CN104059777B - Cananga oil restructuring essential oil of a kind of stability and safety and preparation method thereof - Google Patents

Cananga oil restructuring essential oil of a kind of stability and safety and preparation method thereof Download PDF

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Publication number
CN104059777B
CN104059777B CN201310087043.3A CN201310087043A CN104059777B CN 104059777 B CN104059777 B CN 104059777B CN 201310087043 A CN201310087043 A CN 201310087043A CN 104059777 B CN104059777 B CN 104059777B
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agitator
restructuring
essential oil
intermediates
phenylethyl
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CN104059777A (en
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曹蔚
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Xiamen Amber Perfumery Co Ltd
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Xiamen Hupo Daily Chemical Technology Co Ltd
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Abstract

The present invention discloses a kind of cananga oil restructuring essential oil, it is characterized in that its feed composition and weight percentage content comprise: phenylethyl alcohol 1.5 ~ 2.5, peruscabin 25 ~ 28, methyl benzoate 10 ~ 12, meraneine 2 ~ 4, willow acid benzyl ester 5 ~ 6, methyl phenylacetate 1.0 ~ 1.5, jasmal 15 ~ 16, phantol 14 ~ 16, phenylcarbinol 2 ~ 3, terpinyl acetate 1.0 ~ 1.2, Bornyl acetate 1.0 ~ 1.2, vernol 1.0 ~ 1.2, cinnamic alcohol 3 ~ 4, Geraniol 2.5 ~ 3.5, Phenylethyl ethanoate 1.0 ~ 1.2, phanteine 0.5 ~ 0.8, p-cresyl methyl ether 10 ~ 11, isoeugenol 1.2 ~ 1.5, Terpineol 350 1.0 ~ 1.5.Product can be obtained through stirring, leaving standstill, filter.

Description

Cananga oil restructuring essential oil of a kind of stability and safety and preparation method thereof
Technical field
The present invention relates to a kind of essential oil, cananga oil restructuring essential oil specifically relating to a kind of stability and safety and preparation method thereof.
Background technology
Natural cananga oil mainly Yilan fresh flower obtains cananga oil by wet distillation, and oil yield is 0.1% ~ 1%, is weak yellow liquid at normal temperatures, can be used for the raw material allocated floral type food flavour or make cosmetics.Cananga oil can loosen neural system as essential oil, makes people feel vigorously pleased; Indignation, anxiety, panic mood can be alleviated; There is effect of promoting the sexual maturity, can improvement creeping chill and sexual dysfunction etc.
But natural cananga oil source, fragrance instability, and wherein some become branch can produce the dangerous impacts such as irritated to skin, now commercially all adopt half concocting method (natural jointly use with synthetic perfume) to allocate and substitute essential oil, inherently or can not solve the problem.
Summary of the invention
The object of this invention is to provide a kind of cananga oil restructuring essential oil.This restructuring essential oil all selects the synthetic perfume of safety and stability, adopt the meat flavor formulating technology of natural emulation, ensure that naturalness and the intensity of fragrance, in use solve again the problems such as the stable and skin safe of fragrance simultaneously, can directly substitute natural cananga oil and the alternative essential oil of half allotment.The perfume material that essential oil of the present invention adopts all thinks GRAS or do not limit regulation in daily chemical products according to RIFM, IFRA, EOA, CEorCOE.Do not opening under packaging prerequisite, this shelf life of products can reach 18 months.
The present invention realizes above-mentioned purpose by following proposal:
1, cananga oil restructuring essential oil composition of raw materials (by 100 parts of calculating) is:
Phenylethyl alcohol 1.5 ~ 2.5 parts
Peruscabin 25 ~ 28 parts
Methyl benzoate 10 ~ 12 parts
Meraneine 2.0 ~ 4.0 parts
Willow acid benzyl ester 5.0 ~ 6.0 parts
Methyl phenylacetate 1.0 ~ 1.5 parts
Jasmal 15 ~ 16 parts
Terpinyl acetate 1.0 ~ 1.2 parts
Bornyl acetate 1.0 ~ 1.2 parts
Phenylethyl ethanoate 1.0 ~ 1.2 parts
Vernol 1.0 ~ 1.2 parts
Phantol 14 ~ 16 parts
Cinnamic alcohol 3.0 ~ 4.0 parts
Geraniol 2.5 ~ 3.5 parts
Phenylcarbinol 2.0 ~ 3.0 parts
P-cresyl methyl ether 10 ~ 11 parts
Isoeugenol 1.2 ~ 1.5 parts
Phanteine 0.5 ~ 0.8 part
Terpineol 350 1.0 ~ 1.5 parts
2, take each component according to above-mentioned formula, then proceed as follows:
(1). phenylethyl alcohol, peruscabin, methyl benzoate, meraneine, willow acid benzyl ester, methyl phenylacetate, jasmal, phantol, phenylcarbinol are weighed successively and add agitator kettle, turn on agitator, stir about 20 minutes, closes agitator, obtains intermediates A.
(2). terpinyl acetate, Bornyl acetate, vernol, cinnamic alcohol, Geraniol are weighed successively and join in intermediates A, stir about dissolves to solid for 30 minutes completely, closes agitator, obtains intermediates B.
(3). Phenylethyl ethanoate, phanteine, p-cresyl methyl ether, isoeugenol, Terpineol 350 are weighed successively and adds intermediates B, turn on agitator stir about was closed after 60 minutes, leave standstill purifying 24 hours, with worry net filtrations more than 400 orders, select stainless steel on request, aluminium matter or Brown Glass Brown glass bottles and jars only packaging, be finished product.
Embodiment
To produce 100Kg cananga oil restructuring essential oil:
Example 1
(1). phenylethyl alcohol 1.5Kg, peruscabin 25Kg, methyl benzoate 10Kg, meraneine 2.0Kg willow acid benzyl ester 5.0Kg, methyl phenylacetate 1.5Kg, jasmal 15Kg, phantol 14Kg, phenylcarbinol 2.0Kg weighing are added agitator kettle, turn on agitator, stir about 20 minutes, close agitator, obtain intermediates A.
(2). terpinyl acetate 1.0Kg, Bornyl acetate 1.0Kg, vernol 1.0Kg, cinnamic alcohol 3.0Kg, Geraniol 3.5Kg are weighed successively and join in intermediates A, stir about dissolves to solid for 30 minutes completely, close agitator, obtain intermediates B.
(3). Phenylethyl ethanoate 1.2Kg, phanteine 0.8Kg, p-cresyl methyl ether 10Kg, isoeugenol 1.5Kg, Terpineol 350 1.0Kg are weighed successively and add intermediates B, turn on agitator stir about was closed after 60 minutes, leave standstill purifying 24 hours, with worry net filtration, select stainless steel on request, aluminium matter or Brown Glass Brown glass bottles and jars only packaging, be finished product.
Example 2
(1). phenylethyl alcohol 1.5Kg, peruscabin 25Kg, methyl benzoate 12Kg, meraneine 2.0Kg, willow acid benzyl ester 5.0Kg, methyl phenylacetate 1.0Kg, jasmal 15Kg, phantol 14Kg, phenylcarbinol 2.0Kg weighing are added agitator kettle, turn on agitator, stir about 20 minutes, close agitator, obtain intermediates A.
(2). terpinyl acetate 1.0Kg, Bornyl acetate 1.0Kg, vernol 1.0Kg, cinnamic alcohol 3.0Kg, Geraniol 2.5Kg are weighed successively and join in intermediates A, stir about dissolves to solid for 30 minutes completely, close agitator, obtain intermediates B.
(3). Phenylethyl ethanoate 1.0Kg, phanteine 0.5Kg, p-cresyl methyl ether 10Kg, isoeugenol 1.5Kg, Terpineol 350 1.0Kg are weighed successively and add intermediates B, turn on agitator stir about was closed after 60 minutes, leave standstill purifying 24 hours, with worry net filtration, select stainless steel on request, aluminium matter or Brown Glass Brown glass bottles and jars only packaging, be finished product.

Claims (3)

1. a cananga oil restructuring essential oil for stability and safety, is characterized in that raw material is grouped into by the one-tenth of following weight percents:
Phenylethyl alcohol 1.5 ~ 2.5%
Peruscabin 25 ~ 28%
Methyl benzoate 10 ~ 12%
Meraneine 2.0 ~ 4.0%
Willow acid benzyl ester 5.0 ~ 6.0%
Methyl phenylacetate 1.0 ~ 1.5%
Jasmal 15 ~ 16%
Terpinyl acetate 1.0 ~ 1.2%
Bornyl acetate 1.0 ~ 1.2%
Phenylethyl ethanoate 1.0 ~ 1.2%
Vernol 1.0 ~ 1.2%
Phantol 14 ~ 16%
Cinnamic alcohol 3.0 ~ 4.0%
Geraniol 2.5 ~ 3.5%
Phenylcarbinol 2.0 ~ 3.0%
P-cresyl methyl ether 10 ~ 11%
Isoeugenol 1.2 ~ 1.5%
Phanteine 0.5 ~ 0.8%
Terpineol 350 1.0 ~ 1.5%.
2. restructuring essential oil according to claim 1, is characterized in that the preparation method adopted is:
(1). be the phenylethyl alcohol of 1.5 ~ 2.5 by weight percentage, the peruscabin of 25 ~ 28, methyl benzoate, the meraneine of 2.0 ~ 4.0, willow acid benzyl ester, the methyl phenylacetate of 1.0 ~ 1.5, jasmal, the phantol of 14 ~ 16, the phenylcarbinol of 2.0 ~ 3.0 of 15 ~ 16 of 5.0 ~ 6.0 of 10 ~ 12 weigh successively and add agitator kettle, turn on agitator, stir about 20 minutes, close agitator, obtain intermediates A;
(2). by weight percentage be the terpinyl acetate of 1.0 ~ 1.2,1.0 ~ 1.2 Bornyl acetate, 1.0 ~ 1.2 vernols, 3.0 ~ 4.0 cinnamic alcohols, 2.5 ~ 3.5 Geraniol weigh successively and join in intermediates A, stir about dissolves to solid for 30 minutes completely, close agitator, obtain intermediates B;
(3). be the Phenylethyl ethanoate of 1.0 ~ 1.2 by weight percentage, the phanteine of 0.5 ~ 0.8, p-cresyl methyl ether, the isoeugenol of 1.2 ~ 1.5, the Terpineol 350 of 1.0 ~ 1.5 of 10 ~ 11 weigh successively and add intermediates B, turn on agitator stir about was closed after 60 minutes, leave standstill purifying 24 hours, with strainer filtering, select stainless steel on request, aluminium matter or Brown Glass Brown glass bottles and jars only packaging, be finished product.
3. restructuring essential oil according to claim 2, is characterized in that filter screen is more than 400 orders.
CN201310087043.3A 2013-03-19 2013-03-19 Cananga oil restructuring essential oil of a kind of stability and safety and preparation method thereof Active CN104059777B (en)

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Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0292992A (en) * 1988-09-29 1990-04-03 Takemi Tamura Lighter oil
JP2000355696A (en) * 1999-04-12 2000-12-26 Kao Corp Perfume composition
EP1964542A1 (en) * 2007-03-02 2008-09-03 Takasago International Corporation Sensitive skin perfumes
CN101760306A (en) * 2008-11-24 2010-06-30 王晓明 Ylang ylang oil rose essence

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Address after: 361100 Fujian Province, Xiamen city industrial concentration area with the Park No. 308

Applicant after: XIAMEN AMBER DAILY CHEMICAL TECHNOLOGY CO.,LTD.

Address before: 361100 Fujian Province, Xiamen city industrial concentration area with the Park No. 308

Applicant before: Xiamen Amber Perfume Co.,Ltd.

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Free format text: CORRECT: APPLICANT; FROM: XIAMEN AMBER PERFUME CO., LTD. TO: XIAMEN AMBER COSMETIC TECHNOLOGY CO., LTD.

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Address after: No. 308, Tong'an Park, Tong'an Industrial Concentration Zone, Xiamen City, Fujian Province, 361100

Patentee after: Xiamen Amber Flavor Co.,Ltd.

Address before: No. 308, Tong'an Park, Tong'an Industrial Concentration Zone, Xiamen City, Fujian Province, 361100

Patentee before: XIAMEN AMBER DAILY CHEMICAL TECHNOLOGY CO.,LTD.