CN104273184B - A kind of vegetable insecticide and preparation method thereof - Google Patents
A kind of vegetable insecticide and preparation method thereof Download PDFInfo
- Publication number
- CN104273184B CN104273184B CN201410604954.3A CN201410604954A CN104273184B CN 104273184 B CN104273184 B CN 104273184B CN 201410604954 A CN201410604954 A CN 201410604954A CN 104273184 B CN104273184 B CN 104273184B
- Authority
- CN
- China
- Prior art keywords
- extracting solution
- parts
- solution
- weight
- wuduoyun
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of vegetable insecticide. This insecticide is to be that raw material is prepared from by Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution, white vinegar, capsicum solution, can effectively prevent and kill the vegetable worm such as aphid, Limax, and make vegetable look luxuriant, improve its yield. The liquor residue phase of this insecticide only 8��12 days, nontoxic to people and animals simultaneously. The preparation method that present invention also offers described insecticide. Insecticide effect of the present invention is notable, and cost is low, green non-pollution, has wide market application foreground.
Description
Technical field
The present invention relates to a kind of insecticide, particularly to a kind of vegetable insecticide and preparation method thereof.
Background technology
Vegetable is one of requisite food in people's conventional food. Vegetable can provide multivitamin necessary to human body and mineral. It is one of requisite food in people's diet according to vegetable. Vegetable can provide multivitamin necessary to human body and mineral. According to international food and agricultural organization's nineteen ninety statistics, the 60% of ascorbic 90%, the vitamin A of needed by human is from vegetable. Additionally, vegetable also has diversified phytochemicals, be it have been recognized that to the effective composition of health, such as carotenoid, two propen compounds, methyl sulfide compound etc. Nutrient in current fruit and vegerable can effectively preventing chronic, degenerative disease many kinds of substance studied discovery by people. Vegetable is dish with, feedstuff, the multipurpose breed such as views and admires, and easily, yield is high in cultivation, can repeatedly shell leaf and gather, and the supply phase is long, can list when summer lacks leaf vegetables, and the north can be cultivated at daylight energy-saving greenhouse. But vegetable is very easily insect infestation in growth course, mainly there is the vegetable worm such as aphid, Limax, if preventing not in time and killing vegetable worm, yield and the quality of vegetable can be had a strong impact on.
At present, people are when preventing and treating vegetable worm, it is all generally that the pesticide adopting high concentration is sprayed, although prevention effect is fine, but the farm chemical ingredients of Residues in Vegetables is too high, and human body is damaged, the health making people is susceptible to suffer from various disease, the immunocompetence easily causing each function of human body declines, the vegetable that long-term edible residual pesticide is too high, is more easy to the generation of the various disease of hidden danger.
Summary of the invention
It is an object of the invention to overcome above-mentioned deficiency existing in prior art, it is provided that a kind of vegetable insecticide. This insecticide is to be that raw material is prepared from by Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution, white vinegar, capsicum solution, can effectively prevent and kill the vegetable worm such as aphid, Limax, vegetable is made to look luxuriant, improve yield, the liquor residue phase is short simultaneously, and people and animals are nontoxic.
The preparation method that another object of the present invention is to provide described insecticide.
In order to realize foregoing invention purpose, the invention provides techniques below scheme:
Vegetable insecticide of the present invention is to be the medicament that raw material is prepared from by Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution, white vinegar, capsicum solution.
Described Folium Artemisiae Argyi extractive liquid obtains by the following method: take Folium Artemisiae Argyi, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Folium Artemisiae Argyi extractive liquid.
Described Rhizoma Iridis Japonicae extracting solution obtains by the following method: take Rhizoma Iridis Japonicae, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Rhizoma Iridis Japonicae extracting solution.
Described Melia azedarach L. extracting solution obtains by the following method: take Melia azedarach L., adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Melia azedarach L. extracting solution.
Described WUDUOYUN extracting solution obtains by the following method: take WUDUOYUN, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain WUDUOYUN extracting solution.
Described Bright Yellow extracting solution obtains by the following method: take Bright Yellow, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Bright Yellow extracting solution.
Described Herba Artemisiae Annuae extracting solution obtains by the following method: take Herba Artemisiae Annuae, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Herba Artemisiae Annuae extracting solution.
Natural plants Folium Artemisiae Argyi, Rhizoma Iridis Japonicae, Melia azedarach L., WUDUOYUN, Bright Yellow, Herba Artemisiae Annuae are respectively adopted water soaking 15��40 days by the present invention, make effective ingredient be substantially dissolved in water, are filtrated to get extracting solution. When soak time was less than 15 days, effective ingredient cannot fully be dissolved in water; When soak time was more than 40 days, drug smell runs off, and drug effect reduces. Preferably, soak time is 35 days to the best.
Described capsicum solution obtains by the following method: takes the Fructus Capsici of fresh mature, smashs to pieces, adds 1��water of 3 times of weight, and soaking at room temperature 7��15 days filters, takes filtrate, obtain capsicum solution. Preferably, described capsicum solution obtains by the following method: takes the Fructus Capsici of fresh mature, smashs to pieces, adds the water of 2 times of weight, soaking at room temperature 10 days, filters, take filtrate, obtain capsicum solution. Preferably, described Fructus Capsici is qi xing paprika, and qi xing paprika has the characteristic that pungent is strong.
Folium Artemisiae Argyi is the dried leaves of feverfew Chinese mugwort ArtemisiaargyiLevl.etVant., main containing compositions such as volatile oil, flavonoid, triterpenes, tannins, having the physiologically actives such as hemostasis, anti-bacteria and anti-virus, scavenging free radicals, analgesia, Folium Artemisiae Argyi extractive liquid has penetrating odor, can anthelmintic. Rhizoma Iridis Japonicae is the rhizome shape of Jris herbaceous plant Herba Iridis japonicae, it is distributed mainly on the ground such as East China, south China, southwest and Hebei, Shaanxi, Gansu, it is a kind of ornamental plant, is also traditional Chinese crude drug, traditional medicine is used for help digestion parasite killing, clearing away heat and loosing the bowels, control food abdominal distention etc. Melia azedarach L. is not only material with plant, is also medicinal plants, and its flower, leaf, fruit, root bark all can be used as medicine, can ascarifuge, ancylostome etc., make ointment by Fructus Toosendan and can control tinea capitis. Preferably, Melia azedarach L. extracting solution of the present invention is Folium Meliae extracting solution and/or chinaberry root extracting solution. WUDUOYUN, has another name called Herba Euphorbiae Helioscopiae, Euphorbia esula L, is a kind of herbaceos perennial opening five flowers, has antiinflammatory, insecticidal action. Bright Yellow has another name called gold leaf Fructus durantae repentis, the long oval of leaf, and coloured gold is yellow to yellowish green, and evergreen shrubs, southern china is widely cultivated, leaf bitter and puckery flavor, can strengthen the property of medicine and the penetrating odor of insecticide of the present invention. White vinegar can effectively regulate the pH value of insecticide so that it is in highly acid, plays agent efficacy better.Capsicum solution can strengthen insect protected and insecticidal power.
Applicant is found by lot of experiments, by natural plants Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution and white vinegar, capsicum solution compatibility, the effect of Synergistic can be played, the insecticide obtained has micro-poison, can effectively kill the vegetable worms such as aphid, but people and animals' toxic and side effects is little; This insecticide has very strong pungent odor simultaneously, can effectively drive the vegetable worm such as aphid, Limax, to reach prevention and to kill the purpose of the vegetable worm such as aphid, Limax.
Preferably, the weight of described each raw material is: Folium Artemisiae Argyi extractive liquid 3��10 parts, Rhizoma Iridis Japonicae extracting solution 3��10 parts, Melia azedarach L. extracting solution 3��10 parts, WUDUOYUN extracting solution 1��8 part, Bright Yellow extracting solution 1��8 part, Herba Artemisiae Annuae extracting solution 1��8 part, white vinegar 0.05��2 part, capsicum solution 1��4 part. Insecticide of the present invention is with Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution, white vinegar and capsicum solution for raw material, effect of insect protected, parasite killing should be played, reducing its toxic action to people and animals again, this just brings very big difficulty for the screening of parts by weight of raw materials proportioning. Applicant finds through repeatedly replica test, and insecticide of the present invention is under above-mentioned weight, it is possible to effectively prevents and kills the vegetable worm such as aphid, Limax, significantly improving the yield of vegetable, and the liquor residue phase is short.
It is further preferred that the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 3��10 parts, Folium Artemisiae Argyi extractive liquid 4��8 parts, Melia azedarach L. extracting solution 3��9 parts, WUDUOYUN extracting solution 2��7 parts, Bright Yellow extracting solution 1��6 part, Herba Artemisiae Annuae extracting solution 2��6 parts, white vinegar 0.05��1.5 part, capsicum solution 1��3 part.
It is further preferred that the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 3��8 parts, Folium Artemisiae Argyi extractive liquid 4��7 parts, Melia azedarach L. extracting solution 3��9 parts, WUDUOYUN extracting solution 2��7 parts, Bright Yellow extracting solution 2��6 parts, Herba Artemisiae Annuae extracting solution 2��5 parts, white vinegar 0.08��1.0 part, capsicum solution 1��3 part.
It is further preferred that the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 3��7 parts, Folium Artemisiae Argyi extractive liquid 4��7 parts, Melia azedarach L. extracting solution 4��8 parts, WUDUOYUN extracting solution 2��6 parts, Bright Yellow extracting solution 2��6 parts, Herba Artemisiae Annuae extracting solution 3��5 parts, white vinegar 0.08��0.8 part, capsicum solution 1��3 part.
It is further preferred that the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 4��6 parts, Folium Artemisiae Argyi extractive liquid 4��7 parts, Melia azedarach L. extracting solution 5��7 parts, WUDUOYUN extracting solution 4��6 parts, Bright Yellow extracting solution 3��5 parts, Herba Artemisiae Annuae extracting solution 3��5 parts, white vinegar 0.1��0.5 part and capsicum solution 1��2 part.
Preferably, the weight of described each raw material is the best: Rhizoma Iridis Japonicae extracting solution 6 parts, Folium Artemisiae Argyi extractive liquid 6 parts, Melia azedarach L. extracting solution 5 parts, WUDUOYUN extracting solution 5 parts, Bright Yellow extracting solution 4 parts, Herba Artemisiae Annuae extracting solution 4 parts, white vinegar 0.2 part and capsicum solution 1.8 parts.
By above preferred, it is possible to play the synergistic function between each raw material components further, strengthen the efficacy of drugs of medicament, strengthen the strong sharp aroma of medicament, thus preventing better and killing the vegetable worm such as aphid, Limax, significantly improve the yield of vegetable simultaneously.
The preparation method of vegetable insecticide of the present invention, specifically comprise the following steps that by ratio of weight and the number of copies, Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution and Herba Artemisiae Annuae extracting solution are mixed, it is subsequently adding white vinegar and capsicum solution, mixing, obtains vegetable insecticide.
During use, vegetable of the present invention insecticide aerosol apparatus is uniformly sprayed on vegetable.If it is fine, can spray again once after 3 days; If the rainy day, wait and after becoming a fine day, continue spray.
Compared with prior art, the beneficial effects of the present invention is:
(1) insecticide of the present invention is with natural plants Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution and white vinegar, capsicum solution for raw material components, further by screening the weight of each raw material components, each raw material components is made to play the effect of Synergistic, effectively kill the vegetable worm such as aphid, Limax by its micro-poison having and strong pungent odor, the preventing efficiency of the various vegetable fields such as Fructus Solani melongenae, Radix Raphani, Chinese cabbage, Brassica oleracea L.var.capitata L., Fructus Capsici is reached more than 90%.
(2) vegetable of the present invention effectively prevents with insecticide and kills the vegetable worm such as aphid, Limax, makes vegetable growing way better, output increased more than 10%; The liquor residue phase is short, only 8��12 days.
(2) preparation method of insecticide of the present invention has been sufficiently reserved the active drug composition of each raw material components, and technique is simple, and cost is low.
Detailed description of the invention
Below in conjunction with test example and detailed description of the invention, the present invention is described in further detail. But this should not being interpreted as, the scope of the above-mentioned theme of the present invention is only limitted to below example, and all technology realized based on present invention belong to the scope of the present invention.
Embodiment 1
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: take Folium Artemisiae Argyi, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, takes filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of Rhizoma Iridis Japonicae extracting solution: take Rhizoma Iridis Japonicae, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, takes filtrate, obtain Rhizoma Iridis Japonicae extracting solution.
The preparation of Melia azedarach L. extracting solution: take chinaberry root, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, takes filtrate, obtain Melia azedarach L. extracting solution.
WUDUOYUN extracting solution: take WUDUOYUN, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, takes filtrate, obtain WUDUOYUN extracting solution.
The preparation of Bright Yellow extracting solution: take Bright Yellow, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, takes filtrate, obtain Bright Yellow extracting solution.
The preparation of Herba Artemisiae Annuae extracting solution: take Herba Artemisiae Annuae, adds the water of 3 times of weight, soaks 35 days under room temperature, filters, takes filtrate, obtain Herba Artemisiae Annuae extracting solution.
The preparation of capsicum solution: the ripe red qi xing paprika taking just harvesting is smashed to pieces, adds the water of 2 times of weight, soaking at room temperature 10 days, filters, take filtrate, obtain capsicum solution.
(2) preparation of insecticide
By ratio of weight and the number of copies, take Folium Artemisiae Argyi extractive liquid 6 parts, Rhizoma Iridis Japonicae extracting solution 6 parts, Melia azedarach L. extracting solution 5 parts, WUDUOYUN extracting solution 5 parts, Bright Yellow extracting solution 4 parts and Herba Artemisiae Annuae extracting solution 4 parts mixing, it is subsequently adding white vinegar 0.2 part and capsicum solution 1.8 parts, mixing, obtains vegetable insecticide.
Embodiment 2
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: take Folium Artemisiae Argyi, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, takes filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of Rhizoma Iridis Japonicae extracting solution: take Rhizoma Iridis Japonicae, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, takes filtrate, obtain Rhizoma Iridis Japonicae extracting solution.
The preparation of Melia azedarach L. extracting solution: take Folium Meliae, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, takes filtrate, obtain Melia azedarach L. extracting solution.
WUDUOYUN extracting solution: take WUDUOYUN, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, takes filtrate, obtain WUDUOYUN extracting solution.
The preparation of Bright Yellow extracting solution: take Bright Yellow, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, takes filtrate, obtain Bright Yellow extracting solution.
The preparation of Herba Artemisiae Annuae extracting solution: take Herba Artemisiae Annuae, adds the water of 2 times of weight, soaks 20 days under room temperature, filters, takes filtrate, obtain Herba Artemisiae Annuae extracting solution.
The preparation of capsicum solution: the ripe red qi xing paprika just plucked is smashed to pieces, adds the water of 1 times of weight, soaking at room temperature 7 days, filter, take filtrate, obtain capsicum solution.
(2) preparation of insecticide
By ratio of weight and the number of copies, take Folium Artemisiae Argyi extractive liquid 3 parts, Rhizoma Iridis Japonicae extracting solution 3 parts, Melia azedarach L. extracting solution 3 parts, WUDUOYUN extracting solution 1 part, Bright Yellow extracting solution 1 part and Herba Artemisiae Annuae extracting solution 1 part mixing, it is subsequently adding white vinegar 0.05 part and capsicum solution 1 part, mixing, obtains vegetable insecticide.
Embodiment 3
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: take Folium Artemisiae Argyi, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, take filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of Rhizoma Iridis Japonicae extracting solution: take Rhizoma Iridis Japonicae, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, take filtrate, obtain Rhizoma Iridis Japonicae extracting solution.
The preparation of Melia azedarach L. extracting solution: take chinaberry root, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, take filtrate, obtain Melia azedarach L. extracting solution.
WUDUOYUN extracting solution: take WUDUOYUN, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, take filtrate, obtain WUDUOYUN extracting solution.
The preparation of Bright Yellow extracting solution: take Bright Yellow, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, take filtrate, obtain Bright Yellow extracting solution.
The preparation of Herba Artemisiae Annuae extracting solution: take Herba Artemisiae Annuae, adds the water of 4 times of weight, soaking at room temperature 15 days, filters, take filtrate, obtain Herba Artemisiae Annuae extracting solution.
The preparation of capsicum solution: the ripe red qi xing paprika taking just harvesting is smashed to pieces, adds the water of 3 times of weight, soaking at room temperature 15 days, filters, take filtrate, obtain capsicum solution.
(2) preparation of insecticide
By ratio of weight and the number of copies, take Folium Artemisiae Argyi extractive liquid 10 parts, Rhizoma Iridis Japonicae extracting solution 10 parts, Melia azedarach L. extracting solution 10 parts, WUDUOYUN extracting solution 8 parts, Bright Yellow extracting solution 8 parts and Herba Artemisiae Annuae extracting solution 8 parts mixing, it is subsequently adding white vinegar 2 parts and capsicum solution 3 parts, mixing, obtains vegetable insecticide.
Embodiment 4
(1) preparation of raw material
The preparation of Folium Artemisiae Argyi extractive liquid: take Folium Artemisiae Argyi, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, take filtrate, obtain Folium Artemisiae Argyi extractive liquid.
The preparation of Rhizoma Iridis Japonicae extracting solution: take Rhizoma Iridis Japonicae, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, take filtrate, obtain Rhizoma Iridis Japonicae extracting solution.
The preparation of Melia azedarach L. extracting solution: take Folium Meliae, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, take filtrate, obtain Melia azedarach L. extracting solution.
WUDUOYUN extracting solution: take WUDUOYUN, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, take filtrate, obtain WUDUOYUN extracting solution.
The preparation of Bright Yellow extracting solution: take Bright Yellow, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, take filtrate, obtain Bright Yellow extracting solution.
The preparation of Herba Artemisiae Annuae extracting solution: take Herba Artemisiae Annuae, adds the water of 3 times of weight, soaking at room temperature 40 days, filters, take filtrate, obtain Herba Artemisiae Annuae extracting solution.
The preparation of capsicum solution: the ripe red qi xing paprika taking just harvesting is smashed to pieces, adds the water of 2 times of weight, soaking at room temperature 8 days, filters, take filtrate, obtain capsicum solution.
(2) preparation of insecticide
By ratio of weight and the number of copies, take Folium Artemisiae Argyi extractive liquid 8 parts, Rhizoma Iridis Japonicae extracting solution 5 parts, Melia azedarach L. extracting solution 7 parts, WUDUOYUN extracting solution 4 parts, Bright Yellow extracting solution 3 parts and Herba Artemisiae Annuae extracting solution 5 parts mixing, it is subsequently adding white vinegar 1 part and capsicum solution 2 parts, mixing, obtains vegetable insecticide.
The insecticide of embodiment 1��4 preparation is acid, in faint yellow, has very strong pungent odor.
Comparative example 1
By ratio of weight and the number of copies, take Folium Artemisiae Argyi extractive liquid 6 parts, Melia azedarach L. extracting solution 5 parts, WUDUOYUN extracting solution 5 parts, Bright Yellow extracting solution 4 parts and Herba Artemisiae Annuae extracting solution 4 parts mixing, be subsequently adding white vinegar 0.2 part and capsicum solution 1.8 parts, mixing, obtain vegetable insecticide. The preparation method of described Folium Artemisiae Argyi extractive liquid, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution and capsicum solution is with embodiment 1.
Comparative example 2
By ratio of weight and the number of copies, take Folium Artemisiae Argyi extractive liquid 6 parts, Rhizoma Iridis Japonicae extracting solution 6 parts, Melia azedarach L. extracting solution 5 parts, WUDUOYUN extracting solution 5 parts and Herba Artemisiae Annuae extracting solution 4 parts mixing, be subsequently adding white vinegar 0.2 part and capsicum solution 1.8 parts, mixing, obtain vegetable insecticide. The preparation method of described Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Herba Artemisiae Annuae extracting solution and capsicum solution is with embodiment 1.
Comparative example 3
By ratio of weight and the number of copies, take Folium Artemisiae Argyi extractive liquid 6 parts, Rhizoma Iridis Japonicae extracting solution 6 parts, Melia azedarach L. extracting solution 5 parts, Bright Yellow extracting solution 4 parts and Herba Artemisiae Annuae extracting solution 4 parts mixing, be subsequently adding capsicum solution 1.8 parts, mixing, obtain vegetable insecticide. The preparation method of described Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution and capsicum solution is with embodiment 1.
Embodiment 5
Vegetable prepared by above-described embodiment 1��4 is carried out insect protected test with insecticide: Brassica oleracea L.var.capitata L. ground aphid, Limax insect pest etc. also do not occur monthly is sprayed twice insecticide of the present invention, each fountain height is 20kg/ mu, and second time carries out after first time spray medicine for 3 days. With do not spray any insecticide vegetable field for reference, evaluate the insecticide of the present invention preventing efficiency on vegetable insect pest and the impact on yield of vegetables, simultaneously to spray the vegetable field of insecticide described in comparative example 1��3 for comparative example.
The wherein evaluation methodology of preventing efficiency: spray medicine is after 2 months continuously, randomly selects 200 Brassica oleracea L.var.capitata L., observes the total amount of the vegetable worm such as aphid, Limax on 200 Brassica oleracea L.var.capitata L.. The computing formula of preventing efficiency is: preventing efficiency=(not spraying the worm total quantity of the worm total quantity-spray medicine vegetable field of medicine vegetable field) �� does not spray worm total quantity �� 100% of medicine vegetable field.
Wherein the evaluation methodology of vegetable increase production rate is: timely collecting after vegetable ripeness, weighs. The computing formula of vegetable increase production rate is: vegetable increase production rate=(per mu yield of per mu yield-the do not spray medicine vegetable field of spray medicine vegetable field) �� sprays per mu yield �� 100% of medicine vegetable field.
Experimental result result is as shown in table 1.
Table 1 insect protected is tested
| Group | Preventing efficiency (%) | Vegetable increase production rate (%) |
| Embodiment 1 | 98 | 18 |
| Embodiment 2 | 94 | 15 |
| Embodiment 3 | 93 | 15 |
| Embodiment 4 | 93 | 14 |
| Comparative example 1 | 78 | 7 |
| Comparative example 2 | 80 | 8 |
| Comparative example 3 | 76 | 5 |
Embodiment 6
Vegetable prepared by above-described embodiment 1��4 is carried out insecticidal test with insecticide, method particularly includes: vegetable field aphid, Limax insect pest etc. occur monthly is sprayed 2 insecticides of the present invention, each fountain height is 20kg/ mu, and second time carries out after first time spray medicine for 3 days. With do not spray any insecticide vegetable field for reference, evaluate the insecticide of the present invention preventing efficiency on vegetable insect pest and the impact on yield of vegetables, simultaneously to spray the vegetable field of insecticide described in comparative example 1��3 for comparative example, its result is as shown in table 2.Wherein the evaluation methodology of preventing efficiency and vegetable increase production rate is with embodiment 5. Experimental result is as shown in table 2.
Table 2 insecticidal test
| Group | Preventing efficiency (%) | Vegetable increase production rate (%) |
| Embodiment 1 | 95 | 15 |
| Embodiment 2 | 91 | 11 |
| Embodiment 3 | 92 | 11 |
| Embodiment 4 | 90 | 10 |
| Comparative example 1 | 76 | 6 |
| Comparative example 2 | 76 | 5 |
| Comparative example 3 | 74 | 4 |
In the experimentation of the present embodiment, it is found by the applicant that after vegetable field aphid, Limax insect pest etc. occur is sprayed the insecticide described in the embodiment of the present invention 1��4, aphid begins in 5 minutes and runs chaotically on leaf, in 1h, the aphid of more than 85% stops running, and in 24h, the mortality rate of aphid is more than 90%. Show that insecticide of the present invention can effectively kill aphid and instant effect. But the reaction of Limax and aphid are had any different, and after spraying insecticide of the present invention, Limax climbs rapidly from leaf of vegetable, starts to drain foreign body after 2h. Show that insecticide of the present invention has what Limax was prevented and treated by strong pungent odor mainly by it.
From embodiment 5 and 6, insecticide described in embodiment 1��4 is compared with the insecticide described in comparative example 1��3, it is to the vegetable field of aphid, Limax insect pest etc. also do not occur and the preventing efficiency of vegetable field aphid, Limax insect pest etc. occur being respectively increased about 19%, and vegetable increase production rate improves about 10%. Show that in insecticide of the present invention, each raw material components is Synergistic. The preventing efficiency of the insecticide described in comparing embodiment 1��the 4 and impact of yield of vegetables is known, insecticide described in embodiment 1 is compared with the insecticide described in embodiment 2��4, it is to the vegetable field of aphid, Limax insect pest etc. also do not occur and the preventing efficiency of vegetable field aphid, Limax insect pest etc. occur being respectively increased about 4%, and vegetable increase production rate improves about 4%. Show in insecticide of the present invention that insecticide described in embodiment 1 is preferred embodiment of the invention.
Embodiment 7
Vegetable prepared by above-described embodiment 1��4 is carried out the test of liquor residue phase with insecticide: being sprayed on vegetable leaf respectively by the vegetable insecticide described in the embodiment of the present invention 1��4, fountain height is 20kg/ mu. Vegetable leaf after different time plucks spray medicine respectively, prepare leaf of vegetable extracting solution, adopting TLC-colorimetric method to measure the residual quantity of Azedarachin in detection leaf of vegetable extracting solution, agents useful for same is analytical pure, Azedarachin reference substance is chromatographically pure, and its result is as shown in table 3.
The table 3 liquor residue phase tests
As shown in Table 3, only about the 8 days Azedarachin residual period of vegetable insecticide of the present invention, also i other words the drug residue phase of vegetable insecticide of the present invention short, only about 8 days.
Embodiment 8
Vegetable prepared by above-described embodiment 1��4 is carried out animal toxicity test with insecticide: take Kunming mouse 50, male and female are use all, body weight 18��22g, is randomly divided into five groups, often group 10, the first��tetra-group of insecticide 1000mg/kg distinguished described in acute oral embodiment 1��4; BSA other acute oral commercially available pesticide (dimehypo) 350mg/kg. The death condition of mice in observing 5 days, insecticide of the present invention and the commercially available pesticide toxicity to kunming mice is evaluated with this, result draws, kunming mice is only shown low toxicity reaction by the insecticide of the embodiment of the present invention 1��4 preparation, it does not have dead mouse. And commercially available agricultural insecticide biconjugate kunming mice shows high poison reaction, 10 mices are all dead.
By embodiment 7 and 8 it can be seen that insecticide of the present invention is little to people and animals' toxic and side effects, and the liquor residue phase is short, only about 8 days, it is possible to safe handling.
Claims (10)
1. a vegetable insecticide, it is characterised in that: it is to be the medicament that raw material is prepared from by Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution, Herba Artemisiae Annuae extracting solution, white vinegar, capsicum solution.
2. vegetable insecticide according to claim 1, it is characterised in that: described Folium Artemisiae Argyi extractive liquid obtains by the following method: take Folium Artemisiae Argyi, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Folium Artemisiae Argyi extractive liquid; Described Rhizoma Iridis Japonicae extracting solution obtains by the following method: take Rhizoma Iridis Japonicae, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Rhizoma Iridis Japonicae extracting solution; Described Melia azedarach L. extracting solution obtains by the following method: take Melia azedarach L., adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain Melia azedarach L. extracting solution; Described WUDUOYUN extracting solution obtains by the following method: take WUDUOYUN, adds 2��water of 4 times of weight, and soaking at room temperature 15��40 days filters, takes filtrate, obtain WUDUOYUN extracting solution; Described Bright Yellow extracting solution obtains by the following method: take Bright Yellow, add 2��water of 4 times of weight, soaking at room temperature 15��40 days, filters, takes filtrate, obtain Bright Yellow extracting solution: described Herba Artemisiae Annuae extracting solution obtains by the following method: take Herba Artemisiae Annuae, add 2��water of 4 times of weight, soaking at room temperature 15��40 days, filters, take filtrate, obtain Herba Artemisiae Annuae extracting solution.
3. vegetable insecticide according to claim 1, it is characterised in that described capsicum solution obtains by the following method: take fresh chilli, smashs to pieces, adds 1��water of 3 times of weight, and soaking at room temperature 7��15 days filters, takes filtrate, obtain capsicum solution.
4. vegetable insecticide according to claim 1, it is characterised in that: the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 3��10 parts, Folium Artemisiae Argyi extractive liquid 3��10 parts, Melia azedarach L. extracting solution 3��10 parts, WUDUOYUN extracting solution 1��8 part, Bright Yellow extracting solution 1��8 part, Herba Artemisiae Annuae extracting solution 1��8 part, white vinegar 0.05��2 part, capsicum solution 1��4 part.
5. vegetable insecticide according to claim 4, it is characterised in that: the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 3��10 parts, Folium Artemisiae Argyi extractive liquid 4��8 parts, Melia azedarach L. extracting solution 3��9 parts, WUDUOYUN extracting solution 2��7 parts, Bright Yellow extracting solution 1��6 part, Herba Artemisiae Annuae extracting solution 2��6 parts, white vinegar 0.05��1.5 part, capsicum solution 1��3 part.
6. vegetable insecticide according to claim 5, it is characterised in that: the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 3��8 parts, Folium Artemisiae Argyi extractive liquid 4��7 parts, Melia azedarach L. extracting solution 3��9 parts, WUDUOYUN extracting solution 2��7 parts, Bright Yellow extracting solution 2��6 parts, Herba Artemisiae Annuae extracting solution 2��5 parts, white vinegar 0.08��1.0 part, capsicum solution 1��3 part.
7. vegetable insecticide according to claim 6, it is characterised in that: the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 3��7 parts, Folium Artemisiae Argyi extractive liquid 4��7 parts, Melia azedarach L. extracting solution 4��8 parts, WUDUOYUN extracting solution 2��6 parts, Bright Yellow extracting solution 2��6 parts, Herba Artemisiae Annuae extracting solution 3��5 parts, white vinegar 0.08��0.8 part, capsicum solution 1��3 part.
8. vegetable insecticide according to claim 7, it is characterised in that: the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 4��6 parts, Folium Artemisiae Argyi extractive liquid 4��7 parts, Melia azedarach L. extracting solution 5��7 parts, WUDUOYUN extracting solution 4��6 parts, Bright Yellow extracting solution 3��6 parts, Herba Artemisiae Annuae extracting solution 3��5 parts, white vinegar 0.1��0.5 part and capsicum solution 1��2 part.
9. vegetable insecticide according to claim 8, it is characterised in that: the weight of described each raw material is: Rhizoma Iridis Japonicae extracting solution 6 parts, Folium Artemisiae Argyi extractive liquid 6 parts, Melia azedarach L. extracting solution 5 parts, WUDUOYUN extracting solution 5 parts, Bright Yellow extracting solution 4 parts, Herba Artemisiae Annuae extracting solution 4 parts, white vinegar 0.2 part and capsicum solution 1.8 parts.
10. the preparation method of the vegetable insecticide as described in any one of claim 1��9, it is characterized in that, specifically comprise the following steps that by ratio of weight and the number of copies, Folium Artemisiae Argyi extractive liquid, Rhizoma Iridis Japonicae extracting solution, Melia azedarach L. extracting solution, WUDUOYUN extracting solution, Bright Yellow extracting solution and Herba Artemisiae Annuae extracting solution are mixed, it is subsequently adding white vinegar and capsicum solution, mixing, obtains vegetable insecticide.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410604954.3A CN104273184B (en) | 2014-10-30 | 2014-10-30 | A kind of vegetable insecticide and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410604954.3A CN104273184B (en) | 2014-10-30 | 2014-10-30 | A kind of vegetable insecticide and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104273184A CN104273184A (en) | 2015-01-14 |
| CN104273184B true CN104273184B (en) | 2016-06-08 |
Family
ID=52248927
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410604954.3A Active CN104273184B (en) | 2014-10-30 | 2014-10-30 | A kind of vegetable insecticide and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104273184B (en) |
Families Citing this family (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104956968A (en) * | 2015-06-29 | 2015-10-07 | 贵州黄平靓鸥桑综合开发有限公司 | Environment-friendly pest killing method for fruits and vegetables |
| CN104982467A (en) * | 2015-07-27 | 2015-10-21 | 重庆市农聚福农业发展有限公司 | Vegetable insecticide |
| CN105145674A (en) * | 2015-08-25 | 2015-12-16 | 蚌埠海上明珠农业科技发展有限公司 | Insecticide for vegetables in subsidiary agricultural products and preparation method of insecticide |
| CN105410057A (en) * | 2015-12-09 | 2016-03-23 | 防城港市星湖生态农业有限公司 | Syzygium samarangense pest control pesticide |
| CN106069466A (en) * | 2016-06-13 | 2016-11-09 | 普定县宏峰养殖专业合作社 | A kind of Semen Juglandis implantation methods |
| CN106083247A (en) * | 2016-06-13 | 2016-11-09 | 普定县宏峰养殖专业合作社 | A kind of Fructus Pruni salicinae implantation methods |
| CN106069019A (en) * | 2016-06-16 | 2016-11-09 | 贵州省石阡和记绿色食品开发有限公司 | A kind of pepper seedling raising method |
| CN105875174A (en) * | 2016-06-16 | 2016-08-24 | 贵州省石阡和记绿色食品开发有限公司 | Chili planting method |
| CN106069495A (en) * | 2016-06-20 | 2016-11-09 | 普定县持恒林业科技发展有限公司 | A kind of dahoon tree method for culturing seedlings |
| CN106105936A (en) * | 2016-06-20 | 2016-11-16 | 普定县持恒林业科技发展有限公司 | A kind of shuttle sieve Fructus Persicae implantation methods |
| CN106069496A (en) * | 2016-06-20 | 2016-11-09 | 普定县持恒林业科技发展有限公司 | A kind of Yew cuttage method for culturing seedlings |
| CN106069497A (en) * | 2016-06-20 | 2016-11-09 | 普定县持恒林业科技发展有限公司 | A kind of red light Fructus Pruni pseudocerasi implantation methods |
| CN106069498A (en) * | 2016-06-20 | 2016-11-09 | 普定县持恒林业科技发展有限公司 | A kind of shuttle sieve Fructus Persicae method for culturing seedlings |
| CN106069329A (en) * | 2016-06-22 | 2016-11-09 | 贵州省石阡和记绿色食品开发有限公司 | A kind of pepper seedling raising medium and preparation method thereof |
| CN105993550A (en) * | 2016-06-22 | 2016-10-12 | 贵州省石阡和记绿色食品开发有限公司 | Method for interplanting chilies and sweet wormwood herbs |
| CN106172514A (en) * | 2016-07-13 | 2016-12-07 | 肖兵兵 | Bamboo sprout insecticide |
| CN106171450A (en) * | 2016-07-24 | 2016-12-07 | 普定县瑞鸿生产力促进有限责任公司 | A kind of Rhizoma Pinelliae implantation methods |
| CN106258433A (en) * | 2016-08-19 | 2017-01-04 | 铜仁市金农绿色农业科技有限公司 | A kind of Herba Dendrobii implantation methods |
| CN106305383A (en) * | 2016-08-19 | 2017-01-11 | 铜仁市金农绿色农业科技有限公司 | Dendrobium candidumseedling exercising method |
| CN106278676A (en) * | 2016-08-23 | 2017-01-04 | 广西易多收生物科技有限公司 | One comprises neires toxin medicine fertilizer composition and preparation method thereof |
| CN106316617A (en) * | 2016-08-23 | 2017-01-11 | 广西易多收生物科技有限公司 | Organic fertilizer with bacillus subtilis and preparing method thereof |
| CN106857084A (en) * | 2017-01-05 | 2017-06-20 | 陆川县米场镇合美种养专业合作社联合社 | A kind of method for culturing seedlings of insect prevention selenium-rich rice |
| CN107950593A (en) * | 2017-11-16 | 2018-04-24 | 平昌县得胜小学 | A kind of vegetables insecticide and preparation method thereof |
| CN108041089A (en) * | 2018-01-15 | 2018-05-18 | 东北林业大学 | A kind of Almightiness type environmental-pollution insecticide and preparation method thereof |
| CN108308208A (en) * | 2018-04-09 | 2018-07-24 | 何新桥 | A kind of nontoxic insectifuge for crops and preparation method thereof and use |
| CN109258714A (en) * | 2018-10-30 | 2019-01-25 | 大新县科学技术情报研究所 | A kind of biological insecticides and preparation method thereof for preventing and treating vegetable aphid |
| CN109258724A (en) * | 2018-11-02 | 2019-01-25 | 万物生（深圳）生物科技控股有限公司 | A kind of biological pesticide pest repellant |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1183902A (en) * | 1996-11-28 | 1998-06-10 | 阎福永 | Plant protecting agent |
| CN1220984A (en) * | 1997-12-26 | 1999-06-30 | 佟立明 | Multifunction fertilizer |
| CN101485338A (en) * | 2008-01-18 | 2009-07-22 | 邹如 | Green food pesticide composition and uses thereof |
-
2014
- 2014-10-30 CN CN201410604954.3A patent/CN104273184B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1183902A (en) * | 1996-11-28 | 1998-06-10 | 阎福永 | Plant protecting agent |
| CN1220984A (en) * | 1997-12-26 | 1999-06-30 | 佟立明 | Multifunction fertilizer |
| CN101485338A (en) * | 2008-01-18 | 2009-07-22 | 邹如 | Green food pesticide composition and uses thereof |
Non-Patent Citations (1)
| Title |
|---|
| 植物杀虫剂资源的开发应用于保护;罗伯良;《湖南林业科技》;20000331;第27卷(第1期);第59-63页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104273184A (en) | 2015-01-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104273184B (en) | A kind of vegetable insecticide and preparation method thereof | |
| CN103931686B (en) | A kind of botanical pesticide and its preparation method and application | |
| CN104855442B (en) | For preventing and treating plant pathogeny line insect medicine fertilizer and application process | |
| CN102754667B (en) | High-efficiency composite botanical pesticide | |
| EP0600080A4 (en) | Organic pesticide. | |
| CN101427692B (en) | Plant pesticide and preparation method thereof | |
| JPH10245312A (en) | Plant protecting agent and its production | |
| CN105475376A (en) | Natural plant bactericide for controlling dendrobium insect diseases | |
| CN101116451A (en) | Plant miticide derived from artemisia annul l and method for preparing the same | |
| CN106417289A (en) | Pesticide for preventing and controlling litchi whiteflies and preparation method thereof | |
| CN100411523C (en) | Compound pesticide of triperygium wilfordii alkaloid | |
| CN105360182A (en) | Pesticide for soybeans and preparation method of pesticide | |
| CN107873743A (en) | Plant insecticide containing selfheal and preparation method thereof | |
| CN106332919A (en) | Pesticide for preventing Arbela dea and preparing method thereof | |
| CN107950593A (en) | A kind of vegetables insecticide and preparation method thereof | |
| CN105394106A (en) | Compound pesticide for preventing and treating oilseed rape aphids and preparation method thereof | |
| CN108935538A (en) | A kind of agriculture and forestry control of insect liquid pesticidal and its making and use method | |
| CN106342935A (en) | Pesticide for preventing and treating litchi spotted cerambycid and preparation method thereof | |
| CN103300076A (en) | Insect repellent and preparation method thereof | |
| CN107593788A (en) | A kind of botanical pesticide reagent for preventing and treating landscape flower pest and disease damage and preparation method thereof | |
| CN106332918A (en) | Pesticide for preventing olethreutes leucaspis meyrick in litchi and preparing method thereof | |
| CN106342936A (en) | Pesticide for preventing and treating Oligonychus litchii and preparation method thereof | |
| CN109528961A (en) | A kind of Chinese herbal medicine pesticide for killing pig endoparasite | |
| CN108496994B (en) | Citrus psylla repelling and killing composition and preparation method thereof | |
| CN107372682A (en) | A kind of ornamental plant desinsection environment-protection pesticide and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20201204 Address after: NO.666 Huaihe Road, Huangzhen high tech chemical industry park, Mudan District, Heze City, Shandong Province Patentee after: Shandong Tiandao Bioengineering Co., Ltd Address before: 636472, Ma On Street, Desheng Town, Pingchang County, Bazhong, Sichuan, 47 Patentee before: Zhang Jincheng Patentee before: Wang Meiyi |