CN104148562A - Cogging method for Ti2AlNb-based alloy ingot - Google Patents

Cogging method for Ti2AlNb-based alloy ingot Download PDF

Info

Publication number
CN104148562A
CN104148562A CN201410304835.6A CN201410304835A CN104148562A CN 104148562 A CN104148562 A CN 104148562A CN 201410304835 A CN201410304835 A CN 201410304835A CN 104148562 A CN104148562 A CN 104148562A
Authority
CN
China
Prior art keywords
fire
ti2alnb
base alloy
based alloy
temperature
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201410304835.6A
Other languages
Chinese (zh)
Other versions
CN104148562B (en
Inventor
杨晋
苏海
张衡
朱灵华
邹善垚
彭泉兴
彭华栋
张小林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Gaona Aero Material Co Ltd
AVIC Guizhou Anda Aviation Forging Co Ltd
Original Assignee
Guizhou Anda Aviation Forging Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guizhou Anda Aviation Forging Co Ltd filed Critical Guizhou Anda Aviation Forging Co Ltd
Priority to CN201410304835.6A priority Critical patent/CN104148562B/en
Publication of CN104148562A publication Critical patent/CN104148562A/en
Application granted granted Critical
Publication of CN104148562B publication Critical patent/CN104148562B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Forging (AREA)

Abstract

The invention discloses a cogging method for a Ti2AlNb-based alloy ingot. The cogging method comprises the steps that the Ti2AlNb-based alloy ingot is loaded on a wire cutting machine and manufactured into a Phi290*280mm bar; the Ti2AlNb-based alloy ingot is sleeved with alumina silicate fibers, placed into a high-temperature heating furnace to be heated to 1150 DEG C and then placed on a press after the temperature is kept for 80 minutes, and repeated upsetting and drawing are performed at the strain rate of 0.01S-1; the ingot is drawn out to 350mm after first fire, upset to 350mm after second fire, drawn out to 350mm after third fire, upset to 270mm after fourth fire and drawn out to 350mm after fifth fire, and air cooling is performed. The ingot is returned to the furnace to be heated to 1150 DEG C and the temperature is kept for 40 minutes for each fire, and the final forging temperature of each fire is guaranteed to be equal to or larger than 1050 DEG C. According to the method, the steady state deformation resistance of the Ti2AlNb-based alloy ingot is reduced in a fully dynamic recrystallization state, the technological plasticity is improved, cracking is prevented, a cast structure is smashed completely, and a uniform and dense forge structure is obtained.

Description

Ti 2the cogging method of AlNb base alloy cast ingot
Technical field
The present invention relates to a kind of cogging method of ingot casting, particularly related to Ti 2the cogging method of AlNb base alloy cast ingot.
Background technology
Ti 2alNb base alloy is a kind of novel lightweight high-temperature structural material, it is to have Ti, the intermetallic compound that Al and Nb form, such alloy is with O phase, B2/ β phase is two-phase or the three-phase composite tissue forming with α 2 mutually, there is density low, elastic modelling quantity is high, elevated temperature strength is high, fracture property is high, creep resistance is high, hot expansibility is low, the advantages such as nonmagnetic and fire resistance is good, compare with high-temperature titanium alloy and there is higher serviceability temperature, creep-resistant property and elevated temperature strength, its density and thermal coefficient of expansion are starkly lower than nickel base superalloy again, it is the preferably selection that replaces titanium alloy and high temperature alloy in following aerospace field, have broad application prospects.
Ti 2although AlNb base alloy has many good qualities, but there is a fatal weakness, the malleability of this alloy is very poor, controls bad very easy generation forging crack.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of forging method that adopts three pullings and twice jumping-up, realizes Ti 2the cogging of AlNb base alloy cast ingot.The method can make Ti 2alNb base alloy reduces its stead deformation drag, improves process plastic under the state of complete dynamic recrystallization, prevents cogging crackle, makes as-cast structure completely broken, obtains even, fine and close as-forged microstructure.
For solving the problems of the technologies described above, Ti of the present invention 2the cogging method of AlNb base alloy cast ingot, its technical scheme comprises the following steps:
By Ti 2on AlNb base alloy cast ingot, wire cutting machine is made the bar of a φ 290 * 280mm; Adopt alumina silicate fibre to Ti 2alNb base alloy cast ingot carries out after jacket, inserts and in high-temperature heater, is heated to 1150 ℃ of insulations after 80 minutes on placement force machine, with 0.01S -1strain rate carry out repeatedly jumping-up, pulling: the first fire pulls out to 350mm, and the second fiery jumping-up is to 270mm, and the 3rd fire pulls out to 350mm, and the 4th fiery jumping-up is to 270mm, and the 5th fire pulls out to 350mm, air cooling; Between every fire time, melt down and be heated to 1150 ℃ of insulations 40 minutes, guarantee that the final forging temperature of every fire time should>=1050 ℃.
Compared with prior art, beneficial effect of the present invention is as follows:
Ti of the present invention 2the cogging method of AlNb base alloy cast ingot, the deformation temperature interval that it adopts is 1050 ℃~1150 ℃, and this temperature range is B2 monophase field, when this temperature range distortion, there is the dynamic recrystallization of continuous recrystallization mechanism in B2 crystal grain, can broken as-cast structure by dynamic recrystallization.Meanwhile, under this condition, in the time of can guaranteeing ingot casting distortion, there is good process plastic, can guarantee that again this alloy has lower stead deformation drag when distortion.
Consider when forging, need to enhance productivity as far as possible, reduce the temperature drop of workpiece, and make Ti 2alNb base alloy is recrystallization fully, and during cogging, selected strain rate is Ti 2can there is the strain rate higher limit 0.01S of dynamic recrystallization in AlNb base alloy -1.
The present invention adopts the repeatedly cogging technics of pulling+jumping-up, makes in cogging process, and its total deformation arrives more than 50%, better broken Ti 2alNb base As-cast Microstructure, forges and closes Ti 2alNb base alloy internal flaw, makes microstructure homogenization.
The specific embodiment
Implement Ti of the present invention 2the cogging method of AlNb base alloy cast ingot, need to provide the equipment such as forging high-temperature heating furnace, forcing press, manipulator.The specific embodiment is as follows:
Ti is provided 2alNb base alloy cast ingot, its nominal chemical composition is: Ti-22Al-25Nb.
The cogging technics step of this alloy is as follows:
By Ti 2on AlNb base alloy cast ingot, wire cutting machine is made the bar of a φ 290 * 280mm; Adopt alumina silicate fibre to Ti 2alNb base alloy cast ingot carries out after jacket, inserts and in high-temperature heater, is heated to 1150 ℃ of insulations after 80 minutes on placement force machine, with 0.01S -1strain rate carry out repeatedly jumping-up, pulling: the first fire pulls out to 350mm, and the second fiery jumping-up is to 270mm, and the 3rd fire pulls out to 350mm, and the 4th fiery jumping-up is to 270mm, and the 5th fire pulls out to 350mm, air cooling; Between every fire time, melt down and be heated to 1150 ℃ of insulations 40 minutes, guarantee that the final forging temperature of every fire time should>=1050 ℃.

Claims (2)

1. a Ti 2the cogging method of AlNb base alloy cast ingot, is characterized in that, comprises the following steps:
By Ti 2on AlNb base alloy cast ingot, wire cutting machine is made the bar of a φ 290 * 280mm; Adopt alumina silicate fibre to Ti 2alNb base alloy cast ingot carries out after jacket, inserts and in high-temperature heater, is heated to 1150 ℃ of insulations after 80 minutes on placement force machine, with 0.01S -1strain rate carry out repeatedly jumping-up, pulling: the first fire pulls out to 350mm, and the second fiery jumping-up is to 270mm, and the 3rd fire pulls out to 350mm, and the 4th fiery jumping-up is to 270mm, and the 5th fire pulls out to 350mm, air cooling; Between every fire time, melt down and be heated to 1150 ℃ of insulations 40 minutes, guarantee that the final forging temperature of every fire time should>=1050 ℃.
2. according to the Ti described in claim 1~2 2the cogging method of AlNb base alloy cast ingot, is characterized in that, described Ti 2the nominal composition of AlNb base alloy is Ti-22Al-25Nb.
CN201410304835.6A 2014-06-30 2014-06-30 Cogging method for Ti2AlNb-based alloy ingot Active CN104148562B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410304835.6A CN104148562B (en) 2014-06-30 2014-06-30 Cogging method for Ti2AlNb-based alloy ingot

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410304835.6A CN104148562B (en) 2014-06-30 2014-06-30 Cogging method for Ti2AlNb-based alloy ingot

Publications (2)

Publication Number Publication Date
CN104148562A true CN104148562A (en) 2014-11-19
CN104148562B CN104148562B (en) 2017-01-11

Family

ID=51874295

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410304835.6A Active CN104148562B (en) 2014-06-30 2014-06-30 Cogging method for Ti2AlNb-based alloy ingot

Country Status (1)

Country Link
CN (1) CN104148562B (en)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106319236A (en) * 2016-11-01 2017-01-11 西北有色金属研究院 Preparation method of Ti2AlNb alloy material
CN106914508A (en) * 2017-02-17 2017-07-04 中国航空工业集团公司北京航空材料研究院 A kind of Ti2The preparation method of AlNb alloy wires
CN107952922A (en) * 2017-11-07 2018-04-24 西北工业大学 A kind of method of TiAl alloy cogging forging
CN111230007A (en) * 2020-02-27 2020-06-05 无锡派克新材料科技股份有限公司 Forging method of 1000Kg grade high temperature alloy
CN111394637A (en) * 2020-04-17 2020-07-10 中国航发北京航空材料研究院 Ti2AlNb alloy and preparation method of bar thereof
CN111607751A (en) * 2020-06-09 2020-09-01 无锡派克新材料科技股份有限公司 Forging modifying method for Ti2AlNb alloy
CN112275966A (en) * 2020-12-24 2021-01-29 北京钢研高纳科技股份有限公司 Large specification of Ti2AlNb alloy ring piece and manufacturing method thereof
CN112410698A (en) * 2020-11-03 2021-02-26 中国航发北京航空材料研究院 Three-phase Ti2AlNb alloy multilayer structure uniformity control method
CN114273583A (en) * 2021-12-23 2022-04-05 北京钢研高纳科技股份有限公司 Ti2AlNb-based alloy plate and preparation method and application thereof
CN115971492A (en) * 2022-09-30 2023-04-18 北京钢研高纳科技股份有限公司 Ti2AlNb alloy plate and preparation method and application thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5190603A (en) * 1990-07-04 1993-03-02 Asea Brown Boveri Ltd. Process for producing a workpiece from an alloy containing dopant and based on titanium aluminide
US6132526A (en) * 1997-12-18 2000-10-17 Societe Nationale D'etude Et De Construction De Moteurs D'aviation "Snecma" Titanium-based intermetallic alloys
CN1683097A (en) * 2005-03-04 2005-10-19 宝钢集团上海五钢有限公司 Heat keeping and forging and blank cogging method for GH742 alloy large steel ingot
CN101569763A (en) * 2009-03-30 2009-11-04 上海理工大学 Biomedical beta-titanium alloy material and preparation method thereof
CN103695826A (en) * 2013-12-20 2014-04-02 钢铁研究总院 Fine-grain forging method for large-size GH690 nickel-based alloy bar billet

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5190603A (en) * 1990-07-04 1993-03-02 Asea Brown Boveri Ltd. Process for producing a workpiece from an alloy containing dopant and based on titanium aluminide
US6132526A (en) * 1997-12-18 2000-10-17 Societe Nationale D'etude Et De Construction De Moteurs D'aviation "Snecma" Titanium-based intermetallic alloys
CN1683097A (en) * 2005-03-04 2005-10-19 宝钢集团上海五钢有限公司 Heat keeping and forging and blank cogging method for GH742 alloy large steel ingot
CN101569763A (en) * 2009-03-30 2009-11-04 上海理工大学 Biomedical beta-titanium alloy material and preparation method thereof
CN103695826A (en) * 2013-12-20 2014-04-02 钢铁研究总院 Fine-grain forging method for large-size GH690 nickel-based alloy bar billet

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106319236B (en) * 2016-11-01 2018-08-17 西北有色金属研究院 A kind of preparation method of Ti2AlNb alloy materials
CN106319236A (en) * 2016-11-01 2017-01-11 西北有色金属研究院 Preparation method of Ti2AlNb alloy material
CN106914508A (en) * 2017-02-17 2017-07-04 中国航空工业集团公司北京航空材料研究院 A kind of Ti2The preparation method of AlNb alloy wires
CN106914508B (en) * 2017-02-17 2018-05-29 中国航空工业集团公司北京航空材料研究院 A kind of Ti2The preparation method of AlNb alloy wires
CN107952922A (en) * 2017-11-07 2018-04-24 西北工业大学 A kind of method of TiAl alloy cogging forging
CN111230007A (en) * 2020-02-27 2020-06-05 无锡派克新材料科技股份有限公司 Forging method of 1000Kg grade high temperature alloy
CN111394637A (en) * 2020-04-17 2020-07-10 中国航发北京航空材料研究院 Ti2AlNb alloy and preparation method of bar thereof
CN111394637B (en) * 2020-04-17 2021-06-01 中国航发北京航空材料研究院 Ti2AlNb alloy and preparation method of bar thereof
CN111607751A (en) * 2020-06-09 2020-09-01 无锡派克新材料科技股份有限公司 Forging modifying method for Ti2AlNb alloy
CN112410698B (en) * 2020-11-03 2021-11-02 中国航发北京航空材料研究院 Three-phase Ti2AlNb alloy multilayer structure uniformity control method
CN112410698A (en) * 2020-11-03 2021-02-26 中国航发北京航空材料研究院 Three-phase Ti2AlNb alloy multilayer structure uniformity control method
CN112275966A (en) * 2020-12-24 2021-01-29 北京钢研高纳科技股份有限公司 Large specification of Ti2AlNb alloy ring piece and manufacturing method thereof
CN114273583A (en) * 2021-12-23 2022-04-05 北京钢研高纳科技股份有限公司 Ti2AlNb-based alloy plate and preparation method and application thereof
CN114273583B (en) * 2021-12-23 2022-12-09 北京钢研高纳科技股份有限公司 Ti 2 AlNb-based alloy plate and preparation method and application thereof
CN115971492A (en) * 2022-09-30 2023-04-18 北京钢研高纳科技股份有限公司 Ti2AlNb alloy plate and preparation method and application thereof
CN115971492B (en) * 2022-09-30 2024-03-15 北京钢研高纳科技股份有限公司 Ti2AlNb alloy plate and preparation method and application thereof

Also Published As

Publication number Publication date
CN104148562B (en) 2017-01-11

Similar Documents

Publication Publication Date Title
CN104148562B (en) Cogging method for Ti2AlNb-based alloy ingot
CN104139139B (en) Ti2the roll forming of AlNb base alloy casing ring and heat treatment method
CN105506525B (en) Preparation method of Ti2AlNb-based alloy large-size uniform fine-grain bar
CN102230097B (en) Preparation method of titanium alloy bars
CN107824731B (en) A kind of Ti55 titanium alloy large size bar forging method
CN103341586B (en) Method for achieving forming of GH4738 nickel-base superalloy turbine discs
CN103469136B (en) The preparation method of the TC11 titanium alloy cake material that a kind of fatigue strength is high
CN104532057B (en) A kind of Ti6242 titanium alloy and the preparation method of small-sized bar thereof
CN101927312B (en) Method for processing TC4 titanium alloy into forged rings
CN107217221B (en) A kind of preparation method of high uniform Ti-15Mo titanium alloys bar stock
CN106591625A (en) Titanium alloy with matched high strength and toughness and preparation process of titanium alloy
CN109500330A (en) A kind of cogging method of the big size ingot-casting of nickel-base alloy
CN106555076A (en) A kind of resistance to 650 DEG C of high-temperature titanium alloy materials and preparation method thereof
CN104388860B (en) A kind of nickel base superalloy finish forge cogging method
CN107952794B (en) Single fiery milling method of TC4 titanium alloy cut deal
CN104001845B (en) Forging process method of Ti2AlNb alloy large-size disk parts
CN103302214A (en) Difficultly-deformed nickel-based superalloy superplastic forming method
CN105238955B (en) A kind of high-ductility zircaloy and preparation method thereof
JP2010280002A (en) Method for manufacturing forged piece from gamma titanium-aluminum-based alloy
CN106319236A (en) Preparation method of Ti2AlNb alloy material
CN111906225A (en) Forging method of oversized Ti80 titanium alloy forging stock
CN107815627A (en) A kind of heat-treatment technology method of the 3D printing Inconel718 nickel-base alloys based on selective laser fusing
CN106914508A (en) A kind of Ti2The preparation method of AlNb alloy wires
CN102251146B (en) Nickel-titanium-aluminum-based high-temperature alloy material and isothermal forging preparation method thereof
CN104046846A (en) Multilevel high-strength high-plasticity titanium-zirconium-based alloy and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant
TR01 Transfer of patent right
TR01 Transfer of patent right

Effective date of registration: 20190808

Address after: 561005 East Suburb of Xixiu District, Anshun City, Guizhou Province

Co-patentee after: BEIJING CISRI-GAONA MATERILALS & TECHNOLOGY Co., LTD.

Patentee after: Anda Aviation Forging Co., Ltd., Guizhou

Address before: 561005 Guizhou city of Anshun province Xixiu District No. 322 East Huangguoshu Waterfalls Street

Patentee before: Anda Aviation Forging Co., Ltd., Guizhou