CN104233825A - Environment-friendly silk printing method - Google Patents
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- CN104233825A CN104233825A CN201410446475.3A CN201410446475A CN104233825A CN 104233825 A CN104233825 A CN 104233825A CN 201410446475 A CN201410446475 A CN 201410446475A CN 104233825 A CN104233825 A CN 104233825A
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Abstract
The invention discloses an environment-friendly silk printing method, which comprises the following steps: (1) performing enzyme pretreatment on a fabric, namely putting the silk fabric subjected to degumming and tentering into an enzyme solution for pretreatment; (2) performing sizing; (3) drying; (4) making a document, wherein jet printing is generated by color card software, and ink for the jet printing is regenerative reactive dye-based ink; (5) performing jet printing; (6) steaming and drying; (7) washing, namely washing with cold water, then soaping, and washing with cold water again; and (8) performing tentering drying.
Description
Technical field
The present invention relates to a kind of environmental protection real silk printing method, particularly relate to the real silk printing method using enzyme auxiliary agent.
Background technology
Digital ink-jet printed is the printing technique developed rapidly in recent years, be by the ink containing pigment under compressed-air actuated driving, be ejected on fabric by nozzle, controlled on fabric, to form floral designs by designing requirement by computer, according to the performance of ink set, through suitable post processing, fabric is made to have certain COLOR FASTNESS and vividness.Real silk fabric requires higher to stamp fineness, preliminary treatment is carried out to fabric extremely important to reduce the imbibition degree of ink on fabric, the imbibition process of ink on fabric can be divided into two parts, one be ink-jet printed print time imbibition, two is the imbibitions produced in steaming procedure.Therefore need to carry out starching preliminary treatment to fabric before ink-jet printed, generally select sodium alginate as thickener, add urea as hygroscopic agent, reduce ink on fabric to surrounding imbibition, have better printing effect, but after spray printing, the color of fabric is more shallow.And need in printing with reactive dye process to add a large amount of urea, play hydrotropy effect on the one hand, play moisture absorption and Swelling Functions on the other hand, the moisture pinned can be discharged when decatize, for dyestuff and fiber set provide advantage, and make fiber fully swelling and accelerate dyestuff set.But urea enters in water, natural decomposition becomes carbon dioxide and nitrogen-containing compound, and the latter can accelerate the growth of algae substances, finally causes Water Eutrophication phenomenon, is one of COD and ammonia nitrogen pollutant main source.
Rise on January 1st, 2013 in the new edition GB 4287-2012 " textile dyeing and finishing industrial water pollution thing discharge standard " of enforcement and improve pollutant emission control overflow, wherein strict special emission limit has all been done to ammonia nitrogen, total nitrogen content and COD.Therefore, the colouring method improving dye utilization rate, reduce urea, improve coloring degree is badly in need of.
Enzyme is a kind of pure biologic product, health environment-friendly noresidue, and ferment treatment temperature is low, less energy consumption, can not environmental pollution be caused, belong to green technology, had people that enzyme is used for textile applications, but enzyme is strong as a kind of substrate specificity, high pure biologic product is required to reaction environment, now its to be applied to natural fabric process also very immature, there is many problems, range of application is wideless.
The present invention aims to provide a kind of real silk reactive printing method of conbined usage biology enzyme and shitosan, and passes through the lot of experiment validation the most optimized parameter of technique, and such technique have not been reported.
Summary of the invention
Based on the technical problem that background technology exists, the present invention is directed to the shortcoming of current real silk reactive printing, provide a kind of newly, fully combine the real silk reactive printing technique utilizing biology enzyme and shitosan.
Biology enzyme used by the present invention mainly contains two kinds, papain and cellulase.
Papain is the neutral protease utilizing the milk in immature papaya fruit to refine, belong to peptide protease in sulfydryl, there is wider substrate specificity, act on the peptide bond that L-arginine in protein, 1B, glycine and Cit residue carboxyl participate in being formed, the polypeptide class of holoprotein intramolecule peptide chain-CO-NH-generation molecular weight can be cut, be applied to the process such as medicine, food, feed, leather and weaving.
Cellulase is a kind of complex enzyme, and the cellulase that the present invention adopts is the commercial enzyme of Su Kehan bioengineering Co., Ltd.
Technical scheme of the present invention is as follows:
A kind of environmental protection real silk reactive printing method, its step is as follows:
(1) fabric enzyme preliminary treatment: the real silk fabric after the tentering that comes unstuck is dropped in enzyme solutions and carries out preliminary treatment;
(2) starching: the pretreated real silk fabric of enzyme, starching machine carries out back starching,
(3) dry: adopt infrared drying device, its bake out temperature is 80 ~ 120 DEG C, drying time 3 ~ 5min;
(4) file is made: described spray printing is by colour atla Software Create, and print conditions is: printing precision 360 × 2160dpi, 360 × 2160 6pass CMYK, and spray printing ink used is regeneration activity dye ink;
(5) spray printing: D-2200 code ink jet printing machine carries out spray printing;
(6) decatize is dried;
(7) wash: after cold wash, soap, then carry out a cold wash, described soaping is 10min under 80 DEG C of conditions, and soaping agent is modification Tea Saponin 2 ~ 10g/L.
(8) tentering is dried;
Described step 1 enzyme treatment process condition is: papain 15 ~ 18U/mL, cellulase 3 ~ 5U/mL, pH7, temperature 40 DEG C, time 1h, bath raio 1: 10, and after process, clear water is cleaned air-dry;
Described step 2 slurry is composed as follows by weight percentage:
Surplus is water; Described moisture absorption swelling agent is the mixture of urea, triethylene glycol;
Decatize described in described step 3 is react fixation 30 ~ 50min under 100 ~ 110 DEG C of saturated steam conditions.
Usefulness of the present invention is:
1, there is good K/S value, degree of fixation and wet colour fastness, and improve the utilization rate of reactive dye ink;
2, reduce further the amount of urea in real silk reactive printing process, alleviate blowdown and the sewage disposal burden that causes;
3, printing color is bright-coloured, true to nature;
4, ferment treatment temperature is low, less energy consumption, can not cause environmental pollution, belongs to green technology.
Detailed description of the invention
Embodiment 1:
(1) fabric enzyme preliminary treatment: the real silk fabric after the tentering that comes unstuck is dropped in enzyme solutions and carries out preliminary treatment, enzyme treatment process condition is: papain 15U/mL, cellulase 3U/mL, pH7, temperature 40 DEG C, time 1h, bath raio 1: 10, and after process, clear water is cleaned air-dry;
(2) starching: the pretreated real silk fabric of enzyme, starching machine carries out back starching, and its slurry is composed as follows by weight percentage:
Surplus is water;
Described moisture absorption swelling agent is urea and triethylene glycol mass ratio is 3:7
(3) dry: adopt infrared drying device, its bake out temperature is 100 DEG C, drying time 5min;
(4) file is made: described spray printing is by colour atla Software Create, and print conditions is: printing precision 360 × 2160dpi, 360 × 2160 6pass CMYK, and spray printing ink used is regeneration activity dye ink;
(5) spray printing: D-2200 code ink jet printing machine carries out spray printing;
(6) decatize is dried: decatize is react fixation 30 ~ 50min under 100 ~ 110 DEG C of saturated steam conditions
(7) wash: after cold wash, soap, then carry out a cold wash, described soaping is 10min under 80 DEG C of conditions, and soaping agent is modification Tea Saponin 2 ~ 10g/L;
(8) tentering is dried.
The fabric that said method arranged is tested.
Color fastness to washing: measure with reference to GB/T 3921.1-1997 " textile color stability test color fastness to washing: test 1 ", adopt the test of SW 212 type color fastness to washing experiment instrument.
Light fastness: measure with reference to GB/T 8427-1998 " textile color stability tests resistance to artificial light COLOR FASTNESS: xenon arc ", adopts ATLAS-150 light fastness tester.
Fastness to rubbing: measure with reference to GB/T 3921.1-1997 " textile color stability test fastness to rubbing: test 1 ", adopt the test of Y571A crock fastness machine.
K/S value: adopting Datacolor SF-600 to survey color matching system is that under the condition of 20mm and light source D65/10 °, multi-point sampler fabric is in the dye level K/S value of maximum absorption wave strong point in aperture.
Result shows: color fastness to washing is 5 (cotton is stained with), and light fastness is 4, and fastness to rubbing is dry grinding 5, and wet and rub 4, dye level K/S is 12.38, staining 5 grades, degree of fixation 96.28%;
From sense organ, printing effect is true to nature, bright-colored.
Embodiment 2:
(1) fabric enzyme preliminary treatment: the real silk fabric after the tentering that comes unstuck is dropped in enzyme solutions and carries out preliminary treatment, enzyme treatment process condition is: papain 16U/mL, cellulase 4U/mL, pH7, temperature 40 DEG C, time 1h, bath raio 1: 10, and after process, clear water is cleaned air-dry;
(2) starching: the pretreated real silk fabric of enzyme, starching machine carries out back starching, and its slurry is composed as follows by weight percentage:
Surplus is water;
Described moisture absorption swelling agent is urea and triethylene glycol mass ratio is 2:8
(3) dry: adopt infrared drying device, its bake out temperature is 100 DEG C, drying time 5min;
(4) file is made: described spray printing is by colour atla Software Create, and print conditions is: printing precision 360 × 2160dpi, 360 × 2160 6pass CMYK, and spray printing ink used is regeneration activity dye ink;
(5) spray printing: D-2200 code ink jet printing machine carries out spray printing;
(6) decatize is dried: decatize is react fixation 30 ~ 50min under 100 ~ 110 DEG C of saturated steam conditions
(7) wash: after cold wash, soap, then carry out a cold wash, described soaping is 10min under 80 DEG C of conditions, and soaping agent is modification Tea Saponin 2 ~ 10g/L;
(8) tentering is dried.
The fabric that said method arranged is tested.
Color fastness to washing: measure with reference to GB/T 3921.1-1997 " textile color stability test color fastness to washing: test 1 ", adopt the test of SW 212 type color fastness to washing experiment instrument.
Light fastness: measure with reference to GB/T 8427-1998 " textile color stability tests resistance to artificial light COLOR FASTNESS: xenon arc ", adopts ATLAS-150 light fastness tester.
Fastness to rubbing: measure with reference to GB/T 3921.1-1997 " textile color stability test fastness to rubbing: test 1 ", adopt the test of Y571A crock fastness machine.
K/S value: adopting Datacolor SF-600 to survey color matching system is that under the condition of 20mm and light source D65/10 °, multi-point sampler fabric is in the dye level K/S value of maximum absorption wave strong point in aperture.
Result shows: color fastness to washing is 5 (cotton is stained with), and light fastness is 4, and fastness to rubbing is dry grinding 5, and wet and rub 4, dye level K/S is 12.35, staining 5 grades, degree of fixation 96.35%;
From sense organ, printing effect is true to nature, bright-colored.
Embodiment 3:
(1) fabric enzyme preliminary treatment: the real silk fabric after the tentering that comes unstuck is dropped in enzyme solutions and carries out preliminary treatment, enzyme treatment process condition is: papain 17U/mL, cellulase 5U/mL, pH7, temperature 40 DEG C, time 1h, bath raio 1: 10, and after process, clear water is cleaned air-dry;
(2) starching: the pretreated real silk fabric of enzyme, starching machine carries out back starching, and its slurry is composed as follows by weight percentage:
Surplus is water;
Described moisture absorption swelling agent is urea and triethylene glycol mass ratio is 4:6
(3) dry: adopt infrared drying device, its bake out temperature is 100 DEG C, drying time 5min;
(4) file is made: described spray printing is by colour atla Software Create, and print conditions is: printing precision 360 × 2160dpi, 360 × 2160 6pass CMYK, and spray printing ink used is regeneration activity dye ink;
(5) spray printing: D-2200 code ink jet printing machine carries out spray printing;
(6) decatize is dried: decatize is react fixation 30 ~ 50min under 100 ~ 110 DEG C of saturated steam conditions
(7) wash: after cold wash, soap, then carry out a cold wash, described soaping is 10min under 80 DEG C of conditions, and soaping agent is modification Tea Saponin 2 ~ 10g/L;
(8) tentering is dried.
The fabric that said method arranged is tested.
Color fastness to washing: measure with reference to GB/T 3921.1-1997 " textile color stability test color fastness to washing: test 1 ", adopt the test of SW 212 type color fastness to washing experiment instrument.
Light fastness: measure with reference to GB/T 8427-1998 " textile color stability tests resistance to artificial light COLOR FASTNESS: xenon arc ", adopts ATLAS-150 light fastness tester.
Fastness to rubbing: measure with reference to GB/T 3921.1-1997 " textile color stability test fastness to rubbing: test 1 ", adopt the test of Y571A crock fastness machine.
K/S value: adopting Datacolor SF-600 to survey color matching system is that under the condition of 20mm and light source D65/10 °, multi-point sampler fabric is in the dye level K/S value of maximum absorption wave strong point in aperture.
Result shows: color fastness to washing is 5 (cotton is stained with), and light fastness is 4, and fastness to rubbing is dry grinding 5, and wet and rub 4, dye level K/S is 12.56, staining 5 grades, degree of fixation 97.12%;
From sense organ, printing effect is true to nature, bright-colored.
Embodiment 4:
(1) fabric enzyme preliminary treatment: the real silk fabric after the tentering that comes unstuck is dropped in enzyme solutions and carries out preliminary treatment, enzyme treatment process condition is: papain 18U/mL, cellulase 5U/mL, pH7, temperature 40 DEG C, time 1h, bath raio 1: 10, and after process, clear water is cleaned air-dry;
(2) starching: the pretreated real silk fabric of enzyme, starching machine carries out back starching, and its slurry is composed as follows by weight percentage:
Surplus is water;
Described moisture absorption swelling agent is urea and triethylene glycol mass ratio is 3:7
(3) dry: adopt infrared drying device, its bake out temperature is 100 DEG C, drying time 5min;
(4) file is made: described spray printing is by colour atla Software Create, and print conditions is: printing precision 360 × 2160dpi, 360 × 2160 6pass CMYK, and spray printing ink used is regeneration activity dye ink;
(5) spray printing: D-2200 code ink jet printing machine carries out spray printing;
(6) decatize is dried: decatize is react fixation 30 ~ 50min under 100 ~ 110 DEG C of saturated steam conditions
(7) wash: after cold wash, soap, then carry out a cold wash, described soaping is 10min under 80 DEG C of conditions, and soaping agent is modification Tea Saponin 2 ~ 10g/L;
(8) tentering is dried.
The fabric that said method arranged is tested.
Color fastness to washing: measure with reference to GB/T 3921.1-1997 " textile color stability test color fastness to washing: test 1 ", adopt the test of SW 212 type color fastness to washing experiment instrument.
Light fastness: measure with reference to GB/T 8427-1998 " textile color stability tests resistance to artificial light COLOR FASTNESS: xenon arc ", adopts ATLAS-150 light fastness tester.
Fastness to rubbing: measure with reference to GB/T 3921.1-1997 " textile color stability test fastness to rubbing: test 1 ", adopt the test of Y571A crock fastness machine.
K/S value: adopting Datacolor SF-600 to survey color matching system is that under the condition of 20mm and light source D65/10 °, multi-point sampler fabric is in the dye level K/S value of maximum absorption wave strong point in aperture.
Result shows: color fastness to washing is 5 (cotton is stained with), and light fastness is 4, and fastness to rubbing is dry grinding 5, and wet and rub 4, dye level K/S is 12.39, staining 5 grades, degree of fixation 96.81%;
From sense organ, printing effect is true to nature, bright-colored.
Embodiment 5:
(1) fabric enzyme preliminary treatment: the real silk fabric after the tentering that comes unstuck is dropped in enzyme solutions and carries out preliminary treatment, enzyme treatment process condition is: papain 18U/mL, cellulase 3U/mL, pH7, temperature 40 DEG C, time 1h, bath raio 1: 10, and after process, clear water is cleaned air-dry;
(2) starching: the pretreated real silk fabric of enzyme, starching machine carries out back starching, and its slurry is composed as follows by weight percentage:
Surplus is water;
Described moisture absorption swelling agent is urea and triethylene glycol mass ratio is 2:8
(3) dry: adopt infrared drying device, its bake out temperature is 100 DEG C, drying time 5min;
(4) file is made: described spray printing is by colour atla Software Create, and print conditions is: printing precision 360 × 2160dpi, 360 × 2160 6pass CMYK, and spray printing ink used is regeneration activity dye ink;
(5) spray printing: D-2200 code ink jet printing machine carries out spray printing;
(6) decatize is dried: decatize is react fixation 30 ~ 50min under 100 ~ 110 DEG C of saturated steam conditions
(7) wash: after cold wash, soap, then carry out a cold wash, described soaping is 10min under 80 DEG C of conditions, and soaping agent is modification Tea Saponin 2 ~ 10g/L;
(8) tentering is dried.
The fabric that said method arranged is tested.
Color fastness to washing: measure with reference to GB/T 3921.1-1997 " textile color stability test color fastness to washing: test 1 ", adopt the test of SW 212 type color fastness to washing experiment instrument.
Light fastness: measure with reference to GB/T 8427-1998 " textile color stability tests resistance to artificial light COLOR FASTNESS: xenon arc ", adopts ATLAS-150 light fastness tester.
Fastness to rubbing: measure with reference to GB/T 3921.1-1997 " textile color stability test fastness to rubbing: test 1 ", adopt the test of Y571A crock fastness machine.
K/S value: adopting Datacolor SF-600 to survey color matching system is that under the condition of 20mm and light source D65/10 °, multi-point sampler fabric is in the dye level K/S value of maximum absorption wave strong point in aperture.
Result shows: color fastness to washing is 5 (cotton is stained with), and light fastness is 4, and fastness to rubbing is dry grinding 5, and wet and rub 4, dye level K/S is 12.53, staining 5 grades, degree of fixation 96.77%;
From sense organ, printing effect is true to nature, bright-colored.
The active printing process of real silk of the present invention, take full advantage of enzyme and shitosan, treatment temperature is low, less energy consumption, can not cause environmental pollution, and more common low urea real silk stamp, its printing color is bright-coloured, true to nature, and has good K/S value, degree of fixation and wet colour fastness, and improve the utilization rate of reactive dye ink, be a kind of very outstanding novel environment friendly real silk printing method.
The above; be only the present invention's preferably detailed description of the invention; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (2)
1. an environmental protection real silk reactive printing method, is characterized in that step is as follows:
(1) fabric enzyme preliminary treatment: the real silk fabric after the tentering that comes unstuck is dropped in enzyme solutions and carries out preliminary treatment;
(2) starching: the pretreated real silk fabric of enzyme, starching machine carries out back starching;
(3) dry: adopt infrared drying device, its bake out temperature is 80 ~ 120 DEG C, drying time 3 ~ 5min;
(4) file is made: described spray printing is by colour atla Software Create, and print conditions is: printing precision 360 × 2160dpi, 360 × 2160 6pass CMYK, and spray printing ink used is regeneration activity dye ink;
(5) spray printing: D-2200 code ink jet printing machine carries out spray printing;
(6) decatize is dried;
(7) wash: after cold wash, soap, then carry out a cold wash, described soaping is 10min under 80 DEG C of conditions, and soaping agent is modification Tea Saponin 2 ~ 10g/L;
(8) tentering is dried.
2. method according to claim 1, is characterized in that:
Described step (1) enzyme treatment process condition is: papain 15 ~ 18U/mL, cellulase 3 ~ 5U/mL, pH7, temperature 40 DEG C, time 1h, bath raio 1: 10, and after process, clear water is cleaned air-dry;
Described step (2) slurry is composed as follows by weight percentage:
Sodium alginate 5%
Shitosan 5% ~ 8%
Sodium bicarbonate 2% ~ 3%
Sodium sulphate 2% ~ 3%
Moisture absorption swelling agent 2%
Surplus is water; Described moisture absorption swelling agent is the mixture of urea, triethylene glycol;
Described step (3) decatize is react fixation 30 ~ 50min under 100 ~ 110 DEG C of saturated steam conditions.
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Cited By (15)
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| CN104831566A (en) * | 2015-05-11 | 2015-08-12 | 海安县南莫制丝有限公司 | Chine silk fabric production process |
| CN105019277A (en) * | 2015-07-10 | 2015-11-04 | 湖州三佳纺织有限公司 | Imitated silk fabric reactive printing method |
| CN105064080A (en) * | 2015-07-16 | 2015-11-18 | 鑫缘茧丝绸集团股份有限公司 | Real silk embossing process |
| CN105220532A (en) * | 2015-10-20 | 2016-01-06 | 湖州博仁纺织品有限公司 | A kind of printing in textiles antimigration agent based on shitosan and preparation method thereof |
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| CN105780137A (en) * | 2016-05-13 | 2016-07-20 | 东莞市联洲知识产权运营管理有限公司 | Preparation method of super-soft and highly-hygroscopic silk fibers |
| CN105970690A (en) * | 2016-06-02 | 2016-09-28 | 湖州新隆龙丝绸印花有限公司 | Fabric printing technology |
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| CN106243834A (en) * | 2016-08-23 | 2016-12-21 | 深圳市南方煜森电子有限公司 | One is printed upon non-fading ink and application process thereof on cotton |
| CN106638046A (en) * | 2016-12-29 | 2017-05-10 | 嘉兴金迈纺织科技有限公司 | High-infiltration printing and dyeing slurry preventing discharge of ammonia nitrogen |
| CN106930128A (en) * | 2015-12-31 | 2017-07-07 | 上海水星家用纺织品股份有限公司 | A kind of digital printing method of textile fabric |
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| CN112900123A (en) * | 2019-12-03 | 2021-06-04 | 嵊州市好运来印染有限公司 | Real silk fabric printing method |
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| CN104831566A (en) * | 2015-05-11 | 2015-08-12 | 海安县南莫制丝有限公司 | Chine silk fabric production process |
| CN105019277A (en) * | 2015-07-10 | 2015-11-04 | 湖州三佳纺织有限公司 | Imitated silk fabric reactive printing method |
| CN105064080A (en) * | 2015-07-16 | 2015-11-18 | 鑫缘茧丝绸集团股份有限公司 | Real silk embossing process |
| CN105220532A (en) * | 2015-10-20 | 2016-01-06 | 湖州博仁纺织品有限公司 | A kind of printing in textiles antimigration agent based on shitosan and preparation method thereof |
| CN105421081A (en) * | 2015-12-24 | 2016-03-23 | 南通那芙尔服饰有限公司 | Real-silk jean socks and production method of same |
| CN106930128A (en) * | 2015-12-31 | 2017-07-07 | 上海水星家用纺织品股份有限公司 | A kind of digital printing method of textile fabric |
| CN105780137A (en) * | 2016-05-13 | 2016-07-20 | 东莞市联洲知识产权运营管理有限公司 | Preparation method of super-soft and highly-hygroscopic silk fibers |
| CN105970690A (en) * | 2016-06-02 | 2016-09-28 | 湖州新隆龙丝绸印花有限公司 | Fabric printing technology |
| CN106087479A (en) * | 2016-07-06 | 2016-11-09 | 德清县新鑫达丝绸炼染有限公司 | A kind of real silk reactive printing method |
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| CN106243834B (en) * | 2016-08-23 | 2019-11-05 | 深圳市南方煜森电子有限公司 | One kind being printed upon non-fading ink and its application method on cotton |
| CN108071023A (en) * | 2016-11-08 | 2018-05-25 | 绍兴市海印数码科技有限公司 | A kind of living polymer dye ink and its applied to the ink-jet printed dyeing and printing process on cotton fabric |
| CN108071023B (en) * | 2016-11-08 | 2020-07-17 | 绍兴市海印数码科技有限公司 | Ink-jet printing and dyeing process for applying active macromolecular dye ink to cotton fabric |
| CN106638046A (en) * | 2016-12-29 | 2017-05-10 | 嘉兴金迈纺织科技有限公司 | High-infiltration printing and dyeing slurry preventing discharge of ammonia nitrogen |
| CN109137578A (en) * | 2018-08-17 | 2019-01-04 | 宁波大千纺织品有限公司 | The preparation method of number emulation printed fabric |
| CN112900123A (en) * | 2019-12-03 | 2021-06-04 | 嵊州市好运来印染有限公司 | Real silk fabric printing method |
| CN111676713A (en) * | 2020-07-27 | 2020-09-18 | 湖州市千金金耀制丝有限公司 | Digital printing process of high-color-fastness silk fabric |
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