CN104173248A - Natural plant essential oil-containing disinfecting liquid soap, as well as preparation method and application thereof - Google Patents
Natural plant essential oil-containing disinfecting liquid soap, as well as preparation method and application thereof Download PDFInfo
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- CN104173248A CN104173248A CN201410453948.2A CN201410453948A CN104173248A CN 104173248 A CN104173248 A CN 104173248A CN 201410453948 A CN201410453948 A CN 201410453948A CN 104173248 A CN104173248 A CN 104173248A
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Abstract
The invention relates to disinfecting liquid soap and a preparation method thereof, and particularly relates to natural plant essential oil-containing disinfecting liquid soap and a preparation method thereof. The disinfecting liquid soap is prepared from N-(4-chlorphenyl)-N'-(3,4-dichlorophenyl)urea (triclocarban), ethanol, litsea cubeba essential oil, sweet orange essential oil, PEG40 hydrogenated castor oil (CO-40), N-trimethylglycine (betaine), carbomer U20 (Carbopol Ultrez 20 polymer), triethanolamine and deionized water. Antimicrobial tests indicate that the disinfecting liquid soap has a relatively strong bacteriostatic effect, is applicable to medical mechanisms, hotels, food processing manufacture enterprises, dining and entertainment facilities and the like.
Description
Technical field
The present invention relates to a kind of type disinfecting liquid, especially a kind of type disinfecting liquid that contains natural plant essential oils, is particularly useful for medical institutions, hotel, food processing manufacturing enterprise, food and drink public place of entertainment etc.
Background technology
In human body, both hands are the maximum positions of harmful microorganism such as contact antibacterial, virus.There are some researches show, can adhering on hand of people much more than 150 planted antibacterial, virus etc., comprises escherichia coli, Candida albicans, staphylococcus aureus, bacillus pyocyaneus, Salmonella, tubercule bacillus, influenza virus, hepatitis virus etc.Separately there are some researches show, is all the germ infection having on hand up to more than 80% gastroenteropathy, dermatosis etc.Duty is washed one's hands, and is a kind of mode of effectively pre-preventing germs infection and propagation; And select correct hand-washing article, be whether effectively key point of this mode.Especially for medical personnel, in following patient's contact, in links such as diagnosis and treatment, detection, nursing, handle the courses of infection probability direct and indirect causing and be much higher than general population, therefore select suitable effective handwashing disinfection articles for use most important.
Medium-sized handwashing liquid only has the basic function of clean hand, its bactericidal action is very limited, can only in the process of washing one's hands, by the effect of flowing water, take away 20%～30% antibacterial, as staphylococcus aureus, Candida albicans, the contour pathogenic bacteria of bacillus pyocyaneus, can not kill.This is obviously inadequate for medical personnel, therefore must select to have the professional disinfection hand cleanser of bactericidal effect.This class existing is in the market in the face of medical personnel's professional hand disinfection sterilizing cleaning product, and the overwhelming majority be take " ethanol+isopropyl alcohol+chlorhexidine acetate " composition as main leave antiseptic hand washing gel.Such product alcohol content is high, after contact skin ethanol, can make skin defat, reduces skin elasticity and gloss; And abnormal smells from the patient is large, use impression not good; If the crowd of ethanol allergy is not suitable for using especially.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of type disinfecting liquid containing natural plant essential oils.Effect product sterilization bactericidal effect is obvious, and has the effect of nursing hand skin concurrently, safety and stability, and abnormal smells from the patient is pleasant, is particularly suitable for medical personnel and uses.
The technical scheme that the present invention addresses the above problem is:
A kind of disinfection hand cleanser containing natural plant essential oils, comprise N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea, ethanol, Betaine, Carbopol Ultrez 20 polymer, triethanolamine and deionized water, also is characterized by and contain: Fructus Litseae essential oil, sweet orange oil and Cremophor RH40.
Further, containing a disinfection hand cleanser for natural plant essential oils, described disinfectant solution is aqueous solution, contains following weight ratio ingredient:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (having another name called triclocarban): 0.05%～0.1%
Ethanol: 25%～35%
Fructus Litseae essential oil: 0.01%～0.025%
Sweet orange oil: 0.01%～0.025%
Cremophor RH40 (CO-40): 0.05%～0.1%
Betaine (being betanin): 0.2%～0.5%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.15%～0.3%
Triethanolamine: 0.15%～0.3%
Deionized water: 63.65%～74.38%
Further, the most preferred weight ratio ingredient of this programme is:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (having another name called triclocarban): 0.05%～0.07%
Ethanol: 30%～35%
Fructus Litseae essential oil: 0.01%～0.02%
Sweet orange oil: 0.01%～0.02%
Cremophor RH40 (CO-40): 0.06%～0.09%
Betaine (being betanin): 0.4%～0.5%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.15%～0.2%
Triethanolamine: 0.15%～0.2%
Deionized water: 63.9%～69.17%
Technical advantage of the present invention is as follows:
1. product is clear gel, nontoxic, nonirritant, non-corrosiveness, and alcohol content reduces greatly than conventional products, without pungent alcohol smell; Without essence pigment, not containing the material harmful to human body skin, belong to the sterilizing article of green, safety, environmental protection.
2. the antibacterial agent of a kind of efficient, wide spectrum of the triclocarban that adds in product, safety, it possesses lasting, safe, stable sterilization feature, there is the fabulous compatibility with skin, and gram positive bacteria, gram negative bacteria, fungus, yeast, virus are all had to efficient inhibitory or killing effect.
3. product has added two kind of plant essential oil components especially, wherein in Fructus Litseae essential oil, has natural disinfection effective ingredient citral, for fungus, gram positive bacteria, gram negative bacteria etc., all has obvious antibacterial action; And natural lemon aldehyde is liposoluble constituent, is extremely conducive to skin and absorbs; Sweet orange oil has significant antioxidation, can bactericidal antiphlogistic, and can play the effect of skin whitening.After these two kinds of natural essential oils and triclocarban compatibility, can effectively strengthen the sterilizing effect of product, and carry natural lemon delicate fragrance, after using, skinfeel is better.
4. in product, the special betanin adding is natural amino acid derivant, has significant moistening effect, can reduce the chapped skin sense causing owing to frequently washing one's hands, and keeps moisture of skin.
5. this product, not containing antiseptic composition, because natural essential oil composition has wherein had antiseptic and inhibiting bacteria function effect concurrently, can avoid using chemical preservative, more meets consumer and pursues the natural market demand of protecting product of washing.
6. this product, for exempting from water-washing type gel, is applicable to different occasions and crowd's demand, is particularly suitable for medical personnel and uses, and is also applicable to school, kindergarten, bakery and confectionery, bank and cashier, hotel etc.
Bacteriostatic experiment result shows: type disinfecting liquid of the present invention is suitable for particularly medical personnel's use of medical institutions of public place completely, no matter is stability, and bactericidal effect is all fine; And of the same type chloride better with skinfeel acetic acid class than other after using.
The specific embodiment
Embodiment 1 is containing the preparation of the disinfection hand cleanser of natural plant essential oils
By the N-of 0.05g (4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban) joins in the ethanol of 30g and fully dissolves, then add the Cremophor RH40 (being CO-40) by the Fructus Litseae essential oil of 0.02g, the sweet orange oil of 0.01g and 0.09g to pass through the mixed liquor mixing, and fully mix to such an extent that A is mutually standby.The card ripple U20 (being Carbopol Ultrez20 polymer) of the Betaine of 0.3g (being betanin) and 0.2g is joined and in the deionized water of 69.13g, after heating, fully dissolve cooling standingly, obtain B mutually standby.By above-mentioned A be added to B quite in, after fully mixing, add the triethanolamine of 0.2g, after fully mixing, obtain the finished product of 100g.
Composed as follows by the disinfection hand cleanser of known the present embodiment of preparation method of the present embodiment disinfection hand cleanser:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban): 0.05%
Ethanol: 30%
Fructus Litseae essential oil: 0.02%
Sweet orange oil: 0.01%
Cremophor RH40 (being CO-40): 0.09%
Betaine (being betanin): 0.3%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.2%
Triethanolamine: 0.2%
Deionized water: 69.13%
Embodiment 2 is containing the preparation of the disinfection hand cleanser of natural plant essential oils
By the N-of 0.06g (4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban) joins in the ethanol of 35g and fully dissolves, then add the Cremophor RH40 (being CO-40) by the Fructus Litseae essential oil of 0.01g, the sweet orange oil of 0.02g and 0.09g to pass through the mixed liquor mixing, and fully mix to such an extent that A is mutually standby.The card ripple U20 (being Carbopol Ultrez 20 polymer) of the Betaine of 0.5g (being betanin) and 0.25g is joined and in the deionized water of 63.82g, after heating, fully dissolve cooling standingly, obtain B mutually standby.By above-mentioned A be added to B quite in, after fully mixing, add the triethanolamine of 0.25g, after fully mixing, obtain the finished product of 100g.
Composed as follows by the disinfection hand cleanser of known the present embodiment of preparation method of the present embodiment disinfection hand cleanser:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban): 0.06%
Ethanol: 35%
Fructus Litseae essential oil: 0.01%
Sweet orange oil: 0.02%
Cremophor RH40 (being CO-40): 0.09%
Betaine (being betanin): 0.5%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.25%
Triethanolamine: 0.25%
Deionized water: 63.82%
Embodiment 3 is containing the preparation of the disinfection hand cleanser of natural plant essential oils
By the N-of 0.05g (4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban) joins in the ethanol of 30g and fully dissolves, then add the Cremophor RH40 (being CO-40) by the Fructus Litseae essential oil of 0.01g, the sweet orange oil of 0.01g and 0.06g to pass through the mixed liquor mixing, and fully mix to such an extent that A is mutually standby.The card ripple U20 (being Carbopol Ultrez 20 polymer) of the Betaine of 0.4g (being betanin) and 0.15g is joined and in the deionized water of 69.17g, after heating, fully dissolve cooling standingly, obtain B mutually standby.By above-mentioned A be added to B quite in, after fully mixing, add the triethanolamine of 0.15g, after fully mixing, obtain the finished product of 100g.
Composed as follows by the disinfection hand cleanser of known the present embodiment of preparation method of the present embodiment disinfection hand cleanser:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (having another name called triclocarban): 0.05%
Ethanol: 30%
Fructus Litseae essential oil: 0.01%
Sweet orange oil: 0.01%
Cremophor RH40 (CO-40): 0.06%
Betaine (being betanin): 0.4%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.15%
Triethanolamine: 0.15%
Deionized water: 69.17%
Embodiment 4 is containing the preparation of the disinfection hand cleanser of natural plant essential oils
By the N-of 0.07g (4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban) joins in the ethanol of 35g and fully dissolves, then add the Cremophor RH40 (being CO-40) by the Fructus Litseae essential oil of 0.02g, the sweet orange oil of 0.02g and 0.09g to pass through the mixed liquor mixing, and fully mix to such an extent that A is mutually standby.The card ripple U20 (being Carbopol Ultrez20 polymer) of the Betaine of 0.5g (being betanin) and 0.2g is joined and in the deionized water of 63.9g, after heating, fully dissolve cooling standingly, obtain B mutually standby.By above-mentioned A be added to B quite in, after fully mixing, add the triethanolamine of 0.2g, after fully mixing, obtain the finished product of 100g.
Composed as follows by the disinfection hand cleanser of known the present embodiment of preparation method of the present embodiment disinfection hand cleanser:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (having another name called triclocarban): 0.07%
Ethanol: 35%
Fructus Litseae essential oil: 0.02%
Sweet orange oil: 0.02%
Cremophor RH40 (being CO-40): 0.09%
Betaine (being betanin): 0.5%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.2%
Triethanolamine: 0.2%
Deionized water: 63.9%
Embodiment 5 is containing the preparation of the disinfection hand cleanser of natural plant essential oils
By the N-of 0.05g (4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban) joins in the ethanol of 25g and fully dissolves, then add the Cremophor RH40 (being CO-40) by the Fructus Litseae essential oil of 0.01g, the sweet orange oil of 0.01g and 0.05g to pass through the mixed liquor mixing, and fully mix to such an extent that A is mutually standby.The card ripple U20 (being Carbopol Ultrez 20 polymer) of the Betaine of 0.2g (being betanin) and 0.15g is joined and in the deionized water of 74.38g, after heating, fully dissolve cooling standingly, obtain B mutually standby.By above-mentioned A be added to B quite in, after fully mixing, add the triethanolamine of 0.15g, after fully mixing, obtain the finished product of 100g.
Composed as follows by the disinfection hand cleanser of known the present embodiment of preparation method of the present embodiment disinfection hand cleanser:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (having another name called triclocarban): 0.05%
Ethanol: 25%
Fructus Litseae essential oil: 0.01%
Sweet orange oil: 0.01%
Cremophor RH40 (being CO-40): 0.05%
Betaine (being betanin): 0.2%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.15%
Triethanolamine: 0.15%
Deionized water: 74.38%
Embodiment 6 is containing the preparation of the disinfection hand cleanser of natural plant essential oils
By the N-of 0.1g (4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (being triclocarban) joins in the ethanol of 35g and fully dissolves, then add the Cremophor RH40 (being CO-40) by the Fructus Litseae essential oil of 0.025g, the sweet orange oil of 0.025g and 0.1g to pass through the mixed liquor mixing, and fully mix to such an extent that A is mutually standby.The card ripple U20 (being Carbopol Ultrez20 polymer) of the Betaine of 0.5g (being betanin) and 0.3g is joined and in the deionized water of 63.65g, after heating, fully dissolve cooling standingly, obtain B mutually standby.By above-mentioned A be added to B quite in, after fully mixing, add the triethanolamine of 0.3g, after fully mixing, obtain the finished product of 100g.
Composed as follows by the disinfection hand cleanser of known the present embodiment of preparation method of the present embodiment disinfection hand cleanser:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea (having another name called triclocarban): 0.1%
Ethanol: 35%
Fructus Litseae essential oil: 0.025%
Sweet orange oil: 0.025%
Cremophor RH40 (CO-40): 0.1%
Betaine (being betanin): 0.5%
Card ripple U20 (being Carbopol Ultrez 20 polymer): 0.3%
Triethanolamine: 0.3%
Deionized water: 63.65%
Embodiment 7 is containing the antibacterial action of the disinfection hand cleanser of natural plant essential oils
1, material
Test strain: staphylococcus aureus ATCC 6538, colon bacillus 8099, Candida albicans ATCC 10231, Pseudomonas aeruginosa ATCC 15442.
Nertralizer formula: sodium thiosulfate 10g+ tween (80) 20g+ lecithin 3.0g+PBS 1000mL.
Testing sample: press the disinfection hand cleanser containing natural plant essential oils of embodiment 1 preparation, by the disinfection hand cleanser containing natural plant essential oils of embodiment 2 preparations, by the disinfection hand cleanser containing natural plant essential oils of embodiment 3 preparations, by the disinfection hand cleanser containing natural plant essential oils of embodiment 4 preparations, the disinfection hand cleanser that contains natural plant essential oils of preparing by embodiment 5 and the disinfection hand cleanser that contains natural plant essential oils prepared by embodiment 6.
2, method
With reference to the evaluation methodology > > of the QB/T 2738-2012 < < daily chemical products antibacterial bacteriostatic effect bactericidal effect method of inspection (suspension quantitative method) of 7.2 antimicrobial form daily chemical products wherein
3, result
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils by embodiment 1 preparation sees the following form 1:
Table 1
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils by embodiment 2 preparations sees the following form 2:
Table 2
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils by embodiment 3 preparations sees the following form 3:
Table 3
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils by embodiment 4 preparations sees the following form 4:
Table 4
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils by embodiment 5 preparations sees the following form 5:
Table 5
The disinfection hand cleanser sterilizing rate result of the test containing natural plant essential oils by embodiment 6 preparations sees the following form 6:
Table 6
4, conclusion
The present invention presses the disinfection hand cleanser containing natural plant essential oils of embodiment 1 preparation, press the disinfection hand cleanser containing natural plant essential oils of embodiment 2 preparations, press the disinfection hand cleanser containing natural plant essential oils of embodiment 3 preparations, press the disinfection hand cleanser containing natural plant essential oils of embodiment 4 preparations, the disinfection hand cleanser containing natural plant essential oils of pressing the disinfection hand cleanser containing natural plant essential oils of embodiment 5 preparations and preparing by embodiment 6 is to staphylococcus aureus, colon bacillus, these the 4 kinds of microorganisms of Candida albicans and Pseudomonas aeruginosa have significant bactericidal action, can be for the sterilizing use that comprises that daily life is required.
Claims (10)
1. the disinfection hand cleanser containing natural plant essential oils, comprise N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea, ethanol, Betaine, Carbopol Ultrez 20 polymer, triethanolamine and deionized water, also is characterized by and contain: Fructus Litseae essential oil, sweet orange oil and Cremophor RH40.
2. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 1, is characterized by the component that contains following weight ratio:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea: 0.05%～0.1%;
Ethanol: 25%～35%;
Fructus Litseae essential oil: 0.01%～0.025%;
Sweet orange oil: 0.01%～0.025%;
Cremophor RH40: 0.05%～0.1%;
Betaine: 0.2%～0.5%;
Carbopol Ultrez 20 polymer: 0.15%～0.3%;
Triethanolamine: 0.15%～0.3%;
Deionized water: 63.65%～74.38%.
3. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 2, is characterized by the component that contains following weight ratio:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea: 0.05%;
Ethanol: 30%;
Fructus Litseae essential oil: 0.02%;
Sweet orange oil: 0.01%;
Cremophor RH40: 0.09%;
Betaine: 0.3%;
Carbopol Ultrez 20 polymer: 0.2%;
Triethanolamine: 0.2%;
Deionized water: 69.13%.
4. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 2, is characterized by the component that contains following weight ratio:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea: 0.06%;
Ethanol: 35%;
Fructus Litseae essential oil: 0.01%;
Sweet orange oil: 0.02%;
Cremophor RH40: 0.09%;
Betaine: 0.5%;
Carbopol Ultrez 20 polymer: 0.25%;
Triethanolamine: 0.25%;
Deionized water: 63.82%.
5. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 2, is characterized by the component that contains following weight ratio:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea: 0.05%～0.07%;
Ethanol: 30%～35%;
Fructus Litseae essential oil: 0.01%～0.02%;
Sweet orange oil: 0.01%～0.02%;
Cremophor RH40: 0.06%～0.09%;
Betaine: 0.4%～0.5%;
Carbopol Ultrez 20 polymer: 0.15%～0.2%;
Triethanolamine: 0.15%～0.2%;
Deionized water: 63.9%～69.17%.
6. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 5, is characterized by the component that contains following weight ratio:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea: 0.05%;
Ethanol: 30%;
Fructus Litseae essential oil: 0.01%;
Sweet orange oil: 0.01%;
Cremophor RH40: 0.06%;
Betaine: 0.4%;
Carbopol Ultrez 20 polymer: 0.15%;
Triethanolamine: 0.15%;
Deionized water: 69.17%.
7. a kind of disinfection hand cleanser containing natural plant essential oils according to claim 5, is characterized by the component that contains following weight ratio:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea: 0.07%
Ethanol: 35%
Fructus Litseae essential oil: 0.02%
Sweet orange oil: 0.02%
Cremophor RH40: 0.09%
Betaine: 0.5%
Carbopol Ultrez 20 polymer: 0.2%
Triethanolamine: 0.2%
Deionized water: 63.9%
8. a method of preparing the disinfection hand cleanser containing natural plant essential oils as described in claim 1-7 any one, its step is as follows:
N-(4-chlorphenyl)-N'-(3,4-Dichlorobenzene base) urea is joined in ethanol and fully dissolved, then add the mixed liquor through mixing by Fructus Litseae essential oil, sweet orange oil and Cremophor RH40, and fully mix to such an extent that A is mutually standby; Betaine and Carbopol Ultrez 20 polymer are joined and in deionized water, after heating, fully dissolve cooling standingly, obtain B mutually standby; By above-mentioned A be added to B quite in, after fully mixing, add triethanolamine, after fully mixing, obtain finished product.
9. the application of the disinfection hand cleanser containing natural plant essential oils described in claim 1-7 any one in configuration or preparation dissipation pathogenic bacterium liquid.
10. application according to claim 9, is characterized by pathogenic bacterium and is: staphylococcus aureus, colon bacillus, Candida albicans and Pseudomonas aeruginosa.
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| CN107412090A (en) * | 2017-04-26 | 2017-12-01 | 烟台新时代健康产业日化有限公司 | A kind of long-acting bacteriostatic composition and its preparation method and application |
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