CN104194468A - Environmental protection and high-efficiency ink cleaner and preparation method thereof - Google Patents
Environmental protection and high-efficiency ink cleaner and preparation method thereof Download PDFInfo
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- CN104194468A CN104194468A CN201410480600.2A CN201410480600A CN104194468A CN 104194468 A CN104194468 A CN 104194468A CN 201410480600 A CN201410480600 A CN 201410480600A CN 104194468 A CN104194468 A CN 104194468A
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Abstract
The invention provides an environmental protection and high-efficiency ink cleaner and a preparation method of the environmental protection and high-efficiency ink cleaner. The ink cleaner is a neutral oil-in-water microemulsion ink cleaner, and comprises the following components: environment-friendly oil solvents, alkylphenol polyoxyethylene ether, sodium dodecylbenzene sulfonate, sodium oleate and deionized water. The preparation method of the environmental protection and high-efficiency ink cleaner comprises the following steps: a) taking materials, b) preparing a mixed surfactant solution, and c) preparing an oil-in-water microemulsion. The invention discloses the environmental protection and high-efficiency ink cleaner and the preparation method of the environmental protection and high-efficiency ink cleaner. The ink cleaner is prepared by using a D-phase emulsification method, the preparation method is simple, the preparation cost is low and the use is convenient, the ink cleaner is obvious in ink removing effect, is non-toxic and pollution-free, and has no harm to the human skin, and further cleans ink on hands of printing workers, thereby having good market promotion values.
Description
Technical field
The present invention relates to a kind of detergent for ink, relate in particular to detergent for ink of a kind of environment-friendly high-efficiency and preparation method thereof, belong to technical field of ink.
Background technology
Ink is the important materials for printing, and it is by printing on pattern, the present stock of literal table.Ink is generally comprised of pigment, low-melting ink vehicle, solvent and auxiliary agent etc., and these compositions mix equably and form the gluey fluid of a kind of stickiness through repeat-rolling, and ink is widely used in the various printings such as books and periodicals, packing and decorating, building decoration.Because ink has stronger sticking power and cohesiveness, pressman's hand is printed ink make dirty after, superfine pigment can enter palmmprint with ink base-material, cleans very difficult, with soap and general washing composition, be difficult to clean severe jamming and the normal work that affects workpeople.
In existing technology, the method for cleaning ink has two kinds: a kind of is to clean with organic solvents such as gasoline, kerosene; Another kind is to adopt sawdust or monofilament to add soap to clean.Before a kind of method organic solvent used itself inflammable, poisonous, have bad smell, skin is had and is stimulated and desiccation, harmful to skin after use, a kind of rear method will be rubbed scouring repeatedly, is difficult for cleanly, damages skin, washes defensive position also uncomfortable.At present, also the product that has occurred the cleaning ink of some special uses on market, but the cleaning performance of these products is not clearly, and price comparison is expensive, using method is inconvenient, therefore develop a kind of ink effect product remarkable and that expense is cheap, using method is easy that cleans, seems very necessary.
Summary of the invention
For the demand, the invention provides detergent for ink of a kind of environment-friendly high-efficiency and preparation method thereof, this detergent for ink adopts D phase emulsion process to be prepared, preparation method is simple, preparation cost is cheap, easy to use, its removal ink effect significantly and nontoxic pollution-free, neither can damage human body skin, meet again the cleaning of ink on hand to pressman, there is good market popularization value.
The present invention is detergent for ink of a kind of environment-friendly high-efficiency and preparation method thereof, described detergent for ink is neutral oil-in-water microemulsion detergent for ink, its moiety comprises environment protection oil solvent, alkylphenol polyoxyethylene, Sodium dodecylbenzene sulfonate, sodium oleate and deionized water, described preparation method comprises the steps: a) to join and gets material, b) preparation mixed surfactants solutions, c) preparation oil-in-water microemulsion.
In a preferred embodiment of the present invention, the quality percentage composition of described detergent for ink moiety is: environment protection oil solvent 10~12%, alkylphenol polyoxyethylene 12~14%, Sodium dodecylbenzene sulfonate 8~10%, sodium oleate 6~8%, deionized water 56~64%.
In a preferred embodiment of the present invention, in described step b), preparation mixed surfactants solutions comprises the steps: 1) get a certain amount of deionized water and put into stirred vessel; 2) put into sodium oleate and be stirred to dissolving completely; 3) put into Sodium dodecylbenzene sulfonate and stir 10min; 4) put into alkylphenol polyoxyethylene and stir 20min.
In a preferred embodiment of the present invention, in described step b), stirring technique condition is: 25 ℃ of whipping temps, stirring velocity 350r/min.
In a preferred embodiment of the present invention, in described step c), preparation oil-in-water microemulsion is that the environment protection oil solvent preparing is added in mixed surfactants solutions and produced, and its processing condition are: stirring velocity 500r/min, churning time 20min.
The present invention has disclosed detergent for ink of a kind of environment-friendly high-efficiency and preparation method thereof, this detergent for ink adopts D phase emulsion process to be prepared, preparation method is simple, preparation cost is cheap, easy to use, its removal ink effect significantly and nontoxic pollution-free, neither can damage human body skin, meet again the cleaning of ink on hand to pressman, there is good market popularization value.
Accompanying drawing explanation
Below in conjunction with the drawings and specific embodiments, the present invention is further detailed explanation:
Fig. 1 is the detergent for ink preparation method's of embodiment of the present invention environment-friendly high-efficiency process figure.
Embodiment
Below in conjunction with accompanying drawing, preferred embodiment of the present invention is described in detail, thereby so that advantages and features of the invention can be easier to be it will be appreciated by those skilled in the art that, protection scope of the present invention is made to more explicit defining.
Fig. 1 is the detergent for ink preparation method's of embodiment of the present invention environment-friendly high-efficiency process figure; This detergent for ink is neutral oil-in-water microemulsion detergent for ink, its moiety comprises environment protection oil solvent, alkylphenol polyoxyethylene, Sodium dodecylbenzene sulfonate, sodium oleate and deionized water, described preparation method comprises the steps: a) to join and gets material, b) preparation mixed surfactants solutions, c) preparation oil-in-water microemulsion.
The detergent for ink of the environment-friendly high-efficiency that the present invention mentions using environment protection oil solvent as main solvent, using alkylphenol polyoxyethylene, Sodium dodecylbenzene sulfonate and sodium oleate as mixed surfactant, adopt rational order of addition(of ingredients), under the condition stirring in normal temperature middling speed, be prepared, the neutral water oil-in micro-emulsion ink cleaning agent of producing had both met the cleaning of ink on hand to pressman, again environment was not polluted.The quality percentage composition of this detergent for ink moiety is: environment protection oil solvent 10~12%, alkylphenol polyoxyethylene 12~14%, Sodium dodecylbenzene sulfonate 8~10%, sodium oleate 6~8%, deionized water 56~64%.Wherein, environment protection oil solvent cleaning effect is comparatively desirable and harmless to people's skin, and the microemulsion wiping effect obtaining through Over emulsfication is better and solution-stabilized; In mixed surfactant, the composite use of alkylphenol polyoxyethylene, Sodium dodecylbenzene sulfonate and sodium oleate, is conducive to emulsification and cleaning performance good.
The order of addition(of ingredients) that the detergent for ink of the environment-friendly high-efficiency that the present invention proposes adopts in preparation process is for first adding deionized water, then adds successively sodium oleate, Sodium dodecylbenzene sulfonate, alkylphenol polyoxyethylene, finally adds environment protection oil solvent; The disperse phase that this order of addition(of ingredients) forms is thinner and formation microemulsion is more stable.For save energy, handled easily, be convenient to produce, this detergent for ink is selected to prepare under normal temperature, middling speed agitation condition, because the raw material ratio of selecting is more cheap, production technique is easy, therefore preparation cost is cheap.The detergent for ink of this environment-friendly high-efficiency is removed and is stained with on hand that ink is convenient and swift, cleaning performance is remarkable, during actual use, can directly dip clean-out system wiping and remove, and also after dilutable water, cleans and removes, non-stimulated to skin, without injury.
Embodiment 1
Concrete preparation method is as follows:
A) join and get material, by quality percentage composition, take following material composition: 10% environment protection oil solvent, 12% alkylphenol polyoxyethylene, 8% Sodium dodecylbenzene sulfonate, 6% sodium oleate, 64% deionized water.
B) preparation mixed surfactants solutions, concrete preparation process is: first at 25 ℃ of normal temperature, the deionized water taking is put into stirred vessel, again the sodium oleate taking is put into deionized water for stirring to dissolving completely, then to putting into the Sodium dodecylbenzene sulfonate taking in container, with 350r/min speed, stir 10min, in the most backward container, put into the alkylphenol polyoxyethylene taking and stir 20min with 350r/min speed, produce mixed surfactants solutions.
C) preparation oil-in-water microemulsion, concrete preparation process is: the mixed surfactants solutions of first at normal temperatures the environment protection oil solvent taking being put into step b) preparation, then with 350r/min speed, stir 20min, last discharging makes the micro-emulsion ink cleaning agent of environment-friendly high-efficiency.
Embodiment 2
Concrete preparation method is as follows:
A) join and get material, by quality percentage composition, take following material composition: 12% environment protection oil solvent, 14% alkylphenol polyoxyethylene, 10% Sodium dodecylbenzene sulfonate, 8% sodium oleate, 56% deionized water.
B) preparation mixed surfactants solutions, concrete preparation process is: first at 25 ℃ of normal temperature, the deionized water taking is put into stirred vessel, again the sodium oleate taking is put into deionized water for stirring to dissolving completely, then to putting into the Sodium dodecylbenzene sulfonate taking in container, with 350r/min speed, stir 10min, in the most backward container, put into the alkylphenol polyoxyethylene taking and stir 20min with 350r/min speed, produce mixed surfactants solutions.
C) preparation oil-in-water microemulsion, concrete preparation process is: the mixed surfactants solutions of first at normal temperatures the environment protection oil solvent taking being put into step b) preparation, then with 350r/min speed, stir 20min, last discharging makes the micro-emulsion ink cleaning agent of environment-friendly high-efficiency.
The present invention has disclosed detergent for ink of a kind of environment-friendly high-efficiency and preparation method thereof, this detergent for ink adopts D phase emulsion process to be prepared, preparation method is simple, preparation cost is cheap, easy to use, its removal ink effect significantly and nontoxic pollution-free, neither can damage human body skin, meet again the cleaning of ink on hand to pressman, there is good market popularization value.
The above; it is only the specific embodiment of the present invention; but protection scope of the present invention is not limited to this; any those of ordinary skill in the art are in the disclosed technical scope of the present invention; the variation that can expect without creative work or replacement, within all should being encompassed in protection scope of the present invention.Therefore, protection scope of the present invention should be as the criterion with the protection domain that claims were limited.
Claims (5)
1. detergent for ink of an environment-friendly high-efficiency and preparation method thereof, it is characterized in that, described detergent for ink is neutral oil-in-water microemulsion detergent for ink, its moiety comprises environment protection oil solvent, alkylphenol polyoxyethylene, Sodium dodecylbenzene sulfonate, sodium oleate and deionized water, described preparation method comprises the steps: a) to join and gets material, b) preparation mixed surfactants solutions, c) preparation oil-in-water microemulsion.
2. detergent for ink of environment-friendly high-efficiency according to claim 1 and preparation method thereof, it is characterized in that, the quality percentage composition of described detergent for ink moiety is: environment protection oil solvent 10~12%, alkylphenol polyoxyethylene 12~14%, Sodium dodecylbenzene sulfonate 8~10%, sodium oleate 6~8%, deionized water 56~64%.
3. detergent for ink of environment-friendly high-efficiency according to claim 1 and preparation method thereof, is characterized in that, in described step b), preparation mixed surfactants solutions comprises the steps: 1) get a certain amount of deionized water and put into stirred vessel; 2) put into sodium oleate and be stirred to dissolving completely; 3) put into Sodium dodecylbenzene sulfonate and stir 10min; 4) put into alkylphenol polyoxyethylene and stir 20min.
4. detergent for ink of environment-friendly high-efficiency according to claim 3 and preparation method thereof, is characterized in that, in described step b), stirring technique condition is: 25 ℃ of whipping temps, stirring velocity 350r/min.
5. detergent for ink of environment-friendly high-efficiency according to claim 1 and preparation method thereof, it is characterized in that, in described step c), preparation oil-in-water microemulsion is that the environment protection oil solvent preparing is added in mixed surfactants solutions and produced, and its processing condition are: stirring velocity 500r/min, churning time 20min.
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CN201410480600.2A CN104194468A (en) | 2014-09-19 | 2014-09-19 | Environmental protection and high-efficiency ink cleaner and preparation method thereof |
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CN201410480600.2A CN104194468A (en) | 2014-09-19 | 2014-09-19 | Environmental protection and high-efficiency ink cleaner and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107304316A (en) * | 2016-04-20 | 2017-10-31 | 天津市有为印刷包装有限公司 | A kind of environmentally friendly low foam detergent for ink and preparation method thereof |
CN107858037A (en) * | 2017-11-02 | 2018-03-30 | 中国标准化研究院 | A kind of O/W micro-emulsion types printing-ink environment-friendly cleaning agent |
-
2014
- 2014-09-19 CN CN201410480600.2A patent/CN104194468A/en active Pending
Non-Patent Citations (1)
Title |
---|
李冰等: ""D相乳化法制备油墨清洗剂"", 《清洗世界》 * |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107304316A (en) * | 2016-04-20 | 2017-10-31 | 天津市有为印刷包装有限公司 | A kind of environmentally friendly low foam detergent for ink and preparation method thereof |
CN107858037A (en) * | 2017-11-02 | 2018-03-30 | 中国标准化研究院 | A kind of O/W micro-emulsion types printing-ink environment-friendly cleaning agent |
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Application publication date: 20141210 |