
6th, the present invention is especially added with aloe gel freeze-dried powder, while repellent antipruritic effect is strengthened, solves well
The problem of essential oil class product is volatile, and retention time is short, and fragrance is not lasting enough.Product volatile ingredient can be made slowly to discharge,
The fragrant breath of book on Chinese herbal medicine is substantially more longlasting, and pro-skin experience effect is more preferable.
Embodiment
Below by specific embodiment, technical scheme is described in further detail.
In the present invention, if not refering in particular to, used raw material and equipment etc. are commercially available or commonly used in the art.
Method in following embodiments, it is the conventional method of this area unless otherwise instructed.
Embodiment 1:
It is a kind of to refresh the mind and the compound plant essential oil of repellent antipruritic, it is mixed by the component of following parts by weight meter:Suddenly
Bar seed oil suddenly(It is commercially available)30 parts, 10 parts of peppermint leaf oil, blue gum leaf oil(It is commercially available)1 part, lavender oil(It is commercially available)1 part, bergamot fruit
Oil(It is commercially available)1 part, 1 part of hypericum perforatum oil, 10 parts of patchouli oil, natural menthol(It is commercially available)20 parts, natural borneol(It is commercially available)1
Part, tocopherol(It is commercially available)0.5 part, natural bisabolol(It is commercially available)0.5 part, aloe gel freeze-dried powder(It is commercially available)0.1 part.
Peppermint leaf oil is obtained using carbon dioxide supercritical extraction dried peppermint leaf, is extracted after dried peppermint leaf drying and crushing, titanium dioxide
The state modulator of carbon supercritical extract is:Extracting pressure 8Mpa, 50 DEG C, carbon dioxide flow 25L/h of extraction temperature, extraction time
1.5h。
Hypericum perforatum oil is obtained using carbon dioxide supercritical extraction hypericum perforatum, is extracted after hypericum perforatum drying and crushing,
The state modulator of carbon dioxide supercritical extraction is:Extracting pressure 20Mpa, 40 DEG C, carbon dioxide flow 25L/h of extraction temperature,
Extraction time 1.5h.
Patchouli oil is obtained using carbon dioxide supercritical extraction Pogostemon cablin, is extracted after Pogostemon cablin drying and crushing, titanium dioxide
The state modulator of carbon supercritical extract is:Extracting pressure 15Mpa, 40 DEG C, carbon dioxide flow 20L/h of extraction temperature, quality is dense
The ethanol spent for 90% is entrainer, extraction time 2.5h.
Preparation method, comprise the following steps:
(1)Natural menthol, natural borneol and jojoba seed oil are weighed in proportion, control 20 DEG C of temperature, ultrasound to solid phase
Dissolving, then draws liquid into closed container;
(2)Into closed container, addition peppermint leaf oil, blue gum leaf oil, lavender oil, bergamot fruit are oily, hypericum perforatum is oily,
Patchouli oil, tocopherol and natural bisabolol, it is well mixed to obtain primary essential oil;
(3)Take the primary essential oil for accounting for primary essential oil cumulative volume 15% and aloe gel freeze-dried powder ground and mixed uniform, Ran Houjia
Enter remaining primary essential oil to be well mixed, it is filling into Ethereal oil bottle after homogenizer homogeneous.
Embodiment 2:
It is a kind of to refresh the mind and the compound plant essential oil of repellent antipruritic, it is mixed by the component of following parts by weight meter:Suddenly
Bar seed oil suddenly(It is commercially available)80 parts, 20 parts of peppermint leaf oil, blue gum leaf oil(It is commercially available)10 parts, lavender oil(It is commercially available)10 parts, bergamot
Fruit oil(It is commercially available)10 parts, 10 parts of hypericum perforatum oil, 1 part of patchouli oil, natural menthol(It is commercially available)5 parts, natural borneol(It is commercially available)
10 parts, tocopherol(It is commercially available)5 parts, natural bisabolol(It is commercially available)5 parts, aloe gel freeze-dried powder(It is commercially available)2 parts.
Peppermint leaf oil is obtained using carbon dioxide supercritical extraction dried peppermint leaf, is extracted after dried peppermint leaf drying and crushing, titanium dioxide
The state modulator of carbon supercritical extract is:Extracting pressure 10Mpa, 55 DEG C, carbon dioxide flow 30L/h of extraction temperature, during extraction
Between 1h.
Hypericum perforatum oil is obtained using carbon dioxide supercritical extraction hypericum perforatum, is extracted after hypericum perforatum drying and crushing,
The state modulator of carbon dioxide supercritical extraction is:Extracting pressure 22Mpa, 45 DEG C, carbon dioxide flow 30L/h of extraction temperature,
Extraction time 1h.
Patchouli oil is obtained using carbon dioxide supercritical extraction Pogostemon cablin, is extracted after Pogostemon cablin drying and crushing, titanium dioxide
The state modulator of carbon supercritical extract is:Extracting pressure 16Mpa, 42 DEG C, carbon dioxide flow 25L/h of extraction temperature, quality is dense
The ethanol spent for 95% is entrainer, extraction time 2h.
Preparation method, comprise the following steps:
(1)Natural menthol, natural borneol and jojoba seed oil are weighed in proportion, control 25 DEG C of temperature, ultrasound to solid phase
Dissolving, then draws liquid into closed container;
(2)Into closed container, addition peppermint leaf oil, blue gum leaf oil, lavender oil, bergamot fruit are oily, hypericum perforatum is oily,
Patchouli oil, tocopherol and natural bisabolol, it is well mixed to obtain primary essential oil;
(3)Take the primary essential oil for accounting for primary essential oil cumulative volume 25% and aloe gel freeze-dried powder ground and mixed uniform, Ran Houjia
Enter remaining primary essential oil to be well mixed, it is filling into Ethereal oil bottle after homogenizer homogeneous.
Embodiment 3:
It is a kind of to refresh the mind and the compound plant essential oil of repellent antipruritic, it is mixed by the component of following parts by weight meter:Suddenly
Bar seed oil suddenly(It is commercially available)50 parts, 15 parts of peppermint leaf oil, blue gum leaf oil(It is commercially available)5 parts, lavender oil(It is commercially available)5 parts, bergamot fruit
Oil(It is commercially available)5 parts, 5 parts of hypericum perforatum oil, 5 parts of patchouli oil, natural menthol(It is commercially available)10 parts, natural borneol(It is commercially available)5 parts,
Tocopherol(It is commercially available)2 parts, natural bisabolol(It is commercially available)3 parts, aloe gel freeze-dried powder(It is commercially available)1 part.
Peppermint leaf oil is obtained using carbon dioxide supercritical extraction dried peppermint leaf, is extracted after dried peppermint leaf drying and crushing, titanium dioxide
The state modulator of carbon supercritical extract is:Extracting pressure 9Mpa, 52 DEG C, carbon dioxide flow 30L/h of extraction temperature, extraction time
1.5h。
Hypericum perforatum oil is obtained using carbon dioxide supercritical extraction hypericum perforatum, is extracted after hypericum perforatum drying and crushing,
The state modulator of carbon dioxide supercritical extraction is:Extracting pressure 21Mpa, 42 DEG C, carbon dioxide flow 25L/h of extraction temperature,
Extraction time 1.5h.
Patchouli oil is obtained using carbon dioxide supercritical extraction Pogostemon cablin, is extracted after Pogostemon cablin drying and crushing, titanium dioxide
The state modulator of carbon supercritical extract is:Extracting pressure 15Mpa, 40 DEG C, carbon dioxide flow 25L/h of extraction temperature, quality is dense
The ethanol spent for 90% is entrainer, extraction time 2h.
Preparation method, comprise the following steps:
(1)Natural menthol, natural borneol and jojoba seed oil are weighed in proportion, control 22 DEG C of temperature, ultrasound to solid phase
Dissolving, then draws liquid into closed container;
(2)Into closed container, addition peppermint leaf oil, blue gum leaf oil, lavender oil, bergamot fruit are oily, hypericum perforatum is oily,
Patchouli oil, tocopherol and natural bisabolol, it is well mixed to obtain primary essential oil;
(3)Take the primary essential oil for accounting for primary essential oil cumulative volume 20% and aloe gel freeze-dried powder ground and mixed uniform, Ran Houjia
Enter remaining primary essential oil to be well mixed, it is filling into Ethereal oil bottle after homogenizer homogeneous.
Essential oil product main component of the present invention is micromolecular compound, easily permeates in skin, is easily absorbed by cell, is risen
Effect is rapid.Product fragrance walks string, inducing resuscitation of having one's ideas straightened out, can be thin with fast wake-up brain by the position such as massaging after forehead, temple, ear
Born of the same parents, refresh the mind.Through thousand personnel that go beyond what is acceptable or necessary(User is mainly driving personnel, stay up late overtime work personnel, student etc.)Experience, refreshes oneself
Restoring consciouness, for after bite by mosquitos repellent antipruritic act on, total effective rate is more than 96%.
Foundation《Cosmetics health specification》(Version in 2007), wholesomeness experiment, result of the test table are carried out to the present invention
It is bright:Micro-biology experiment, hygienic chemistry index meet code requirement.Repeatedly skin irritation test result is:It is nonirritant.
Assay is as follows:
Micro biological Tests result
Inspection project |
Assay |
Limit value |
Total plate count(CFU/g or CFU/mL) |
<10 |
≤1000 |
Yeast and mold sum(CFU/g or CFU/mL) |
<10 |
≤100 |
Excrement colibacillus group/g (or mL) |
Do not detect |
It must not detect |
Staphylococcus aureus/g (or mL) |
Do not detect |
It must not detect |
Pseudomonas aeruginosa/g (or mL) |
Do not detect |
It must not detect |
Health chemical testing result
Inspection project |
Unit |
Assay |
The method of inspection |
Method concentrations |
Limit value |
Mercury |
mg/kg |
0.049 |
Hydride generation atomic fluorescence photometry |
0.006 |
≤1 |
Arsenic |
mg/kg |
<0.04 |
Hydride generation atomic fluorescence photometry |
0.04 |
≤10 |
Lead |
mg/kg |
<5 |
Atomic absorption spectrophotometry |
5 |
≤40 |
Embodiment described above is a kind of preferable scheme of the present invention, not the present invention is made any formal
Limitation, there are other variants and remodeling on the premise of without departing from the technical scheme described in claim.