CN104262981A - Wood fiber with flame-retardant and waterproof effects and preparation method thereof - Google Patents

Abstract

The invention discloses a wood fiber with flame-retardant and waterproof effects. The wood fiber is characterized by being prepared from the following raw materials in pats by weight: 38-45 parts of wood fibers, 5-8 parts of PP (Polyproylene) fibers, 15-18 parts of ramie fibers, 10-12 parts of pineapple fibers, 10-13 parts of glass fibers, 0.2-0.5 part of hydroxypropyl methyl cellulose, 7-9 parts of hydrogenated rosin, 2-4 parts of clove oil, 3-6 parts of a styrene-acrylic emulsion, 8-10 parts of triphenyl phosphate, 0.4-0.7 part of cetyl trimethyl ammonium bromide, 1-3 parts of diatomite, 11-14 parts of rice hulls, 2-3 parts of radix paeoniae alba, 1-4 parts of bighead atractylodes rhizome, 2-5 parts of auxiliaries and a proper amount of water. The wood fiber disclosed by the invention is simple to prepare and operate and wide in source of raw materials. By mutually compounding the beneficial components of triphenyl phosphate, ramie fibers and pineapple fibers and the like, and the prepared wood fiber has the advantages of flame retardance, sweat absorption and ventilation and water prevention and the like. Compared with the wood fiber in the prior art, the product prepared by the wood fiber is more excellent.

Description

A kind of have xylon of fire-resistant waterproof effect and preparation method thereof

Technical field

The present invention relates to a kind of xylon modification field, be specifically related to a kind of to there is xylon of fire-resistant waterproof effect and preparation method thereof.

Background technology

Pure natural wood fiber product is the same with cotton be all 100% green product, there is natural antibiotic health care, remove peculiar smell, from self-cleaning clearly function, soft-touch, does not harden hardening, be one real, the healthy products of pure green.Therefore the extremely popular favor of pure natural xylon, is widely used in the fields such as towel, underwear, T-shirt, kitchen towel, socks, shirt, Western-style clothes, baby's textiles, bedclothes, curtain, fabric, bedding and padding.

In prior art, xylon is inflammable exists many weak points: because xylon has the water absorbability more superior than cotton fibre and ventilation property, therefore apt to rot time for being processed into fiberboard, easy conductive, inflammable etc., and xylon is compared to comparatively hard for quality time knitting cotton fibre, sense of touch is poor; Secondly, because time prepared by xylon, starting material are limited, and existing life multiple demands etc. cannot be met, so xylon is restricted in its use range of a very long time.

Summary of the invention

Object of the present invention is just to provide a kind ofly has xylon of fire-resistant waterproof effect and preparation method thereof, to overcome the deficiencies in the prior art.

The object of the present invention is achieved like this:

A kind of xylon with fire-resistant waterproof effect, it is characterized in that, be made up of the raw material of following weight part: xylon 38-45, PP fiber 5-8, ramee 15-18, pina fibre 10-12, glass fibre 10-13, Vltra tears 0.2-0.5, staybelite 7-9, Syzygium aromaticum stem oil 2-4, benzene emulsion 3-6, triphenylphosphate 8-10, cetyl trimethylammonium bromide 0.4-0.7, diatomite 1-3, rice husk 11-14, root of herbaceous peony 2-3, bighead atractylodes rhizome 1-4, auxiliary agent 2-5, suitable quantity of water.

Described auxiliary agent is made up of following raw materials in part by weight: tealeaves fiber 10-13, nano zine oxide 2-4, silicon powder 1-3, dual polyethylene polydimethylsiloxane 0.03-0.05, glyceryl monostearate 1.2-3.1, polyoxyethylene glycol 3-6, methylisothiazolinone 2.1-3.6, Oleum Pelargonii Graveolentis 3.2-4.7, Flos Pelargonii Hortori 0.2-0.4, linolic acid 1.3-2.4, Dyhard RU 100 0.1-0.2, ethyl acrylate 4-7, fire retardant CP 0.04-0.07, its preparation method be first by nano zine oxide ultrasonic disperse in polyoxyethylene glycol, add tealeaves blending in of fibers and stir 5-8 hour, take out drying and grinding 10-15 minute, obtained modification tealeaves fiber, then by Oleum Pelargonii Graveolentis, Flos Pelargonii Hortori adds water stirring, and add silicon powder and stir 30-40 minute, spraying dry obtains modified silicon micro mist, finally by ethyl acrylate, linolic acid, Dyhard RU 100, methylisothiazolinone stirring and evenly mixing, adds above-mentioned obtained modification tealeaves fiber and modified silicon micro mist, glyceryl monostearate, dual polyethylene polydimethylsiloxane, fire retardant CP supersound process 30-40 minute and get final product.

Described a kind of preparation method with the xylon of fire-resistant waterproof effect, is characterized in that comprising the following steps:

(1) add water after getting rice husk, the root of herbaceous peony, the bighead atractylodes rhizome pulverizing boiling pulping, adds Vltra tears agitation grinding 20-30 minute, send in defibrator and be processed into modified composite fiber;

(2) diatomite is put into calcining furnace pyroprocessing 20-40 minute, add PP fiber stirring and evenly mixing while hot, cooling grinding 10-15 minute obtained modification infusorial earth;

(3) by staybelite, Syzygium aromaticum stem oil heated and stirred, add triphenylphosphate and stir 5-8 minute, add benzene emulsion, cetyl trimethylammonium bromide, modification infusorial earth supersound process 20-40 minute;

(4) xylon, ramee, pina fibre, glass fibre, modified composite fiber are put into pulverizing mill and worn into 80-100 order powder, putting into high mixer after drying mixes to 80-90 DEG C, add step (3) reaction product and remaining component is mixed to 100-120 DEG C, leave standstill supersound process 10-15 minute after 15-20 hour, wash, filter, dry to constant weight and get final product.

The present invention has following beneficial effect: it is simple that the present invention prepares ease of Use, raw material sources are wide, add the mutual compounds of beneficiating ingredient such as triphenylphosphate, ramee, pina fibre, obtained xylon has the advantages such as fire-retardant, absorbing sweat ventilative, waterproof, and the product utilizing the present invention to obtain is more excellent than the xylon performance of prior art.

Embodiment

Described a kind of xylon with fire-resistant waterproof effect, it is characterized in that, be made up of the raw material of following weight part: xylon 39, PP fiber 6, ramee 17, pina fibre 11, glass fibre 12, Vltra tears 0.2, staybelite 7, Syzygium aromaticum stem oil 4, benzene emulsion 3, triphenylphosphate 8, cetyl trimethylammonium bromide 0.6, diatomite 1, rice husk 13, the root of herbaceous peony 2, the bighead atractylodes rhizome 4, auxiliary agent 2, suitable quantity of water.

Described auxiliary agent is made up of following raw materials in part by weight: tealeaves fiber 12, nano zine oxide 2, silicon powder 1, dual polyethylene polydimethylsiloxane 0.05, glyceryl monostearate 1.9, polyoxyethylene glycol 4, methylisothiazolinone 2.8, Oleum Pelargonii Graveolentis 4.5, Flos Pelargonii Hortori 0.3, linolic acid 1.9, Dyhard RU 100 0.1, ethyl acrylate 4, fire retardant CP 0.07, its preparation method be first by nano zine oxide ultrasonic disperse in polyoxyethylene glycol, add tealeaves blending in of fibers and stir 5-8 hour, take out drying and grinding 10-15 minute, obtained modification tealeaves fiber, then by Oleum Pelargonii Graveolentis, Flos Pelargonii Hortori adds water stirring, and add silicon powder and stir 30-40 minute, spraying dry obtains modified silicon micro mist, finally by ethyl acrylate, linolic acid, Dyhard RU 100, methylisothiazolinone stirring and evenly mixing, adds above-mentioned obtained modification tealeaves fiber and modified silicon micro mist, glyceryl monostearate, dual polyethylene polydimethylsiloxane, fire retardant CP supersound process 30-40 minute and get final product.

Making method comprises the following steps:

(1) add water after getting rice husk, the root of herbaceous peony, the bighead atractylodes rhizome pulverizing boiling pulping, adds Vltra tears agitation grinding 20-30 minute, send in defibrator and be processed into modified composite fiber;

(2) diatomite is put into calcining furnace pyroprocessing 20-40 minute, add PP fiber stirring and evenly mixing while hot, cooling grinding 10-15 minute obtained modification infusorial earth;

(3) by staybelite, Syzygium aromaticum stem oil heated and stirred, add triphenylphosphate and stir 5-8 minute, add benzene emulsion, cetyl trimethylammonium bromide, modification infusorial earth supersound process 20-40 minute;

(4) xylon, ramee, pina fibre, glass fibre, modified composite fiber are put into pulverizing mill and worn into 80-100 order powder, putting into high mixer after drying mixes to 80-90 DEG C, add step (3) reaction product and remaining component is mixed to 100-120 DEG C, leave standstill supersound process 10-15 minute after 15-20 hour, wash, filter, dry to constant weight and get final product.

The technical parameter index of the xylon using the present invention to produce is as follows:

(1) soft fluffy smooth flexible, intensity is high;

(2) oxygen index (OI): 27.5%, flame retardant effect is excellent;

(3) bacteriostasis rate of finished product to intestinal bacteria, streptococcus aureus, Candida albicans is all greater than 99.7%.

Claims (2)

1. one kind has the xylon of fire-resistant waterproof effect, it is characterized in that, be made up of the raw material of following weight part: xylon 38-45, PP fiber 5-8, ramee 15-18, pina fibre 10-12, glass fibre 10-13, Vltra tears 0.2-0.5, staybelite 7-9, Syzygium aromaticum stem oil 2-4, benzene emulsion 3-6, triphenylphosphate 8-10, cetyl trimethylammonium bromide 0.4-0.7, diatomite 1-3, rice husk 11-14, root of herbaceous peony 2-3, bighead atractylodes rhizome 1-4, auxiliary agent 2-5, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: tealeaves fiber 10-13, nano zine oxide 2-4, silicon powder 1-3, dual polyethylene polydimethylsiloxane 0.03-0.05, glyceryl monostearate 1.2-3.1, polyoxyethylene glycol 3-6, methylisothiazolinone 2.1-3.6, Oleum Pelargonii Graveolentis 3.2-4.7, Flos Pelargonii Hortori 0.2-0.4, linolic acid 1.3-2.4, Dyhard RU 100 0.1-0.2, ethyl acrylate 4-7, fire retardant CP 0.04-0.07, its preparation method be first by nano zine oxide ultrasonic disperse in polyoxyethylene glycol, add tealeaves blending in of fibers and stir 5-8 hour, take out drying and grinding 10-15 minute, obtained modification tealeaves fiber, then by Oleum Pelargonii Graveolentis, Flos Pelargonii Hortori adds water stirring, and add silicon powder and stir 30-40 minute, spraying dry obtains modified silicon micro mist, finally by ethyl acrylate, linolic acid, Dyhard RU 100, methylisothiazolinone stirring and evenly mixing, adds above-mentioned obtained modification tealeaves fiber and modified silicon micro mist, glyceryl monostearate, dual polyethylene polydimethylsiloxane, fire retardant CP supersound process 30-40 minute and get final product.

2. a kind of making method with the xylon of fire-resistant waterproof effect according to claim 1, is characterized in that comprising the following steps:

(1) add water after getting rice husk, the root of herbaceous peony, the bighead atractylodes rhizome pulverizing boiling pulping, adds Vltra tears agitation grinding 20-30 minute, send in defibrator and be processed into modified composite fiber;

(2) diatomite is put into calcining furnace pyroprocessing 20-40 minute, add PP fiber stirring and evenly mixing while hot, cooling grinding 10-15 minute obtained modification infusorial earth;

(3) by staybelite, Syzygium aromaticum stem oil heated and stirred, add triphenylphosphate and stir 5-8 minute, add benzene emulsion, cetyl trimethylammonium bromide, modification infusorial earth supersound process 20-40 minute;

(4) xylon, ramee, pina fibre, glass fibre, modified composite fiber are put into pulverizing mill and worn into 80-100 order powder, putting into high mixer after drying mixes to 80-90 DEG C, add step (3) reaction product and remaining component is mixed to 100-120 DEG C, leave standstill supersound process 10-15 minute after 15-20 hour, wash, filter, dry to constant weight and get final product.