CN104140692B - 一种疏水效果好的改性纳米二氧化钛及其制备方法 - Google Patents
一种疏水效果好的改性纳米二氧化钛及其制备方法 Download PDFInfo
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- CN104140692B CN104140692B CN201410327907.9A CN201410327907A CN104140692B CN 104140692 B CN104140692 B CN 104140692B CN 201410327907 A CN201410327907 A CN 201410327907A CN 104140692 B CN104140692 B CN 104140692B
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- Prior art keywords
- powder
- nano
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- stir
- titanium dioxide
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- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical class [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 title claims abstract description 15
- 230000002209 hydrophobic effect Effects 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title claims description 7
- 239000000843 powder Substances 0.000 claims abstract description 31
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 26
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 15
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 14
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 claims abstract description 14
- 229920001903 high density polyethylene Polymers 0.000 claims abstract description 14
- 239000004700 high-density polyethylene Substances 0.000 claims abstract description 14
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 13
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 10
- 239000004814 polyurethane Substances 0.000 claims abstract description 9
- 229920002635 polyurethane Polymers 0.000 claims abstract description 9
- 229910017083 AlN Inorganic materials 0.000 claims abstract description 7
- PIGFYZPCRLYGLF-UHFFFAOYSA-N Aluminum nitride Chemical compound [Al]#N PIGFYZPCRLYGLF-UHFFFAOYSA-N 0.000 claims abstract description 7
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims abstract description 7
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 claims abstract description 7
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004411 aluminium Substances 0.000 claims abstract description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052782 aluminium Inorganic materials 0.000 claims abstract description 7
- 239000007822 coupling agent Substances 0.000 claims abstract description 7
- 229910052749 magnesium Inorganic materials 0.000 claims abstract description 7
- 239000011777 magnesium Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000011029 spinel Substances 0.000 claims abstract description 7
- 229910052596 spinel Inorganic materials 0.000 claims abstract description 7
- 239000011787 zinc oxide Substances 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims description 18
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 6
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 6
- LDCRTTXIJACKKU-ONEGZZNKSA-N dimethyl fumarate Chemical compound COC(=O)\C=C\C(=O)OC LDCRTTXIJACKKU-ONEGZZNKSA-N 0.000 claims description 6
- 229960004419 dimethyl fumarate Drugs 0.000 claims description 6
- 229920001971 elastomer Polymers 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 239000010977 jade Substances 0.000 claims description 6
- 239000011812 mixed powder Substances 0.000 claims description 6
- 239000000725 suspension Substances 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 3
- GEMHFKXPOCTAIP-UHFFFAOYSA-N n,n-dimethyl-n'-phenylcarbamimidoyl chloride Chemical compound CN(C)C(Cl)=NC1=CC=CC=C1 GEMHFKXPOCTAIP-UHFFFAOYSA-N 0.000 claims description 3
- 239000005543 nano-size silicon particle Substances 0.000 claims description 3
- 230000010355 oscillation Effects 0.000 claims description 3
- 229960001866 silicon dioxide Drugs 0.000 claims description 3
- 235000012239 silicon dioxide Nutrition 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 7
- 229920000642 polymer Polymers 0.000 abstract description 2
- 238000009736 wetting Methods 0.000 description 2
- 230000010748 Photoabsorption Effects 0.000 description 1
- 239000004964 aerogel Substances 0.000 description 1
- -1 alcohol titanium salt Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009388 chemical precipitation Methods 0.000 description 1
- 238000005229 chemical vapour deposition Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000593 microemulsion method Methods 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 238000004065 wastewater treatment Methods 0.000 description 1
Landscapes
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
样品 | 原纳米二氧化钛 | 改性纳米二氧化钛 |
比表面积/m2/g | 90-200 | 160-250 |
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201410327907.9A CN104140692B (zh) | 2014-07-10 | 2014-07-10 | 一种疏水效果好的改性纳米二氧化钛及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201410327907.9A CN104140692B (zh) | 2014-07-10 | 2014-07-10 | 一种疏水效果好的改性纳米二氧化钛及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN104140692A CN104140692A (zh) | 2014-11-12 |
CN104140692B true CN104140692B (zh) | 2016-01-20 |
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CN201410327907.9A Active CN104140692B (zh) | 2014-07-10 | 2014-07-10 | 一种疏水效果好的改性纳米二氧化钛及其制备方法 |
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CN (1) | CN104140692B (zh) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104562636B (zh) * | 2015-01-14 | 2017-04-12 | 哈尔滨工业大学 | 表面接枝纳米二氧化钛的连续亚麻纤维束及其制备方法 |
CN104785349B (zh) * | 2015-04-29 | 2017-05-03 | 浙江冠旗纳米科技有限公司 | 纳米级固体粉末高效制备方法 |
CN105860593B (zh) * | 2016-04-08 | 2018-07-27 | 佛山中科欧泊科技有限公司 | 一种提高珠光颜料珠光效应的组合物、制备方法与应用 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102660154A (zh) * | 2012-04-28 | 2012-09-12 | 常州大学 | 一种纳米二氧化钛的表面修饰方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP2495291A1 (en) * | 2009-10-29 | 2012-09-05 | Sakai Chemical Industry Co., Ltd. | Method for producing organic solvent dispersion of inorganic oxide microparticles |
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Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102660154A (zh) * | 2012-04-28 | 2012-09-12 | 常州大学 | 一种纳米二氧化钛的表面修饰方法 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
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TR01 | Transfer of patent right |
Effective date of registration: 20201125 Address after: Room 2364, No.26 Guoding Branch Road, Yangpu District, Shanghai Patentee after: NALINV NANOTECHNOLOGY (SHANGHAI) Co.,Ltd. Address before: 247100 Anhui city of Chizhou Province Economic and Technological Development Zone Jinan Industrial Park Patentee before: CHIZHOU ENP TECHNOLOGY Co.,Ltd. |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A kind of modified nano titanium dioxide with good hydrophobic effect and preparation method thereof Effective date of registration: 20220831 Granted publication date: 20160120 Pledgee: Shanghai Rural Commercial Bank Co.,Ltd. Yangpu Sub branch Pledgor: NALINV NANOTECHNOLOGY (SHANGHAI) CO.,LTD. Registration number: Y2022310000221 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231102 Granted publication date: 20160120 Pledgee: Shanghai Rural Commercial Bank Co.,Ltd. Yangpu Sub branch Pledgor: NALINV NANOTECHNOLOGY (SHANGHAI) CO.,LTD. Registration number: Y2022310000221 |