CN104127351B - A kind of cosmetic composition and preparation method thereof - Google Patents

A kind of cosmetic composition and preparation method thereof Download PDF

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Publication number
CN104127351B
CN104127351B CN201410371185.7A CN201410371185A CN104127351B CN 104127351 B CN104127351 B CN 104127351B CN 201410371185 A CN201410371185 A CN 201410371185A CN 104127351 B CN104127351 B CN 104127351B
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extract
cosmetic composition
parts
mixing
fevervine
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CN104127351A (en
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不公告发明人
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Guangzhou Sitilon Cosmetic Co ltd
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Guangzhou Danqi Daily Chemical Co Ltd
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Abstract

The invention discloses a kind of cosmetic composition, by weight, including following components: plant extraction liquid 2~20 parts, NMF 3~11 parts, thickener 0.2~0.4 part, emulsifying agent 0.1~0.5 part, silica 0.1~2 parts, potassium hydroxide 0.03~0.07 part, pH adjusting agent 0.055~0.88 part, preservative 0.8~4 parts, water 60~90 parts.Wherein, described plant extraction liquid comprises Herba Houttuyniae extract and fevervine extract, and preservative comprises Pogostemon cablin extract.The mixed liquor of Herba Houttuyniae extract and fevervine extract is applied in cosmetic composition by the present invention, effectively improves skin function, prevention dermatitis.

Description

A kind of cosmetic composition and preparation method thereof
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of cosmetic combinations preventing dermatitis Thing and preparation method thereof.
Background technology
Cosmetics are to smear, spray or methods that other are similar, impose on any portion of human body surface Position (skin, nail, lip, the ripe film in oral cavity etc.), with reach cleaning, eliminate bad smell, Skin care, improve looks and modify the product of purpose.
The skin of people is strong fragile again, to chemicals, protein, bacterium, fungi, does Dry weathers etc. are likely to produce allergic reaction, are scytitis.The most effectively change Kind skin function, prevention dermatitis will be important topics.
Along with the development of cosmetics industry, natural plants series products is owing to using safety, making Welcome by gentle, the effect advantage such as substantially.Contained generally by corresponding processing The plant extracts of active ingredient, and add in cosmetics.
At present, the DeGrain of cosmetics prevention dermatitis on the market, and easily cause allergy Phenomenon.Therefore, select which kind of plant, and by its safety be applied in cosmetics reach prevention The effect of dermatitis, is problem demanding prompt solution.
Summary of the invention
Based on this, it is an object of the invention to provide a kind of cosmetic composition.
Concrete technical scheme is as follows:
A kind of cosmetic composition, by weight, including following components:
Wherein, above-mentioned NMF comprises Herba Houttuyniae extract and fevervine extract, preservative bag Containing Pogostemon cablin extract.
Wherein in an embodiment, described plant extraction liquid be weight part ratio be (1~10): The Herba Houttuyniae extract of (1~10) and the mixing of fevervine extract.
Wherein in an embodiment, described Herba Houttuyniae extract and the weight of fevervine extract Part is than being (5~8): (5~10).
Wherein in an embodiment, described NMF be weight part ratio be (0.1~1): (2~10) Trehalose, the mixing of glycerine.
Wherein in an embodiment, described thickener be weight part ratio be (0.1~0.2): The transparent xanthan gum of (0.1~0.2) and the mixing of carbomer.
Wherein in an embodiment, described emulsifying agent is cetearyl olive grease/sorb Alcohol olive grease.
Wherein in an embodiment, described pH adjusting agent is that mass parts compares for (0.005~0.08): The NaOH of (0.05~0.8) and the mixing of water.
Wherein in an embodiment, described preservative be weight part ratio be (0.3~1): (0.5~3) Sodium Benzoate/potassium sorbate and the mixing of Pogostemon cablin extract.
Wherein in an embodiment, the weight portion of described Pogostemon cablin extract is 1~2 part.
The Herba Houttuyniae extract of the present invention, fevervine extract and Pogostemon cablin extract can pass through Prepared by conventional alcohol extracting method, following extracting method: by dry plant (Pogostemon cablin, chicken Vow rattan, cordate houttuynia) join in the ethanol that mass ratio is 50%, extract under backflow and dipping 1~3h, extract 1~3 time;Subsequently, with filter cloth, extract is filtered, obtain filtrate.Mixing The filtrate of 1~3 time is concentrated to dryness to obtain plant (Pogostemon cablin, fevervine, cordate houttuynia) extract.
The preparation method of above-mentioned cosmetic composition, comprises the following steps:
(1) thickener is first scattered with the glycerine in NMF, add emulsification pot, then Add plant extraction liquid, remaining NMF, skinfeel conditioning agent, emulsifying agent, be heated to 75~85 DEG C, Insulated and stirred 10~20 minutes, stir speed (S.S.) is 20~40rpm, then homogeneous 2~5 minutes, Stir speed (S.S.) is 2000~4000rpm, cools, and obtains A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) the A phase of step (1) is cooled to 65~70 DEG C, adds the B in step (2) Phase, stirs, and continues cooling;
(4) when the temperature in step (3) near 40~45 DEG C, adding preservative, stirring is all Even, cosmetic composition.
Cordate houttuynia is gained the name because there being the fishy smell of one fish, calls heartleaf houttuynia, affine cudweed etc., is three white Grass section heartleaf houttuynia belongs to herbaceos perennial.It is distributed in east Asia and the southeast.China Zhejiang, Jiangsu, Anhui, Fujian, Henan, Guangdong, Guangxi, Hunan, Hubei, Sichuan, Guizhou, All there is product the provinces and regions such as Yunnan, Shaanxi, Gansu.Cordate houttuynia is the plant of medicine-food two-purpose, Zao Tang For just having in " Tang materia medica ", " leaf, like buckwheat, also can be overgrow fertilely.Stem puniceus, gives birth to more Wetland, at the moon of mountain valley.Shan Nan river Zuoren eats it raw well " record.The present invention uses and is dried entirely Grass.Herba Houttuyniae extract has good inhibiting effect to plasmin and trypsase, Skin function and the generation of prevention dermatitis can be improved.
Fevervine has another name called Chinese Fevervine Herb, for the herb of madder wort fevervine.Originate in Yunnan, expensive State, Sichuan, Guangxi, Guangdong, Fujian, Jiangxi, Hunan, Hubei, Anhui, Jiangsu, Zhejiang The ground such as river.Gather summer herb, dry.The present invention uses its dry herb.Fevervine extracts Stem cell is connected by liquid inhibitory action, and stem cell connects the generation of indication scytitis, i.e. Fevervine extract can effectively prevent the generation of dermatitis.
In the cosmetic composition of the present invention add silica be skinfeel conditioning agent can make people from Psychology is combined with physiology improves skin condition, increases moisture of skin;The effect of pH adjusting agent is Cosmetic composition of the present invention is made to have acid-base value preferable to skin effect.
Pogostemon cablin is the dry aerial parts that the Labiatae thorn stamen wide flower bud of grass platymiscium is fragrant, perennial grass This, be now distributed in the provinces and regions such as Guangdong, Hainan, Guangxi, Taiwan and Yunnan.Annual 6~adopt July Collection, dries.Wide flower bud perfume (or spice) herb is medicinal, and the present invention uses its dry herb.Pogostemon cablin extract Fungi is had wide spectrum and strong suppression, uses as preservative in the present invention.Preservative Act as prevention, press down bactericidal, protect a product from microorganism pollute, extend product shelf Phase;Prevent consumer from using the product polluted by microorganism to cause possible infection, it is ensured that peace Quan Xing.
The following component title that the application occurs is INCI (International Nomenclaure Cosmetic Ingredient, i.e. international cosmetic raw material name) title of defined: spermaceti is hard Aliphatic radical olive grease/sorbierite olive grease and Sodium Benzoate/potassium sorbate.
Advantages of the present invention is as follows:
Compared with prior art, the cosmetic composition of the present invention can improve skin function, prevention Dermatitis;Separately, the present invention uses natural botanical extraction liquid use as preservative, and reach Preferably effect.
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme is described further.
Embodiment 1
The preparation of plant extraction liquid
Dry cordate houttuynia is joined in the ethanol that mass ratio is 50%, under backflow and dipping Extract 1h, extract 3 times;Subsequently, with filter cloth, extract is filtered, obtain filtrate.Mixed The filtrate closing 3 times is concentrated to dryness to obtain Herba Houttuyniae extract.
Dry fevervine is joined in the ethanol that mass ratio is 50%, under backflow and dipping Extract 1.5h, extract 2 times;Subsequently, with filter cloth, extract is filtered, obtain filtrate.Mixed The filtrate closing 2 times is concentrated to dryness to obtain fevervine extract.
Dry plant Pogostemon cablin is joined in the ethanol that mass ratio is 50%, in backflow and leaching Extract 1.5h under stain, extract 2 times;Subsequently, with filter cloth, extract is filtered, obtain filtrate. The filtrate mixing 2 times is concentrated to dryness to obtain Pogostemon cablin extract.
Embodiment 2
The preparation of cosmetic composition
One, the formula of cosmetic composition
Experimental example 1~3 and the cosmetic combinations composition formula of comparative example 1~3 be shown in Table 1.
Table 1
Experimental example 4~6 and the cosmetic combinations composition formula of comparative example 4~6 be shown in Table 2.
Table 2
The cosmetic combinations composition formula of experimental example 7~12 is shown in Table 3.
Table 3
The cosmetic combinations composition formula of experimental example 13~18 is shown in Table 4.
Table 4
Two, the preparation of cosmetic composition
The cosmetic composition of above-mentioned experimental example 1-18 and comparative example 1-6 is by following preparation method Prepare:
(1) thickener is first scattered with the glycerine in NMF, add emulsification pot, then Add plant extraction liquid, remaining NMF, skinfeel conditioning agent, emulsifying agent, be heated to 80 DEG C, Insulated and stirred 15 minutes, stir speed (S.S.) is 30rpm, then homogeneous 3 minutes, stir speed (S.S.) For 3000rpm, cool, obtain A phase;
(2) pH adjusting agent mixed dissolution is complete, obtain B phase;
(3) the A phase of step (1) is cooled to 70 DEG C, adds the B phase in step (2), Stir, continue cooling;
(4) when the temperature in step (3) near 40 DEG C, add preservative, stir, Cosmetic composition.
Embodiment 3
Effect experimental
By experimental example in above-mentioned Tables 1 and 2 1~12 and the cosmetics group for preparing of comparative example 1~6 Compound, 100 personnel through 20~55 years old try out 30 days continuously respectively, comparative analysis evaluation The prevention dermatitis effects of cosmetic composition obtained in above-mentioned each experimental example.Wherein, described The improvement situation that effect is fash, itch, erythema and skin damage etc., the results are shown in Table 5.
Table 5
The cosmetic composition of above-mentioned experimental example 1-12 and comparative example 1-6 during on probation the most not Find excitant and allergic phenomena.
As known from Table 5: in experimental example, each cosmetic composition is fash, itch, erythema and skin Substantially than in control group, the improvement degree of each product is high for the improvement degree of damage etc.;And cordate houttuynia carries The weight portion taking liquid and fevervine extract is the biggest, improves degree the highest;Herba Houttuyniae extract When weight portion is 5~8, the weight portion of fevervine extract is 5~10, cosmetic composition Cost performance is the highest.
Embodiment 4
Anti-corrosive properties are tested
This experiment is with reference to preventing that Americanized cosmetic, toilet articles and essence association (CTFA) are recommended Rotten System Effectiveness evaluation method, with the anticorrosion single of classical 28 days by a definite date that CTFA recommends Challenge experiment.
1. challenge with microorganism: bacterium and mould
2. the mode inoculated and quantity
(1) mode inoculated: use combined inoculation.Because the microorganism of nature has mixed life to live together Feature, so combined inoculation meets the situation of actual pollution.
(2) quantity inoculated: each bacterial classification is inoculated in suitable culture medium, (thin in 37 DEG C Bacterium) and 28 DEG C of (mould) incubators in cultivate.Bacteria Culture 48 hours, mycotic culture 72 After hour, select typical bacterium colony in the fluid nutrient medium of sterilizing, make certain density bacterium Mix suspension with mould, be placed in refrigerator cold-storage standby.Bacterium: every gram of suspension bacteria containing amount is 1 ×106CFU/g or CFU/ml;Mould be every gram of suspension bacteria containing amount be 1 × 105CFU/g or CFU/ml。
3. Microbial Challenge experiment
Weigh each 100 grams of experimental example 13~18 cosmetic sample, add in the container of sterilizing, Add mixed cell and mould bacteria suspension, fully mix.Every gram of sample containing amount of bacteria be 1 × 106CFU/g or CFU/ml;It is 1 × 10 containing mould amount5CFU/g or CFU/ml.Then It is placed at 28 DEG C.Connecing the 0 of bacterium, 7,14,21,28 days sample analysis: accurately weigh 10 grams of samples, are added in the conical flask containing glass pellet and 90ml sterile saline, Fully shaking mixing, this suspension is 1:10 dilution, the most again with physiological saline by 1: 10 dilute successively.Cultivate 48 hours at 37 DEG C of bacterium;72 are cultivated little at 28 DEG C of mould Time, by bacteria containing amount in flat board tilt-pour process count samples.
4. evaluation method
Containing bacterium or mould at 10CFU/g~100CFU/g (CFU/ml) in 28 days samples, Show that microorganism is had stronger pressing down to kill effect by the protective system of this sample, tested by challenge, Dropping to below 1000CFU/g (CFU/m1) at the 7th day to be considered as passing through, other is considered as not Pass through.
5. experimental result
In 0,7,14,2l and sampling detection in 28 days of inoculation, experimental example 13~18 is made up Product composition sample anticorrosion test result is shown in Table 7.
Table 7
As known from Table 7: in experimental example, each cosmetic composition has certain antiseptic effect;Extensively The weight portion of wrinkled giant hyssop extract is the biggest, and antiseptic effect is the most obvious;Show that Pogostemon cablin extract has relatively Good antisepsis.When the weight portion of Pogostemon cablin extract is 1~2, Pogostemon cablin extract Antisepsis is preferable, and cost performance is the highest.
Embodiment described above only have expressed the several embodiments of the present invention, and its description more has Body is with detailed, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.Should refer to Go out, for the person of ordinary skill of the art, before without departing from present inventive concept Putting, it is also possible to make some deformation and improvement, these broadly fall into protection scope of the present invention. Therefore, the protection domain of patent of the present invention should be as the criterion with claims.

Claims (7)

1. a cosmetic composition, it is characterised in that by weight, including following components: plant extraction liquid 2~20 Part, NMF 3~11 parts, thickener 0.2~0.4 part, emulsifying agent 0.1~0.5 part, silica 0.1~2 parts, PH adjusting agent 0.055~0.88 part, preservative 0.8~4 parts, water 60~90 parts: wherein, described plant extract Liquid is Herba Houttuyniae extract and the mixing of fevervine extract, and preservative comprises Pogostemon cablin extract;Described Herba Houttuyniae extract and The weight part ratio of fevervine extract is (5~8): (5~10).
Cosmetic composition the most according to claim 1, it is characterised in that described NMF be weight part ratio be (0.1~ 1): the trehalose of (2~10), the mixing of glycerine.
Cosmetic composition the most according to claim 1, it is characterised in that described thickener be weight part ratio be (0.1~ 0.2): the transparent xanthan gum of (0.1~0.2) and the mixing of carbomer.
Cosmetic composition the most according to claim 1, it is characterised in that described emulsifying agent is cetearyl olive grease / sorbierite olive grease.
Cosmetic composition the most according to claim 1, it is characterised in that described pH adjusting agent is that mass parts ratio is (0.005~0.08): the NaOH of (0.05~0.8) and the mixing of water.
Cosmetic composition the most according to claim 1, it is characterised in that described preservative be weight part ratio be (0.3~ 1): the Sodium Benzoate/potassium sorbate of (0.5~3): the mixing of Pogostemon cablin extract.
Cosmetic composition the most according to claim 6, it is characterised in that the weight portion of described Pogostemon cablin extract is 1~2 part.
CN201410371185.7A 2014-07-30 2014-07-30 A kind of cosmetic composition and preparation method thereof Expired - Fee Related CN104127351B (en)

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CN105997726B (en) * 2016-07-09 2019-05-14 科丽思化妆品(上海)有限公司 A kind of antibiotic skin-care cream
CN111407679B (en) * 2019-03-29 2023-06-09 张帆 Moisturizing and repairing mask liquid

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KR20080088769A (en) * 2007-03-30 2008-10-06 조순묵 Cosmetic composition for sun protection, method for preparing cosmetic product of pouch pump dispenser type containing the same, and thereof product
CN102266419A (en) * 2010-09-21 2011-12-07 河南科技大学 Preparation method of houttuynia antibacterial cream
CN103565673A (en) * 2013-10-30 2014-02-12 广州品赫化妆品有限公司 Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion

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Publication number Priority date Publication date Assignee Title
KR20080088769A (en) * 2007-03-30 2008-10-06 조순묵 Cosmetic composition for sun protection, method for preparing cosmetic product of pouch pump dispenser type containing the same, and thereof product
CN102266419A (en) * 2010-09-21 2011-12-07 河南科技大学 Preparation method of houttuynia antibacterial cream
CN103565673A (en) * 2013-10-30 2014-02-12 广州品赫化妆品有限公司 Emollient lotion for moisturizing skin and controlling oil and preparation method of emollient lotion

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Inventor after: Guan Wei

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Effective date of registration: 20161111

Address after: Room 1607, Pearl River Tower, No. 15 Zhujiang West Road, Guangzhou, Guangdong, Tianhe District

Patentee after: GUANGZHOU SITILON COSMETIC Co.,Ltd.

Address before: 510370 Guangdong province Guangzhou City Creek Road in Panlong industrial zone of Liwan District dragon two friends of a 6 storey industrial building

Patentee before: CANTON DAMEKISS DAILY CHEMICAL FACTORY Ltd.

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Granted publication date: 20160831