CN104152055A - Concentrated liquid used for preparing leather polishing nursing products, and use thereof - Google Patents
Concentrated liquid used for preparing leather polishing nursing products, and use thereof Download PDFInfo
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Abstract
The invention discloses a concentrated liquid used for preparing leather polishing nursing products, and a use thereof. The concentrated liquid can be rapidly dissolved in cold water, is stable in the cold water without layering, still has excellent polishing and nursing efficacies after thirty-fold dilution, is very suitable for the production application of functional wet wipes and other leather nourishing polishing products, is convenient to add, and does not need an emulsification technology.
Description
Technical field
The present invention relates to a kind of concentrated solution and purposes of polishing leather care products, be mainly used in the preparation of polishing leather care products.
Background technology
Polishing leather care products mainly comprises in the market: a kind of is polishing leather nursing sprays, is mainly used in the glossing care of fur clothing, leather sofa and automotive leather interior trim; Be a polishing leather conditioning liquid, adopt nursing brush or other soft cotton to carry out wiping leatherware; Also having a kind of is polishing leather nursing wet tissue, the main steeping fluid with glossing care effect that adopts, and with non-woven fabrics, as carrier, wiping leatherware, is disposable product.Leather nursing glazing spray and glazing liquid, owing to carrying inconvenience, limited its use range.Wet tissue is as the growth of one-time consumption product in recent years and develop rapidly.Its functional product, as kitchen cleaning wet tissue, polishing leather nursing wet tissue, cleaning glass wet tissue etc., is more and more subject to consumers in general's favor.
Polishing leather nursing generally all adopts the organic composition with nursing and glazing, such as vegetable wax, animal wax, mineral wax, synthesis modification wax, organosilicon etc.The steeping fluid of using as wet tissue, generally all adopts the form of emulsion to give the function of nursing glazing.But for wet tissue manufacturing enterprise, a large amount of production emulsions are cumbersome things.Show as: the firstth, power consumption, preparation emulsion need to be heated to water more than 80 ℃, more than again the oil phases such as various solid wax being heated to fusing point, being stirred to solid wax is dissolved in oil phase completely, water is slowly joined in oil phase, mixing and emulsifying is carried out in lasting stirring, and this needs considerable heat energy; Even if adopt low-energy emulsification method, because turnout is large, also consume energy very much, after emulsification, to lower the temperature again, heat energy major part has all lost, and does not meet the mode of production of current environmental protection.The secondth, consuming time, in whole emulsion process, the heat-up time of water and oil phase, mixing and emulsifying time and temperature fall time, need the time longer, is unfavorable for scale operation.The 3rd is to need special equipment, and traditional stirred autoclave can not reach the function demand of emulsification, and preparation emulsion needs emulsion tank, and this occupies very large cost on producing.Therefore it is necessary, preparing a kind of (cold water preparation, dissolves fast) easy to use, diluent good stability, using the leather nursing glazing wet tissue concentrated solution of (allotment of can filling a prescription as required) flexibly.
It is fewer that polishing leather is nursed special-purpose wet tissue concentrated solution in the market.This concentrated solution not only will guarantee to dilute stability and the glossing care function of rear solution, also will guarantee that glossing care active component content is enough high, like this glossing care function of diluent after guarantee dilution.China Patent Publication No. CN101802117A, open day on 08 11st, 2008, invention and created name " polish product that does not contain volatile constituent ", this application case discloses a kind of polish product, the wax component that comprises 20-60%, the non-aqueous non-volatile liquid component of 20-60%, and the lipid fraction of 1-40%, preferred 5-15%, preferred fatty acid, is mainly the small pieces solid existing with thickener form, is not suitable for preparation wet tissue.
China Patent Publication No. CN1297012A, open day 05 month 30 days calendar year 2001, invention and created name " a kind of general fur clothing, leather nursing glazing liquid formula and working method thereof ", comprise brightening agent, mould inhibitor, antioxidant etc., brightening agent has adopted the materials such as Ka Nabala, has the functions such as nursing glazing.China Patent Publication No. CN1167798A, open day on December 17th, 1997, invention and created name " spray leahter care polishing agent ", comprise and take Nitrocellulose as brightening agent main body, add acrylic resin guarantor light guarantor look, and allocate ethyl acetate, silicone oil, dibutyl phthalate, positive alcohol etc. into.Prior art is all generally the nursing that is directly used in leatherware, as wet tissue concentrated solution, use, mainly contain 2 disadvantages: the one, fill a prescription and do not consider dilution problem, in the process of application, may produce breakdown of emulsion, precipitation, the 2nd, after dilution, upper light effect is not very desirable.
Summary of the invention
The invention provides a kind of polishing leather care products that can be used for preparing, as the concentrated solution of wet tissue, cloth for cleaning, cotton etc., its objective is for a kind of polishing leather nursing concentrated solution that can dissolve fast dispersion in cold water (general 10～15 ℃) is provided, and formed emulsion-stabilizing is not stratified.Concentrated solution of the present invention, has optimized the formula of polishing leather nursing activeconstituents, at dilution thirtyfold number still thering is good stability after interior; Find simultaneously, add after emulsifying animal grease in concentrated solution, can significantly improve the upper light effect of diluent, be very suitable for the production application of the leather nursing glazing products such as functional wipes, convenient interpolation, without emulsification process.
According to the present invention, described concentrated solution comprises:
A) oil phase component of 0.5～50 % by weight;
B) emulsifier component of 0.15～30 % by weight;
C) the water component of 40～98 % by weight;
D) binder component of 0.05～5 % by weight.
Described A) oil phase component comprises animal grease, and they are mixtures of a kind of in lard, butter, sheep oil or at least two kinds, also contain the lustering agent component that plays glossiness-giving effect;
A in described concentrated solution) in oil phase, lustering agent is at least one in glossing care wax, silicone oil.
A in described concentrated solution) oil phase % by weight is preferably 2.0～40, and more preferably 3.0～35;
B in described concentrated solution) emulsifying agent % by weight is preferably 0.8～25, and more preferably 1.0～20;
C in described concentrated solution) water % by weight is preferably 45～95, and more preferably 50～90;
D in described concentrated solution) weight of additive % is preferably 0.2～4.5, and more preferably 0.5～2.
The present invention also comprises that described concentrated solution is for the preparation of the purposes of leather nursing glazing product (as wet tissue, cloth for cleaning, cotton), concrete good nursing and the glazing effect of described product.
The present invention also comprises that described concentrated solution can also be for the preparation of leather sprays, glossing care liquid product.
The present invention also comprises a kind of leather nursing glazing product that contains concentrated solution (as wet tissue, cloth for cleaning, cotton, sprays, glossing care liquid), concrete good nursing and the glazing effect of this product.Described concentrated solution comprises:
A) oil phase component of 0.5～50 % by weight; % by weight is preferably 2.0～40, and more preferably 3.0～35;
B) emulsifier component of 0.15～30 % by weight; % by weight is preferably 0.8～25, and more preferably 1.0～20;
C) the water component of 40～98 % by weight; % by weight is preferably 45～95, and more preferably 50～90;
D) binder component of 0.05～5 % by weight; % by weight is preferably 0.2～4.5, and more preferably 0.5～2.
Described A) oil phase component comprises animal grease, and they are mixtures of a kind of in lard, butter, sheep oil or at least two kinds, also contain the lustering agent component that plays glossiness-giving effect;
A in described concentrated solution) in oil phase, lustering agent is at least one in glossing care wax, silicone oil.
The present invention also comprises a kind of preparation method of the leather nursing glazing product (as wet tissue, cloth for cleaning, cotton) that contains concentrated solution, comprising: a) get leather nursing glazing product material ready; B) by after 20～300 times of described concentrated solution dilutions, apply or be soaked on material; C) be prepared into leather nursing glazing product; Leather nursing glazing product prepared by the method has good nursing and upper light effect.Described concentrated solution comprises:
A) oil phase component of 0.5～50 % by weight; % by weight is preferably 2.0～40, and more preferably 3.0～35;
B) emulsifier component of 0.15～30 % by weight; % by weight is preferably 0.8～25, and more preferably 1.0～20;
C) the water component of 40～98 % by weight; % by weight is preferably 45～95, and more preferably 50～90;
D) binder component of 0.05～5 % by weight; % by weight is preferably 0.2～4.5, and more preferably 0.5～2.
Described A) oil phase component comprises animal grease, and they are mixtures of a kind of in lard, butter, sheep oil or at least two kinds, also contain the lustering agent component that plays glossiness-giving effect;
In described concentrated solution, in A oil phase, lustering agent is at least one in glossing care wax, silicone oil.
In described concentrated solution, in A oil phase component, glossing care wax is animal wax, vegetable wax, mineral wax or synthetic wax; Be specially: animal wax is the mixture of a kind of in beeswax, Insect Wax, spermaceti, shellac wax or at least two kinds; Vegetable wax is the mixture of a kind of in rice bran wax, carnauba wax, gama wax, Chinese haze tallow or at least two kinds; Mineral wax is the mixture of a kind of in paraffin, Microcrystalline Wax, montanin wax or at least two kinds; Synthetic wax is the mixture of a kind of in polyethylene wax, oxidized polyethlene wax, hydrogenated castor oil wax, S wax, E wax or at least two kinds.
In described concentrated solution, in A oil phase component, silicone oil specifically comprises the silicone oil of following structure:
In formula, R is alkyl, aryl, and R' is alkyl, aryl, hydrogen, carbon functional group and polyether chain etc.; X is alkyl, aryl, alkenyl, hydrogen, hydroxyl, alkoxyl group, acetoxyl group, chlorine, carbon functional group and polyether chain etc.; N, m=0,1,2,3 For example, methyl-silicone oil, dimethyl silicone oil, ethyl silicon oil, phenyl silicone oil etc.
In described concentrated solution, B emulsifier component is to have the Compositional type emulsifying agent of HLB value (being hydrophile-lipophile balance value) between 6～20, composite by different emulsifying agents, not only can regulate HLB value, more can coordinate the emulsification property of each emulsifying agent, make final emulsion more stable.Specifically comprised two kinds or the mixture of at least three kinds in following four class emulsifying agents, they are:
1) emulsifying agent that contains following structure:
In formula, R is alkyl; N=3,8,9,10,15,20,25,30,35;
2) emulsifying agent that contains following structure:
In formula, R is alkyl; N > 6;
3) sorbitan fatty acid ester, commodity are called sapn, are selected from the mixture of a kind of in Arlacel-20, Arlacel-40, Arlacel-60, Arlacel-80 or at least two kinds.
4) polyoxyethylene sorbitan fatty acid ester, commodity are called tween, are selected from the mixture of a kind of in tween 20, Tween-40, Tween-60, tween-80 or at least two kinds.
In described concentrated solution, B emulsifier component also comprises the mixture of a kind of in the condenses, ethoxylated alkyl sulfate of condenses, hydrogenated castor oil and the oxyethane of Sodium dodecylbenzene sulfonate, palmityl trimethyl ammonium chloride, stearyl dimethyl benzyl ammonium chloride, cetalkonium chloride, dodecyl benzyl dimethyl ammonium chloride, oxyethane and Viscotrol C or at least two kinds.
In described concentrated solution, C water component is water-soluble component, is specifically selected from the mixture of a kind of in butyleneglycol, propylene glycol, C16～18 alcohol, pentanediol, propyl carbinol, primary isoamyl alcohol or at least two kinds and water.
In described concentrated solution, D binder component is trolamine, sodium cellulose glycolate, Walocel MT 20.000PV, Natvosol, sodium hydroxyethyl cellulose, methylisothiazolinone, methylchloroisothiazandnone, BIT, bronopol, diazonium Imidurea, Imidurea, DMDMH (1, two (methylol)-5 of 3-, 5-methylimidazole quinoline-2,4-diketone), two kinds or the mixture of at least three kinds in methylol glycine sodium.
Concentrated solution of the present invention can adopt this area ordinary method preparation; Or preparation method is: 1. by A) and B) component mix post-heating to melted state, be incubated 20～60 minutes, as oil phase, use; 2. by C) be heated to 80～90 ℃, be incubated 20～60 minutes, as water, use; 3. emulsion tank is heated to after 80 ℃, oil phase is added to emulsion tank, then 1/3 water is slowly added in emulsion tank, again by remaining water suction, high-speed stirring, homogeneous 10～40 minutes, emulsification is complete, be incubated 20～60 minutes, add D after being cooled to 40 ℃) component, continues to stir 5～10 minutes.
Polishing leather care products of the present invention includes but not limited to wet tissue, cloth for cleaning, cotton etc.
The advantage that the present invention has is: concentrated solution both can dilute at cold water, and formed diluent is stablized not stratified, leather is had to good nursing and the effect of glazing simultaneously, be very suitable for the production application of polishing leather care products, convenient interpolation, without a large amount of emulsification process, existing extraordinary economic benefit, has again good environment-friendly production process.
Embodiment
The following stated embodiment describes the present invention in detail.In these embodiments, all consumptions all be weight %.
Embodiment 1
The preparation method of 1 to No. 12 concentrated solution of numbering is: 1. by A) and B) component mix post-heating to melted state, be incubated 20～60 minutes, as oil phase, use; 2. by C) be heated to 80～90 ℃, be incubated 20～60 minutes, as water, use; 3. emulsion tank is heated to, after 80 ℃, oil phase be added to emulsion tank, then 1/3 water is slowly added in emulsion tank, again by remaining water suction, high-speed stirring, homogeneous 10～40 minutes, emulsification is complete, insulation half an hour, adds D after being cooled to 40 ℃) component, continues to stir 5～10 minutes.
Table 1. charging capacity of respectively filling a prescription
Note:
AEO-n, n=10,15,20 is fatty alcohol-polyoxyethylene ether, S-40 is Arlacel-40, S-60 Arlacel-60, S-80 Arlacel-80, T-60 is Tween-60, T-40 is Tween-40, and EL-10 is the condenses of oxyethane and Viscotrol C, and HEL-20 is the condenses of oxyethane and hydrogenated castor oil.
Embodiment 2
Diluent stability, will number in embodiment 1 after 5～30 times of 1 to No. 12 cold water for concentrated solution (11 ℃) dilutions, within 24 hours, observes whether layering, the results are shown in Table 2, and the diluent of visible concentrated solution of the present invention does not have demixing phenomenon, has good stability.
The stability of table 2. diluent
Embodiment 3 glossing care evaluations
Evaluate to adopt sensory evaluation method, by numbering in dense embodiment 1 after 5,10 and 20 times of 1 to No. 12 contracting liquid dilutions, with spunlace non-woven cloth (cotton content 60%), flood respectively, water content is controlled at the 300%-400% of non-woven fabrics weight, standby.
With this wet tissue wiping designated area on leather sofa, area is 10cm * 10cm, and evaluation score is 25,50,75 and 100, is expressed as successively glossing care poor effect, general, better, fine.Evaluation number is 5 people, after test, averages, and its result is as shown in table 3.
Table 3. glossing care evaluation result
As can be seen from Table 3, concentrated solution of the present invention, after 20 times of dilutions, evaluation score, more than 50, still has certain glossing care effect, after 5 and 10 times of dilutions, has preferably glossing care effect.Wherein formulation examples 11 and 12 pairs recently see, on identical basic components, add the formula 11 after butter, have significant upper light effect.
Claims (16)
1. for the preparation of a concentrated solution for polishing leather care products, it is characterized in that, described concentrated solution comprises:
A) oil phase component of 0.5～50 % by weight;
B) emulsifier component of 0.15～30 % by weight;
C) the water component of 40～98 % by weight;
D) binder component of 0.05～5 % by weight;
Described A) oil phase component comprises animal grease, and they are mixtures of a kind of in lard, butter, sheep oil or at least two kinds, also contain the lustering agent component that plays glossiness-giving effect;
Described D) binder component is the mixture of a kind of in a kind of in trolamine, sodium cellulose glycolate, Walocel MT 20.000PV, Natvosol, sodium hydroxyethyl cellulose or at least two kinds of mixtures and methylisothiazolinone, methylchloroisothiazandnone, BIT, bronopol, diazonium Imidurea, Imidurea, DMDMH, Sodium hydroxymethyl glycinate or at least two kinds.
2. concentrated solution according to claim 1, is characterized in that, A in described concentrated solution) lustering agent is at least one in glossing care wax, silicone oil in oil phase.
3. concentrated solution according to claim 2, is characterized in that, in described lustering agent component, glossing care wax is animal wax, vegetable wax, mineral wax or synthetic wax.
4. concentrated solution according to claim 3, is characterized in that, described animal wax is the mixture of a kind of in beeswax, Insect Wax, spermaceti, wool wax or at least two kinds; Vegetable wax is the mixture of a kind of in rice bran wax, carnauba wax, gama wax, Chinese haze tallow, sugar-cane wax, laurel wax or at least two kinds; Mineral wax is the mixture of a kind of in paraffin, Microcrystalline Wax, montanin wax or at least two kinds; Synthetic wax is the mixture of a kind of in polyethylene wax, oxidized polyethlene wax, hydrogenated castor oil wax, S wax, E wax or at least two kinds.
5. concentrated solution according to claim 2, is characterized in that, in described lustering agent component, silicone oil is the silicone oil that comprises following structure:
In formula, R is alkyl, aryl, and R' is alkyl, aryl, hydrogen, carbon functional group and polyether chain; X is alkyl, aryl, alkenyl, hydrogen, hydroxyl, alkoxyl group, acetoxyl group, chlorine, carbon functional group and polyether chain; N, m=0,1,2,3 ...
6. concentrated solution according to claim 1, is characterized in that, B in described concentrated solution) emulsifier component comprises two kinds or the mixture of at least three kinds in following four class emulsifying agents, and they are:
1) emulsifying agent that contains following structure:
In formula, R is alkyl; N=3,8,9,10,15,20,25,30,35;
2) emulsifying agent that contains following structure:
In formula, R is alkyl; N > 6;
3) sorbitan fatty acid ester;
4) polyoxyethylene sorbitan fatty acid ester.
7. concentrated solution according to claim 6, is characterized in that, described sorbitan fatty acid ester is the mixture of a kind of in Arlacel-20, Arlacel-40, Arlacel-60, Arlacel-80 or at least two kinds; Described polyoxyethylene sorbitan fatty acid ester is the mixture of a kind of in tween 20, Tween-40, Tween-60, tween-80 or at least two kinds.
8. emulsifier component according to claim 6, wherein also includes the mixture of a kind of in the condenses, ethoxylated alkyl sulfate of condenses, hydrogenated castor oil and the oxyethane of Sodium dodecylbenzene sulfonate, palmityl trimethyl ammonium chloride, stearyl dimethyl benzyl ammonium chloride, cetalkonium chloride, dodecyl benzyl dimethyl ammonium chloride, oxyethane and Viscotrol C or at least two kinds.
9. concentrated solution according to claim 1, is characterized in that, C in described concentrated solution) water component is a kind of in butyleneglycol, propylene glycol, C16～18 alcohol, pentanediol, propyl carbinol, primary isoamyl alcohol or at least two kinds and the mixture of water.
10. according to the arbitrary described concentrated solution of claim 1～9, it is characterized in that,
A in described concentrated solution) oil phase % by weight is 2.0～40;
B in described concentrated solution) emulsifying agent % by weight is 0.8～25;
C in described concentrated solution) water % by weight is 45～95;
D in described concentrated solution) weight of additive % is 0.2～4.5;
Described A) oil phase component comprises animal grease, and they are mixtures of a kind of in lard, butter, sheep oil or at least two kinds, also contain the lustering agent component that plays glossiness-giving effect.
11. concentrated solutions according to claim 10, is characterized in that,
A in described concentrated solution) oil phase % by weight is 3.0～35;
B in described concentrated solution) emulsifying agent % by weight is 1.0～20;
C in described concentrated solution) water % by weight is 50～90;
D in described concentrated solution) weight of additive % is 0.5～2;
Described A) oil phase component comprises animal grease, and they are mixtures of a kind of in lard, butter, sheep oil or at least two kinds, also contain the lustering agent component that plays glossiness-giving effect.
12. according to the purposes of the arbitrary described concentrated solution of claim 1～11, for the preparation of leather nursing glazing product.
13. 1 kinds of leather nursing glazing products that contain concentrated solution, is characterized in that, described concentrated solution is the arbitrary described concentrated solution of claim 1～11.
The preparation method of 14. 1 kinds of leather nursing glazing products that contain concentrated solution, comprising: a) get leather nursing glazing product material ready; B) by after 20～300 times of described concentrated solution dilutions, apply or be soaked on material; C) be prepared into leather nursing glazing product; Leather nursing glazing product prepared by the method has good nursing and upper light effect; Described concentrated solution is the arbitrary described concentrated solution of claim 1～11.
15. according to the preparation method of the arbitrary described concentrated solution of claim 1～11, it is characterized in that, 1. by A) and B) component mix post-heating to melted state, insulation 20-60 minute, is used as oil phase; 2. by C) be heated to 80～90 ℃, insulation 20-60 minute, is used as water; 3. emulsion tank is heated to, after 80 ℃, oil phase be added to emulsion tank, then 1/3 water is slowly added in emulsion tank, again by remaining water suction, high-speed stirring, homogeneous 10～40 minutes, emulsification is complete, is incubated 20-60 minute, adds D after being cooled to 40 ℃) component, continues to stir 5～10 minutes.
16. according to the purposes of the arbitrary described concentrated solution of claim 1～11, for the preparation of leather sprays and polishing leather conditioning liquid product.
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105176409A (en) * | 2015-10-23 | 2015-12-23 | 高大元 | Preparation method of automobile surface polishing agent |
| CN105623529A (en) * | 2016-01-11 | 2016-06-01 | 上海馨臣家化有限公司 | Silicon-oil-containing leather cleaning glazing caring wet tissue |
| CN105779670A (en) * | 2016-04-29 | 2016-07-20 | 四川力久知识产权服务有限公司 | Wax emulsion for leather finishing and preparing method of wax emulsion |
| CN107675552A (en) * | 2017-10-24 | 2018-02-09 | 苏州丰倍生物科技有限公司 | A kind of plant type paper products water and oil repellent agent capable of washing and preparation method thereof |
| CN108441341A (en) * | 2018-03-21 | 2018-08-24 | 陈溢豪 | Water-soluble wax car washing liquid and preparation method thereof |
| CN108587193A (en) * | 2018-04-16 | 2018-09-28 | 江南大学 | A kind of pair of distributed compound wax emulsion and preparation method thereof |
| CN108864951A (en) * | 2018-08-09 | 2018-11-23 | 台州智子科技有限公司 | A kind of shoe polish and preparation method thereof with anti-aging function |
| CN108913037A (en) * | 2018-08-09 | 2018-11-30 | 上海皇宇科技发展有限公司 | A kind of nano-scale multifunctional light care agent and preparation method thereof |
| CN114317843A (en) * | 2021-12-29 | 2022-04-12 | 山东省润荷卫生材料有限公司 | Wet tissue for renovating leather products and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105176409A (en) * | 2015-10-23 | 2015-12-23 | 高大元 | Preparation method of automobile surface polishing agent |
| CN105623529A (en) * | 2016-01-11 | 2016-06-01 | 上海馨臣家化有限公司 | Silicon-oil-containing leather cleaning glazing caring wet tissue |
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| CN108587193A (en) * | 2018-04-16 | 2018-09-28 | 江南大学 | A kind of pair of distributed compound wax emulsion and preparation method thereof |
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| CN108913037A (en) * | 2018-08-09 | 2018-11-30 | 上海皇宇科技发展有限公司 | A kind of nano-scale multifunctional light care agent and preparation method thereof |
| CN114317843A (en) * | 2021-12-29 | 2022-04-12 | 山东省润荷卫生材料有限公司 | Wet tissue for renovating leather products and preparation method thereof |
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Application publication date: 20141119 |