CN104111195A - Method for analyzing breakage strength of essence capsule applied to cigarette filter - Google Patents

Method for analyzing breakage strength of essence capsule applied to cigarette filter Download PDF

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Publication number
CN104111195A
CN104111195A CN201410360908.3A CN201410360908A CN104111195A CN 104111195 A CN104111195 A CN 104111195A CN 201410360908 A CN201410360908 A CN 201410360908A CN 104111195 A CN104111195 A CN 104111195A
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China
Prior art keywords
essence capsule
essence
breakdown strength
capsule
push
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CN201410360908.3A
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CN104111195B (en
Inventor
徐岚
叶惠民
卢琳
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SHANGHAI BAIYULAN TOBACCO MATERIAL CO Ltd
Shanghai Tobacco Group Co Ltd
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SHANGHAI BAIYULAN TOBACCO MATERIAL CO Ltd
Shanghai Tobacco Group Co Ltd
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Priority to CN201410360908.3A priority Critical patent/CN104111195B/en
Publication of CN104111195A publication Critical patent/CN104111195A/en
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  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The invention relates to a method for analyzing breakage strength of an essence capsule applied to a cigarette filter. By virtue of the method, the breakage strength of the essence capsule is accurately measured by using a push-pull force tester; by virtue of a testing method, the blank of detection of characteristic indexes of a special filter stick which is a capsule filter stick is filled; only conventional detection is carried out on the conventional filter sticks; the characteristic detection aiming at various special filter sticks is not carried out. With the adoption of the detection scheme, the control over the quality of cigarette products can be facilitated.

Description

Essence capsule breakdown strength analytical approach for cigaratte filter
Technical field
The present invention relates to a kind of essence capsule material damage intensive analysis method for cigaratte filter, belong to testing of materials method field.
Background technology
Cigarette product is trend of the times to the low harm of low tar development, but cigarette is when reducing tar, and smoke is the partially light and fragrant deficiency of cigarette thereupon also, therefore certainly will have higher requirement to perfuming cigarette is reinforced.The method of perfuming has multiple, has and directly adds in pipe tobacco, also can be added in filter tip, when suction, bringing into play different effects, and perfuming has following advantage in filter tip: 1. in filter tip, temperature is lower, and essence is not volatile, composition can not change yet, and can guarantee the pure of cigarette fragrance; 2. in filter tip, add essence, from oral cavity close to, filtration is little, can make full use of essence.Wherein essence capsule filter tip is owing to needing consumer to pinch brokenly capsule competence exertion perfuming function, thereby the volatilization loss that not only can prevent from aspirating front fragrance, for apt to deteriorate and the high spices of susceptibility, after encapsulated, avoid the impact of extraneous factor simultaneously, improved storage-stable.So many brand cigarettes have been applied essence capsule filter tip both at home and abroad, and obtain the approval in market.
Breakdown strength is one of most important characteristic index of essence capsule material, and its characteristic index situation directly affects filter stick formation and consumer spending impression.As too small in breakdown strength, in filter stick formation process, easily cause capsule damaged, pollute former, affect filter stick formation efficiency.And the consumer group that cigarette is faced, has all kinds of personages of different sexes, all ages and classes level, and as excessive in breakdown strength, the consumer groups such as Ms, the old man more difficult capsule of pinching brokenly carry out cigarette smoking, directly affect consumer's consumption impression.Essence capsule filter tip at home brand cigarette Applicative time is not long, tobacco business does not have capsule breakdown strength standard method of analysis at present, and the present invention is by the essence capsule material damage intensive analysis method that detection method is studied, analytical equipment parts are introduced and technological transformation foundation is comparatively scientific and reasonable.
Summary of the invention
The object of the present invention is to provide essence capsule breakdown strength analytical approach for a kind of cigaratte filter, the qualified essence capsule filter tip that meets consumer spending demand for producing provides assurance.
The present invention is achieved by the following technical solutions:
An essence capsule breakdown strength analytical approach for cigaratte filter, for adopting push-pull effort tester to carry out the accurate measurement of essence capsule breakdown strength; Described push-pull effort tester comprises pushing and drawing force testing machine and the computing machine being connected with described pushing and drawing force testing machine; Described pushing and drawing force testing machine comprises that one for placing mounting table and the detection probe of essence capsule; Described detection probe comprises a detection pressure head and a built-in digital displacement detection system; On described computing machine, testing software is housed; Specifically comprise the following steps:
(1) essence capsule to be measured and push-pull effort tester are placed in to constant-temperature constant-humidity environment balance;
(2) switch on power, open the preheating of push-pull effort tester;
(3) getting an essence capsule to be measured is placed on described mounting table;
(4) open the testing software on computing machine, control detection probe and be displaced downwardly to and detect pressure head and essence capsule to be measured touches, continue to press down until essence capsule is racked, now downforce reaches peak value; Afterwards, on the interface of testing software, automatically obtain the breakdown strength value of described essence capsule to be measured;
Essence capsule of the present invention refers to the whole capsule particle that is built-in with essence, at present in flavouring cigarette method, toward the essence microcapsule adding in filter tip.
Being shaped as of essence capsule of the present invention is spherical, is of a size of diameter 2-5mm.
Preferably, be provided for placing the groove of essence capsule on described mounting table, the diameter of groove is 0.5-1mm, and makes the axle center of described breakdown strength detection probe and being centered close on same vertical curve of described groove.Essence capsule to be measured is positioned in described groove and can avoids its slip on mounting table in test process.
Preferably, in the test process of step (4), the speed that described breakdown strength detection probe moves down is 0.3-0.8mm/s.
The detection of the detection probe of described testing software one side control instrument to the breakdown strength of capsule, data analysis and the statistical treatment that described detection probe can be recorded on the other hand.
Preferably, the qualified detectability of the testing software on described computing machine is set as 0~30 N, to adapt to the detection of capsule material; Test result, in above scope, can be judged as certified products, exceeds above scope and is judged as unacceptable product.
Preferably, in step (1), it is that the constant-temperature constant-humidity environment that 22 ℃ ± 2 ℃, humidity are 60%RH ± 5%RH is placed that essence capsule material to be measured and described push-pull effort tester are all placed in to temperature.
Preferably, in step (2), after switching on power, open push-pull effort tester preheating at least 30 minutes.
Technique effect of the present invention and advantage are:
Method of testing of the present invention has been filled up the blank that extraordinary filter stick (capsule filter stick) characteristic index detects, and filter stick is only had to conventional sense in the past, the Characteristics Detection of needleless to all kinds of extraordinary filter sticks, and testing result is accurate, is conducive to control the product quality of checking on.
Accompanying drawing explanation
The pushing and drawing force testing machine of Fig. 1 push-pull effort tester
Reference numeral:
1, mounting table;
2, detection probe;
3, groove.
Embodiment
By specific instantiation, technical scheme of the present invention is described below.Should be understood that one or more method steps that the present invention mentions do not repel between the step that also has additive method step or clearly mention at these before and after described combination step can also insert additive method step; Should also be understood that these embodiment are only not used in and limit the scope of the invention for the present invention is described.And, except as otherwise noted, the numbering of various method steps is only for differentiating the convenient tool of various method steps, but not for limiting the ordering of various method steps or limiting the enforceable scope of the present invention, the change of its relativeness or adjustment, without essence change technology contents in the situation that, when being also considered as the enforceable category of the present invention.
Embodiment
An essence capsule material damage intensive analysis method, for adopting push-pull effort tester to carry out the accurate measurement of essence capsule breakdown strength; Described push-pull effort tester comprises pushing and drawing force testing machine and the computing machine being connected with described pushing and drawing force testing machine; Described pushing and drawing force testing machine comprises that one for placing mounting table and the detection probe of essence capsule; Described detection probe comprises a detection pressure head and a built-in digital displacement detection system; On described computing machine, testing software is housed;
1, checkout equipment specifications parameter:
Mounting table is provided with for placing the groove of essence capsule, and the diameter of groove is 0.5-1mm;
Breakdown strength detection probe rate travel: 0.3-0.8mm/s;
The qualified detectability of the testing software on computing machine is set as 0~30 N;
2, flavouring essence for tobacco capsule material breakdown strength is measured concrete grammar step
(1) balance of testing sample and detecting instrument
A. every batch of essence capsule sample of material to be checked must be through the 24 hours constant temperature and humidity balances in testing laboratory.(22 ℃ ± 2 ℃ of temperature; Humidity: 60.0%RH ± 5%RH)
B. detecting instrument is deposited, operating environment must be controlled by constant temperature and humidity.(22 ℃ ± 2 ℃ of temperature; Humidity: 60.0%RH ± 5%RH) if not in this testing environment, should give and stop detecting.(except drying box and part measurement instrument)
(2) start preheating and measurement
A. each detecting instrument is due to after long-time shutdown, while restarting machine, and electronic component needs just can obtain accurate measurement result after preheating, and General Requirements connects AC power at least 30 minutes, or through the power attenuation of long duration.
B. installation testing software (TextExpert testing software), avoids due to software issue the usability of lowering apparatus.
C. first check that pushing and drawing force testing machine, computing machine guarantee normal connection; Then first connect pushing and drawing force testing machine power supply and open, opening again subsequently computing machine; At least preheating 30 minutes after start, waits instrument to reach after stable and could start to detect;
D. double-click the testing software on computing machine, start to measure, control detection probe and be displaced downwardly to and detect pressure head and essence capsule to be measured touches, continue to press down until essence capsule is racked, now downforce reaches peak value; Afterwards, on the interface of software, automatically obtain the intensity level that crushes of described essence capsule to be measured;
(3) close instrument power source, cleaning work platform.
(4) maintaining
A. ban use of metal, sharp-pointed article, or barbarous operation detection instrument.
B. after using detecting instrument at every turn, need to use special-purpose clean article to detecting instrument maintain, cleaning.
C. need weekly specialty maintenance.
The present embodiment adopts above test parameter and testing procedure, and 4 batches of essence capsules from the different places of production (20 every batch, spherical, diameter 2-5mm) are carried out to breakdown strength test, and result is as shown in table 1:
Table 1 essence capsule breakdown strength test data
By detecting above data, can see, different places of production essence capsule breakdown strength detects data significant difference, as too small in breakdown strength, cause in process of production, essence capsule breaks in a large number because of production contact friction, cause production environment to pollute and defective filter stick product, affect filter stick formation efficiency.And breakdown strength is excessive, the capsule of pinching brokenly as more difficult in consumer groups such as Ms, old men carries out cigarette smoking, directly affects consumer's consumption impression.
In addition different places of production essence capsule breakdown strength SD numerical value is also obviously different, illustrates that different places of production essence capsule breakdown strength stability has obvious difference, and this is also to analyze the important evidence of understanding essence capsule quality of materials stability.
Because essence capsule filter stick is current domestic and international emerging extraordinary filter stick product, for the importance of essence capsule breakdown strength index, thereby research is set up essence capsule breakdown strength detection method, the raising of the promotion capsule filter stick quality of production and batch production efficiency.

Claims (7)

1. an essence capsule breakdown strength analytical approach for cigaratte filter, for adopting push-pull effort tester to carry out the accurate measurement of essence capsule breakdown strength; Described push-pull effort tester comprises pushing and drawing force testing machine and the computing machine being connected with described pushing and drawing force testing machine; Described pushing and drawing force testing machine comprises that one for placing mounting table and the detection probe of essence capsule; Described detection probe comprises a detection pressure head and a built-in digital displacement detection system; On described computing machine, testing software is housed; Specifically comprise the following steps:
(1) essence capsule to be measured and push-pull effort tester are placed in to constant-temperature constant-humidity environment balance;
(2) switch on power, open the preheating of push-pull effort tester;
(3) getting an essence capsule to be measured is placed on described mounting table;
(4) open the testing software on computing machine, control detection probe and be displaced downwardly to and detect pressure head and essence capsule to be measured touches, continue to press down until essence capsule is racked, now downforce reaches peak value; Afterwards, on the interface of testing software, automatically obtain the breakdown strength value of described essence capsule to be measured.
2. essence capsule breakdown strength analytical approach for a kind of cigaratte filter as claimed in claim 1, is characterized in that, being shaped as of described essence capsule is spherical, and diameter is 2-5mm.
3. essence capsule breakdown strength analytical approach for a kind of cigaratte filter as claimed in claim 1, it is characterized in that, described mounting table is provided with for placing the groove of essence capsule, and the diameter of groove is 0.5-1mm, and the center of described groove and the axle center of described detection probe are on same vertical curve.
4. essence capsule breakdown strength analytical approach for a kind of cigaratte filter as claimed in claim 1, is characterized in that, in step (4), the speed that described detection probe moves down is 0.3-0.8mm/s.
5. essence capsule breakdown strength analytical approach for a kind of cigaratte filter as claimed in claim 1, is characterized in that, the qualified detectability of the testing software on described computing machine is set as 0~30 N.
6. essence capsule breakdown strength analytical approach for a kind of cigaratte filter as claimed in claim 1, it is characterized in that, in step (1), it is that the constant-temperature constant-humidity environment that 22 ℃ ± 2 ℃, humidity are 60%RH ± 5%RH is placed that essence capsule to be measured and described push-pull effort tester are all placed in to temperature.
7. essence capsule breakdown strength analytical approach for a kind of cigaratte filter as claimed in claim 1, is characterized in that, in step (2), after switching on power, opens push-pull effort tester preheating at least 30 minutes.
CN201410360908.3A 2014-07-25 2014-07-25 Cigarette filter essence capsule breakdown strength analyzes method Active CN104111195B (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107621406A (en) * 2016-07-15 2018-01-23 贵州中烟工业有限责任公司 A kind of cigarette capsule particle intensity and the detection method and equipment of deformation quantity
CN108225985A (en) * 2016-12-21 2018-06-29 贵州中烟工业有限责任公司 A kind of cigarette capsule particle strength detecting method
CN114414177A (en) * 2021-12-27 2022-04-29 江苏辰星药业股份有限公司 Detection device and system for centrifugal plant hollow capsule production

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US20110232658A1 (en) * 2003-06-23 2011-09-29 R.J. Reynolds Tobacco Company Filtered cigarette incorporating a breakable capsule
US20120037173A1 (en) * 2003-09-30 2012-02-16 R. J. Reynolds Tobacco Company Filtered cigarette incorporating an adsorbent material
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JP2008116349A (en) * 2006-11-06 2008-05-22 Shimadzu Corp Microcompression testing machine
CN101788426A (en) * 2010-03-04 2010-07-28 河北科技大学 Device for testing axial compressibility of fiber material
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CN203164056U (en) * 2013-03-28 2013-08-28 昆明理工大学 Experimental system for testing nut hull-breaking mechanical property

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107621406A (en) * 2016-07-15 2018-01-23 贵州中烟工业有限责任公司 A kind of cigarette capsule particle intensity and the detection method and equipment of deformation quantity
CN108225985A (en) * 2016-12-21 2018-06-29 贵州中烟工业有限责任公司 A kind of cigarette capsule particle strength detecting method
CN114414177A (en) * 2021-12-27 2022-04-29 江苏辰星药业股份有限公司 Detection device and system for centrifugal plant hollow capsule production
CN114414177B (en) * 2021-12-27 2022-12-16 江苏辰星药业股份有限公司 Detection device and system for centrifugal plant hollow capsule production

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