CN104190923B - Nano metal powder coating unit and method for coating - Google Patents

Nano metal powder coating unit and method for coating Download PDF

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Publication number
CN104190923B
CN104190923B CN201410475889.9A CN201410475889A CN104190923B CN 104190923 B CN104190923 B CN 104190923B CN 201410475889 A CN201410475889 A CN 201410475889A CN 104190923 B CN104190923 B CN 104190923B
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CN
China
Prior art keywords
insulation shell
nano metal
metal powder
argon gas
valve
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Expired - Fee Related
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CN201410475889.9A
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Chinese (zh)
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CN104190923A (en
Inventor
刘平安
赵�怡
朱力
董惠
王革
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Harbin Engineering University
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Harbin Engineering University
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Priority to CN201410475889.9A priority Critical patent/CN104190923B/en
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Publication of CN104190923B publication Critical patent/CN104190923B/en
Expired - Fee Related legal-status Critical Current
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Abstract

The invention provides a kind of nano metal powder coating unit and method for coating, comprise insulation shell, base, drive motors, speed regulator, the driving shaft and the paddle that are connected with drive motors output, the upper part of driving shaft is positioned at insulation shell inside through the opening of insulation shell middle, paddle is arranged on part on driving shaft, also comprise argon gas storage tank and heater, argon gas storage tank is arranged in the cavity between insulation shell and base, argon gas storage tank upper end is connected with the opening of insulation shell bottom by wireway, lower end is fixedly connected with base, the bottom of insulation shell arranges heater, middle, insulation shell top has charging aperture, charging aperture is connected with nano metal powder production line, two ends on insulation shell top set out respectively pore, on venthole, set out pore valve. adopt the present invention can effectively avoid the nano metal powder just made oxidized, its activity of effective guarantee, and simple to operate, easy to use.

Description

Nano metal powder coating unit and method for coating
Technical field
The present invention relates to a kind of coating unit and method for coating, relate in particular to a kind of coating unit and coated side of nano metal powderMethod.
Background technology
At present, the main energy sources that industrial production and resident living are used comes from the fossil fuels such as coal, oil, natural gas. ItFeature be, forming process is extremely slow, fast consume under be faced with by exhausted situation. And fossil fuel combustionBurn the carbon dioxide producing and will increase the weight of tellurian greenhouse effects, its burning such as inner contained sulfide, nitride etc. will produceThe pollutant such as oxysulfide, nitrogen oxide, causes atmosphere pollution and forms acid rain, and harm natural environment has been not enough to adapt toThe fast development of modern industry.
Metal fuel is as a kind of New-type fuel of high heating value, and its energy density is far away higher than fossil combustions such as coal, oil, natural gasesMaterial. And, in the process of burning, can not produce the pernicious gas such as oxysulfide, nitrogen oxide. Meanwhile, on the earth, have richRich metallic mineral resources, and metal smelt technology maturation, can provide solid foundation for the application of metal fuel.
Owing to being subject to the restriction of metal dust production and processing level, traditional metal powder granulates diameter is larger, conventionally at 1 micronAbove, therefore its application is subject to larger restriction. Mainly as the filler of solid propellant rocket propellant, firebomb, photographThe luminous agent of bright bullet, the filler in explosive etc., range of application is relatively narrow. Along with novel production works such as discharge-induced explosion method, laser methodsThe appearance of skill, the particle diameter of metal dust has obtained further reduction. At present, diameter is less than the metal dust of 100 nanometersProduction technology very ripe, and can under controlled condition, to produce average grain diameter be 30 nanometers, 50 nanometers, 80The metal dust that nanometer etc. are different. Along with the reduction of metal powder granulates diameter, the specific area of metal dust increases exponentially,Its active significantly enhancing. This make nano metal powder can break away from before only as the state of metallic addition, become fuelMain body. Give full play to the characteristic of its high energy having, environmental protection. But the increase of nano metal powder activity has also brought oneFixed problem. If the nano metal powder of producing is directly exposed in air, will be by airborne dioxygen oxidation. NoOnly can make a part of nano metal powder lose activity, cause the decline of nano metal powder acting ability, and Nano metal powderThe heat that end produces in oxidizing process will make nano metal powder temperature raise, and likely causes chain reaction, cause fire orExplosion accident. For the nano metal powder that prevents from just having generated oxidized in the process contacting with air, need to be in nanometerWhen the harsh product of metal dust completes, just, at the coated one deck organic matter in its surface, prevent nano metal powder oxidation by air to reachObject.
Technical scheme of the present invention proposes under above-mentioned background, is intended to device by mentioning in technical scheme and correspondingMethod for coating, complete coated to nano metal powder.
Summary of the invention
Object of the present invention has two, and the one, a kind of nm of gold is provided in order simply and effectively nano metal powder to be coatedBelong to powder packets coating device, two are to provide a kind of nano metal powder coating unit that uses carries out coated nanometer to nano metal powderMetal dust method for coating.
The object of the present invention is achieved like this: nano metal powder coating unit comprises insulation shell, is positioned at insulation shell belowBase, be arranged on drive motors on base, be arranged on the speed regulator of drive motors one side, be connected with drive motors outputDriving shaft and paddle, the upper part of driving shaft is positioned at insulation shell inside through the opening of insulation shell middle, stirsOar is arranged on part on driving shaft, also comprises argon gas storage tank and heater, and argon gas storage tank is arranged between insulation shell and baseIn cavity, argon gas storage tank upper end by wireway be connected with the opening of insulation shell bottom, lower end is fixedly connected with base, insulationThe bottom of housing arranges heater, and middle, insulation shell top has charging aperture, and charging aperture and nano metal powder production line connectConnect, set out respectively pore at the two ends on insulation shell top, on venthole, set out pore valve;
The method for coating of nano metal powder comprises the following steps:
Step 1: clad material is put into insulation shell;
Step 2: open valve and venthole valve on the wireway that argon gas storage tank is connected with insulation shell, make argon gas stream excessively wholeIndividual housing, within 20-30 minute, insulation shell inside manufactures after ar gas environment, by the valve closing of opening;
Step 3: open heater heating and thermal insulation housing, make insulation shell internal temperature reach the fusing point of clad material;
Step 4: open the valve of nano metal powder production line pipeline, nano metal powder is transported to insulation cladding through charging apertureThe inside of body, closes the valve of nano metal powder production line pipeline, drive motors work, and paddle rotation, starts nanometerBeing coated of metal dust.
The present invention also comprises some architectural features like this:
1. described in, insulation shell comprises upper shell and lower house, and the intersection of upper shell and lower house is stairstepping, and is provided withSealing ring, upper-lower casing connects by buckle.
2. described in, paddle has two pairs, and two pairs of paddles are oppositely arranged on driving shaft.
3. described in, the rotating speed of paddle is per minute 10000 to turn.
Compared with prior art, the invention has the beneficial effects as follows: nano metal powder coating unit provided by the present invention and coatedMethod is under argon shield environment, to carry out nano metal powder to be coated, and has prevented to greatest extent the nm of gold of just having madeBelong to powder by airborne dioxygen oxidation. Make environment temperature be controlled at the molten of organic coating material by heater heating and thermal insulation housingPoint, makes Coated with Organic Matter material can cover uniformly nano metal powder surface. Device charging aperture and nano metal powderProduction line is directly connected, and has outside air to enter oxidized metal powder while avoiding injecting metal dust. Adopt speed regulator to driving electricityRotating speed and the direction of machine regulate, and can regulate as required the rotating speed of paddle to reach per minute 10000 and turn above, make to receiveRice metal dust carries out high speed shear, destroys the agglomeration of nanometer powder, makes Coated with Organic Matter material cover uniformly nanometerMetal dust surface, can reach better covered effect.
Brief description of the drawings
Fig. 1 is structural representation of the present invention;
Fig. 2 is clamping part separation structure schematic diagram of the present invention.
Detailed description of the invention
Below in conjunction with accompanying drawing and detailed description of the invention, the present invention is described in further detail.
In conjunction with Fig. 1 and Fig. 2, the present invention comprises insulation shell 2, is positioned at the base 1 of insulation shell below, is arranged on base 1Drive motors 6, driving shaft 14 and that are arranged on the speed regulator 7 of drive motors 6 one sides, are connected with drive motors 6 outputsPaddle 9, the upper part of driving shaft 14 is positioned at insulation shell 2 inside, paddle through the opening of insulation shell 2 middles9 are arranged on part on driving shaft 14, and paddle 9 is arranged on driving shaft 14 by key, in the middle of insulation shell 2 bottomsAnd between driving shaft 14, be provided with Limit Bearing 13, also comprise argon gas storage tank 10 and heater 8, argon gas storage tank 10 is arranged on guarantorIn cavity between temperature housing 2 and base 1, be mounted in specifically a side of cavity, argon gas storage tank 10 upper ends are by air guidePipe is connected with the opening of insulation shell 2 bottoms, lower end is fixedly connected with base 1, and the bottom of insulation shell 2 arranges heater 8,To realize the heating to insulation shell 2, insulation shell 2 middles, top have charging aperture 4, charging aperture 4 and Nano metal powderEnd production line connects, and sets out respectively pore 11 at the two ends on insulation shell 2 tops, sets out pore valve on venthole 11,Realize the control to venthole switch.
Insulation shell 2 of the present invention is made up of upper shell 2-1 and lower house 2-2 two parts, upper shell 2-1 and lower houseThe intersection of 2-2 is stairstepping, and is provided with sealing ring 12 interface is sealed, and housing 2 is by upper shell 2-1Linking together by buckle 3 with lower house 2-2, is mainly the crowded of two parts up and down to insulation shell 2 by buckle 3Pressure effect realizes and connecting. Paddle of the present invention has two pairs, and two pairs of paddles are oppositely arranged on driving shaft, realize stirring action.
Using nano metal powder coating unit provided by the present invention to carry out in the coated process of nano metal powder, coatedThe key step of method comprises:
Step 1: clad material is put into insulation shell;
Step 2: open valve and venthole valve on the wireway that argon gas storage tank is connected with insulation shell, make argon gas stream excessively wholeIndividual housing, within 20-30 minute, insulation shell inside manufactures after ar gas environment, by the valve closing of opening;
Step 3: open heater heating and thermal insulation housing, make insulation shell internal temperature reach the fusing point of clad material;
Step 4: open the valve of nano metal powder production line pipeline, nano metal powder is transported to insulation cladding through charging apertureThe inside of body, closes the valve of nano metal powder production line pipeline, drive motors work, and paddle rotation, starts nanometerBeing coated of metal dust.
In concrete implementation process, first Coated with Organic Matter material is packed in lower house 2-2, then upper and lower by housing 2Two parts are buckled together, and use buckle 3 fastenings, and charging aperture 4 is connected with the production line pipeline of nano metal powder, andClose the valve of charging aperture pipeline; Open valve and venthole valve on the wireway that argon gas storage tank 10 is connected with insulation shell,Make argon gas stream cross whole insulation shell, within 20-30 minute, insulation shell inside manufactures after ar gas environment, by the valve closing of opening;Open heater 8 heating and thermal insulation housings 2, make the internal temperature of insulation shell reach the fusing point of Coated with Organic Matter material, open lifeProduce the valve in spool road, nano metal powder is transported to the inside of insulation shell 2 through charging aperture 4; Open drive motors 6,Make nano metal powder and organic coating material under the stirring of paddle 9, carry out blending, and adjust and drive electricity by speed regulator 7The rotating speed of machine 6 is increased to gradually per minute 10000 and turns, and organic coating material can fully be contacted with nano metal powder, allBe coated on the surface of nano metal powder evenly. After nano metal powder is covered to complete, open buckle 3, by insulation shell 2Take down on top, can encapsulate completing coated nano metal powder. Nano metal powder is pulled down paddle 9 after taking out,Paddle 9 and driving shaft 14, insulation shell 2 etc. are cleaned thoroughly and dried, can carry out the coated work of next groupDo.
The present invention carries out coated to nano metal powder in the environment of the protective gas of argon gas, can ensure Nano metal powderEnd is not oxidized and can under atmospheric pressure environment, be coated. Adopt drive motors to drive to be positioned at two couple of insulation shell inside reversePaddle carries out high-speed stirred to nano metal powder and organic coating material, and use speed regulator control paddle rotating speed andDirection, finally makes organic coating material be uniformly distributed in the surface of nano metal powder, can effectively avoid the nm of gold of just having madeBelong to powder by airborne dioxygen oxidation, reaching the object that prevents that it is oxidized, can effectively ensure nano metal powderActivity, and simple to operate, easy to use, be easy to realize.

Claims (2)

1. a nano metal powder method for coating, is characterized in that: comprise nano metal powder coating unit, Nano metal powderEnd coating unit comprises insulation shell, be positioned at the base of insulation shell below, be arranged on drive motors on base, be arranged on and driveThe speed regulator of moving motor one side, driving shaft and the paddle being connected with drive motors output, the upper part of driving shaft is through insulationThe opening of housing middle and be positioned at insulation shell inside, paddle is arranged on part on driving shaft, also comprises argon gas storage tank and addsHot device, argon gas storage tank is arranged in the cavity between insulation shell and base, and argon gas storage tank upper end is by wireway and insulation shellOpening connection, the lower end of bottom are fixedly connected with base, and the bottom of insulation shell arranges heater, middle, insulation shell topHave charging aperture, charging aperture is connected with nano metal powder production line, sets out respectively pore at the two ends on insulation shell top,On venthole, set out pore valve;
Step 1: clad material is put into insulation shell;
Step 2: open valve and venthole valve on the wireway that argon gas storage tank is connected with insulation shell, make argon gas stream excessively wholeIndividual housing, within 20-30 minute, insulation shell inside manufactures after ar gas environment, by the valve closing of opening;
Step 3: open heater heating and thermal insulation housing, make insulation shell internal temperature reach the fusing point of clad material;
Step 4: open the valve of nano metal powder production line pipeline, nano metal powder is transported to insulation cladding through charging apertureThe inside of body, closes the valve of nano metal powder production line pipeline, drive motors work, and paddle rotation, starts nanometerBeing coated of metal dust.
2. a kind of nano metal powder method for coating according to claim 1, is characterized in that: the rotating speed of described paddle isPer minute 10000 turn.
CN201410475889.9A 2014-09-18 2014-09-18 Nano metal powder coating unit and method for coating Expired - Fee Related CN104190923B (en)

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Publication number Priority date Publication date Assignee Title
CN112453389B (en) * 2020-10-31 2023-01-13 湖北小蚂蚁金刚石工具有限公司 Device for coating diamond
CN112934125A (en) * 2021-02-02 2021-06-11 江苏智仁景行新材料研究院有限公司 Metal powder high temperature suspension device

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WO1989008516A1 (en) * 1988-03-11 1989-09-21 Michitoshi Hirata Fine metal powder and method of producing same
CN1381325A (en) * 2001-04-13 2002-11-27 深圳市东方亮化学材料有限公司 Technology and equipment for processing alloy powder used for paste solder
CN2633477Y (en) * 2003-07-10 2004-08-18 王志平 High purity metal nano powder passive film synthetic equipment
CN1778498A (en) * 2005-09-30 2006-05-31 中国工程物理研究院激光聚变研究中心 Production and its apparatus for organic coated metal nanometer powdery
CN1994626A (en) * 2006-12-30 2007-07-11 江苏天一超细金属粉末有限公司 Method and equipment for coating metal bond on abrasive particle
CN101015861A (en) * 2006-11-09 2007-08-15 昆山密友实业有限公司 Continuous production apparatus for nano metal powder
CN101474672A (en) * 2007-12-31 2009-07-08 王志平 Device for continuously inactivating metal nano powder
CN102179523A (en) * 2011-04-08 2011-09-14 华中科技大学 Continuous preparing and in-situ coating device for oxidizable metallic nanomaterial
CN103357869A (en) * 2013-07-24 2013-10-23 清华大学 Device and system applied to particle coating
CN204171354U (en) * 2014-09-18 2015-02-25 哈尔滨工程大学 Nano metal powder coating unit

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Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1989008516A1 (en) * 1988-03-11 1989-09-21 Michitoshi Hirata Fine metal powder and method of producing same
CN1381325A (en) * 2001-04-13 2002-11-27 深圳市东方亮化学材料有限公司 Technology and equipment for processing alloy powder used for paste solder
CN2633477Y (en) * 2003-07-10 2004-08-18 王志平 High purity metal nano powder passive film synthetic equipment
CN1778498A (en) * 2005-09-30 2006-05-31 中国工程物理研究院激光聚变研究中心 Production and its apparatus for organic coated metal nanometer powdery
CN101015861A (en) * 2006-11-09 2007-08-15 昆山密友实业有限公司 Continuous production apparatus for nano metal powder
CN1994626A (en) * 2006-12-30 2007-07-11 江苏天一超细金属粉末有限公司 Method and equipment for coating metal bond on abrasive particle
CN101474672A (en) * 2007-12-31 2009-07-08 王志平 Device for continuously inactivating metal nano powder
CN102179523A (en) * 2011-04-08 2011-09-14 华中科技大学 Continuous preparing and in-situ coating device for oxidizable metallic nanomaterial
CN103357869A (en) * 2013-07-24 2013-10-23 清华大学 Device and system applied to particle coating
CN204171354U (en) * 2014-09-18 2015-02-25 哈尔滨工程大学 Nano metal powder coating unit

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