CN104109430A - Emulsion type waterproof corrosion-resistant acrylate exterior wall coating - Google Patents
Emulsion type waterproof corrosion-resistant acrylate exterior wall coating Download PDFInfo
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Abstract
The invention discloses an emulsion type waterproof corrosion-resistant acrylate exterior wall coating, comprising the following raw materials by weight: 50 to 60 parts of a base material, 5 to 15 parts of an alcohol-ester 12 film-forming additive and 30 to 40 parts of an accessory material. The base material comprises the following raw materials by weight: 5 to 10 parts of a drying oil alkyd resin, 50 to 60 parts of acrylic emulsion, 30 to 40 parts of silica sol, 2 to 6 parts of a coupling agent and 1 to 4 parts of sodium butylnaphthalenesulfonate. The accessory material comprises the following raw materials by weight: 20 to 25 parts of borax, 15 to 20 parts of light calcium carbonate, 15 to 20 parts of titanium dioxide, 18 to 23 parts of wollastonite powder, 5 to 10 parts of nanometer zinc oxide, 0.5 to 1 part of polyvinylpyrrolidone, 0.5 to 1.5 parts of an antifoaming agent, 0.8 to 1.3 parts of carboxymethylcellulose sodium, 1 to 2 parts of 1,2-benzoisothiazole-3-one, 1 to 1.3 parts of ammonia water, 10 to 15 parts of water and 2 to 5 parts of methyl nylon acid ester. The emulsion type waterproof corrosion-resistant acrylate exterior wall coating has excellent waterproof performance, good corrosion resistance and long service life.
Description
Technical field
The present invention relates to acrylate paint for external wall technical field, relate in particular to the corrosion-resistant acrylate paint for external wall of a kind of emulsion-type waterproof.
Background technology
The Cultivar development of China's protective system is very rapid, at present, developed the protective system of many excellent propertys, as many kinds such as high-temperature anticorrosion paint, anti-static and anti-corrosive paint, snappiness protective system, nonpoisonous anti-corrosive paints, along with the continually developing and applying of High Performance Corrosion Protective Coatings, protective system research is had to important scientific value and social value.Although protective system development rapidly, the erosion resistance of protective system and water resistance are to be further improved in addition.
Summary of the invention
The present invention proposes the corrosion-resistant acrylate paint for external wall of a kind of emulsion-type waterproof, water resistance is excellent, corrosion resistance and good, long service life.
The corrosion-resistant acrylate paint for external wall of a kind of emulsion-type waterproof that the present invention proposes, its raw material comprises 50-60 part base-material, 5-15 part alcohol ester 12 film coalescence aid and 30-40 part auxiliary material by weight;
The raw materials by weight of described base-material comprises: drying oil alkyd resin 5-10 part, ACRYLIC EMULSION 50-60 part, silicon sol 30-40 part, coupling agent 2-6 part, sodium butylnaphthalenesulfonate 1-4 part, adopt following technique preparation: ACRYLIC EMULSION and silicon sol are placed in to reactor, at 75-80 ℃, stir, then add coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin to stir and obtain base-material;
Auxiliary material comprises by weight: borax 20-25 part, light calcium carbonate 15-20 part, titanium dioxide 15-20 part, wollastonite powder 18-23 part, nano zine oxide 5-10 part, polyvinylpyrrolidone 0.5-1 part, defoamer 0.5-1.5 part, Xylo-Mucine 0.8-1.3 part, 1,2-benzisothiazole-3-ketone 1-2 part, ammoniacal liquor 1-1.3 part, water 10-15 part, nylon acid methyl esters 2-5 part;
In preparation process, first base-material is put into agitator, under the rotating speed of 400-500r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 10-15min, under 700-750r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1300-1400r/min disperses, inspection by sampling fineness is less than after 50 microns, under 800-850r/min rotating speed, dropping into nylon acid methyl esters disperses after 8-13min, under the rotating speed of 550-600r/min, add defoamer to disperse 8-13min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
Preferably, the weight ratio of base-material, alcohol ester 12 film coalescence aid and auxiliary material is 55-60:10-15:30-35.
Preferably, the weight ratio of base-material, alcohol ester 12 film coalescence aid and auxiliary material is 55:15:30.
Preferably, its auxiliary material comprises by weight: borax 22-24 part, light calcium carbonate 16-18 part, titanium dioxide 18-20 part, wollastonite powder 20-22 part, nano zine oxide 8-10 part, polyvinylpyrrolidone 0.6-0.8 part, defoamer 1-1.4 part, Xylo-Mucine 1-1.2 part, 1,2-benzisothiazole-3-ketone 1.5-2 part, ammoniacal liquor 1-1.2 part, water 12-14 part, nylon acid methyl esters 2-4 part.
Preferably, the weight ratio of Xylo-Mucine and 1,2-benzisothiazole-3-ketone is 1.2:1.6.
Preferably, in preparation process, first base-material is put into agitator, under the rotating speed of 450r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 12min, under 720r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1350r/min disperses, inspection by sampling fineness is less than after 50 microns, under 820r/min rotating speed, dropping into nylon acid methyl esters disperses after 12min, under the rotating speed of 580r/min, add defoamer to disperse 12min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
In the present invention, the deficiency that the compound action of ACRYLIC EMULSION and silicon sol can overcome separately produces synergistic effect, add appropriate coupling agent and emulsifying agent can improve both interface performances, make the crosslinked compound phase mutual effect of ACRYLIC EMULSION and silicon sol to form hydrophobic coating closely, can make composite emulsion stability more excellent, product is in isolation rainwater, can significantly strengthen the anti-cracking performance of exterior wall base material, make base material avoid the erosion of acid rain, Acid Rain corrosive nature is good, with borax, light calcium carbonate, titanium dioxide, wollastonite powder and nano zine oxide acting in conjunction, the compactness extent of coating strengthens, to light to cover efficiency high, coupling agent has the effect of bridge formation, inorganics and organism closely can be linked together, make product particle more be tending towards complete, and add appropriate 1, 2-benzisothiazole-3-ketone sanitas, waterproof and the Corrosion Protection of product further strengthen, and paint film can keep primary colors not fade for a long time, also stronger to base material sticking power, select alcohol ester 12 film coalescence aid film-formation results good, paint film is closely knit, even dry under disadvantageous temperature and humidity, also can reach good paint film property, this product waterproof property is excellent, and corrosion resistance is strong, long service life.
Embodiment
Embodiment 1
In the present embodiment, the corrosion-resistant acrylate paint for external wall of a kind of emulsion-type waterproof, its raw material comprises 50 parts of base-materials, 15 parts of alcohol ester 12 film coalescence aid and 30 parts of auxiliary materials by weight;
The raw materials by weight of described base-material comprises: 10 parts of drying oil alkyd resins, 50 parts of ACRYLIC EMULSION, 40 parts of silicon sol, 2 parts of coupling agents, 4 parts of sodium butylnaphthalenesulfonates, adopt following technique preparation: ACRYLIC EMULSION and silicon sol are placed in to reactor, at 75 ℃, stir, then add coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin to stir and obtain base-material;
Auxiliary material comprises by weight: 25 parts of boraxs, 15 parts of light calcium carbonates, 20 parts of titanium dioxides, 18 parts of wollastonite powder, 10 parts of nano zine oxides, 0.5 part of polyvinylpyrrolidone, 1.5 parts of defoamers, 0.8 part of Xylo-Mucine, 2 parts of 1,2-benzisothiazole-3-ketones, 1 part of ammoniacal liquor, 15 parts, water, 2 parts of nylon acid methyl esters;
In preparation process, first base-material is put into agitator, under the rotating speed of 500r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 10min, under 750r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1300r/min disperses, inspection by sampling fineness is less than after 50 microns, under 850r/min rotating speed, dropping into nylon acid methyl esters disperses after 8min, under the rotating speed of 600r/min, add defoamer to disperse 8-13min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
Embodiment 2
In the present embodiment, the corrosion-resistant acrylate paint for external wall of a kind of emulsion-type waterproof, its raw material comprises 55 parts of base-materials, 10 parts of alcohol ester 12 film coalescence aid and 35 parts of auxiliary materials by weight;
The raw materials by weight of described base-material comprises: 9 parts of drying oil alkyd resins, 53 parts of ACRYLIC EMULSION, 38 parts of silicon sol, 4 parts of coupling agents, 3 parts of sodium butylnaphthalenesulfonates, adopt following technique preparation: ACRYLIC EMULSION and silicon sol are placed in to reactor, at 77 ℃, stir, then add coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin to stir and obtain base-material;
Auxiliary material comprises by weight: 24 parts of boraxs, 17 parts of light calcium carbonates, 18 parts of titanium dioxides, 20 parts of wollastonite powder, 8 parts of nano zine oxides, 0.6 part of polyvinylpyrrolidone, 1.3 parts of defoamers, 1.2 parts of Xylo-Mucines, 1.7 parts of 1,2-benzisothiazole-3-ketones, 1.1 parts of ammoniacal liquor, 14 parts, water, 3 parts of nylon acid methyl esters;
In preparation process, first base-material is put into agitator, under the rotating speed of 450r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 12min, under 720r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1350r/min disperses, inspection by sampling fineness is less than after 50 microns, under 820r/min rotating speed, dropping into nylon acid methyl esters disperses after 12min, under the rotating speed of 580r/min, add defoamer to disperse 12min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
Embodiment 3
In the present embodiment, the corrosion-resistant acrylate paint for external wall of a kind of emulsion-type waterproof, its raw material comprises 60 parts of base-materials, 5 parts of alcohol ester 12 film coalescence aid and 40 parts of auxiliary materials by weight;
The raw materials by weight of described base-material comprises: 5 parts of drying oil alkyd resins, 60 parts of ACRYLIC EMULSION, 30 parts of silicon sol, 6 parts of coupling agents, 1 part of sodium butylnaphthalenesulfonate, adopt following technique preparation: ACRYLIC EMULSION and silicon sol are placed in to reactor, at 80 ℃, stir, then add coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin to stir and obtain base-material;
Auxiliary material comprises by weight: 22 parts of boraxs, 18 parts of light calcium carbonates, 19 parts of titanium dioxides, 20 parts of wollastonite powder, 9 parts of nano zine oxides, 0.8 part of polyvinylpyrrolidone, 1 part of defoamer, 1.2 parts of Xylo-Mucines, 1.6 parts of 1,2-benzisothiazole-3-ketones, 1.1 parts of ammoniacal liquor, 14 parts, water, 3 parts of nylon acid methyl esters;
In preparation process, first base-material is put into agitator, under the rotating speed of 400r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 15min, under 700r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1400r/min disperses, inspection by sampling fineness is less than after 50 microns, under 800r/min rotating speed, dropping into nylon acid methyl esters disperses after 13min, under the rotating speed of 550r/min, add defoamer to disperse 13min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
Embodiment 4
In the present embodiment, the corrosion-resistant acrylate paint for external wall of a kind of emulsion-type waterproof, its raw material comprises 55 parts of base-materials, 15 parts of alcohol ester 12 film coalescence aid and 30 parts of auxiliary materials by weight;
The raw materials by weight of described base-material comprises: 7 parts of drying oil alkyd resins, 57 parts of ACRYLIC EMULSION, 33 parts of silicon sol, 5 parts of coupling agents, 2 parts of sodium butylnaphthalenesulfonates, adopt following technique preparation: ACRYLIC EMULSION and silicon sol are placed in to reactor, at 78 ℃, stir, then add coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin to stir and obtain base-material;
Auxiliary material comprises by weight: 24 parts of boraxs, 16 parts of light calcium carbonates, 18 parts of titanium dioxides, 22 parts of wollastonite powder, 8 parts of nano zine oxides, 0.6 part of polyvinylpyrrolidone, 1.4 parts of defoamers, 1 part of Xylo-Mucine, 1.5 parts of 1,2-benzisothiazole-3-ketones, 1.2 parts of ammoniacal liquor, 12 parts, water, 4 parts of nylon acid methyl esters;
In preparation process, first base-material is put into agitator, under the rotating speed of 470r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 12min, under 740r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1380r/min disperses, inspection by sampling fineness is less than after 50 microns, under 840r/min rotating speed, dropping into nylon acid methyl esters disperses after 12min, under the rotating speed of 590r/min, add defoamer to disperse 12min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
The corrosion-resistant acrylate paint for external wall of emulsion-type waterproof described in embodiment 1-4 is carried out to performance test, and test result is as follows:
| Performance test | Testing standard | Test result |
| Water tolerance | 168h is without extremely | 168h is without extremely |
| Erosion resistance (20% aqueous sulfuric acid soaks) | 10 days without abnormal | 10 days without abnormal |
| Resistance to coating temperature sex change can (circulate for 10 times) | Without abnormal | Without abnormal |
The above; it is only preferably embodiment of the present invention; but protection scope of the present invention is not limited to this; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; according to technical scheme of the present invention and inventive concept thereof, be equal to replacement or changed, within all should being encompassed in protection scope of the present invention.
Claims (6)
1. the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof, is characterized in that, its raw material comprises 50-60 part base-material, 5-15 part alcohol ester 12 film coalescence aid and 30-40 part auxiliary material by weight;
The raw materials by weight of described base-material comprises: drying oil alkyd resin 5-10 part, ACRYLIC EMULSION 50-60 part, silicon sol 30-40 part, coupling agent 2-6 part, sodium butylnaphthalenesulfonate 1-4 part, adopt following technique preparation: ACRYLIC EMULSION and silicon sol are placed in to reactor, at 75-80 ℃, stir, then add coupling agent, sodium butylnaphthalenesulfonate and drying oil alkyd resin to stir and obtain base-material;
Auxiliary material comprises by weight: borax 20-25 part, light calcium carbonate 15-20 part, titanium dioxide 15-20 part, wollastonite powder 18-23 part, nano zine oxide 5-10 part, polyvinylpyrrolidone 0.5-1 part, defoamer 0.5-1.5 part, Xylo-Mucine 0.8-1.3 part, 1,2-benzisothiazole-3-ketone 1-2 part, ammoniacal liquor 1-1.3 part, water 10-15 part, nylon acid methyl esters 2-5 part;
In preparation process, first base-material is put into agitator, under the rotating speed of 400-500r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 10-15min, under 700-750r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1300-1400r/min disperses, inspection by sampling fineness is less than after 50 microns, under 800-850r/min rotating speed, dropping into nylon acid methyl esters disperses after 8-13min, under the rotating speed of 550-600r/min, add defoamer to disperse 8-13min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
2. according to right, will remove the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof described in 1, it is characterized in that, the weight ratio of base-material, alcohol ester 12 film coalescence aid and auxiliary material is 55-60:10-15:30-35.
3. according to right, will remove the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof described in 1 or 2, it is characterized in that, the weight ratio of base-material, alcohol ester 12 film coalescence aid and auxiliary material is 55:15:30.
4. according to right, will remove the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof described in 1-3 any one, it is characterized in that, its auxiliary material comprises by weight: borax 22-24 part, light calcium carbonate 16-18 part, titanium dioxide 18-20 part, wollastonite powder 20-22 part, nano zine oxide 8-10 part, polyvinylpyrrolidone 0.6-0.8 part, defoamer 1-1.4 part, Xylo-Mucine 1-1.2 part, 1,2-benzisothiazole-3-ketone 1.5-2 part, ammoniacal liquor 1-1.2 part, water 12-14 part, nylon acid methyl esters 2-4 part.
5. according to right, will remove the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof described in 1-4 any one, it is characterized in that, the weight ratio of Xylo-Mucine and 1,2-benzisothiazole-3-ketone is 1.2:1.6.
6. according to right, to remove the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof described in 1-5 any one, it is characterized in that, in preparation process, first base-material is put into agitator, under the rotating speed of 450r/min, drop into successively alcohol ester 12 film coalescence aid, polyvinylpyrrolidone, Xylo-Mucine, 1, 2-benzisothiazole-3-ketone, ammoniacal liquor and water-dispersion 12min, under 720r/min rotating speed, drop into borax, light calcium carbonate, titanium dioxide, after wollastonite powder and nano zine oxide, rotating speed being increased to 1350r/min disperses, inspection by sampling fineness is less than after 50 microns, under 820r/min rotating speed, dropping into nylon acid methyl esters disperses after 12min, under the rotating speed of 580r/min, add defoamer to disperse 12min to obtain the corrosion-resistant acrylate paint for external wall of emulsion-type waterproof.
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| CN201410310476.5A CN104109430B (en) | 2014-07-01 | 2014-07-01 | A kind of emulsion-type waterproof anti-corrosion acrylate paint for external wall |
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| CN105238223A (en) * | 2015-11-17 | 2016-01-13 | 刘广利 | High-strength environmental-friendly water-based paint and preparation method thereof |
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| CN114656860A (en) * | 2022-01-24 | 2022-06-24 | 广东中城海创新材料有限公司 | Barium sulfate exterior wall coating and preparation method thereof |
| CN116478601A (en) * | 2022-01-24 | 2023-07-25 | 广东中城海创新材料有限公司 | Barium sulfate exterior wall coating and preparation method thereof |
| CN116200083A (en) * | 2023-02-13 | 2023-06-02 | 一汽解放汽车有限公司 | Water-based acrylic coating and application thereof |
| CN116200083B (en) * | 2023-02-13 | 2024-05-07 | 一汽解放汽车有限公司 | Water-based acrylic coating and application thereof |
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| CN104109430B (en) | 2016-08-24 |
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