CN104046419A - Lubricating oil for magnesuim-aluminium alloy wire-drawing - Google Patents
Lubricating oil for magnesuim-aluminium alloy wire-drawing Download PDFInfo
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- CN104046419A CN104046419A CN201410170075.4A CN201410170075A CN104046419A CN 104046419 A CN104046419 A CN 104046419A CN 201410170075 A CN201410170075 A CN 201410170075A CN 104046419 A CN104046419 A CN 104046419A
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Abstract
The invention relates to drawing oil, specifically to lubricating oil for magnesuim-aluminium alloy wire-drawing. The drawing oil is prepared from the following raw materials, by weight, 50-60 parts of machine oil, 80-100 parts of trimethylolpropane trioleate, 10-12 parts of fatty alcohol polyoxyethylene ether, 2-3 parts of petroleum sodium sulfonate, 1-3 parts of zine stearate, 1-2 parts of butylated hydroxytoluene, 1-2 parts of tricresyl phosphate, 1-2 parts of high basic value calcium sulfurized alkyl phenate and 2-3 parts of an auxiliary agent. According to the drawing oil, machine oil and synthetic ester oil are mixed as base oil. The drawing oil has excellent heat stability and still can maintain excellent lubricating property during high-speed drawing process. With the combination of additives such as petroleum sodium sulfonate, zinc stearate, high basic value calcium sulfurized alkyl phenate and the like, the drawing oil provided by the invention has a tough oil film, and friction coefficient between a wire and a die can be reduced effectively. Thus, phenomena such as breaking, scratching and the like are reduced effectively, and the wire-drawing effect is improved.
Description
Technical field
The present invention relates to a kind of wire drawing oil, be specifically related to a kind of magnalium lubricating oil for wire drawing and preparation technology thereof.
Background technology
Wire drawing oil is the important industrial auxiliary agent of a class, in wire drawing, drawing process process, does efficient lubricant oil use, has lubricated, cleaning, the effect such as cooling, antirust, assists metal flow, avoids mould to drag colored bracing wire, improves yield rate, reduces production loss.Existing wire drawing oil is mainly divided into oiliness wire drawing oil and water-based wire drawing oil, this two classes wire drawing oil cuts both ways when reality is used, as oiliness wire drawing oil exists heat dispersion poor, cleaning chip removal difficulty, the problems such as waste liquid difficult degradation, and although the wire drawing oil heat dispersion of water-based is good compared with oiliness wire drawing oil, but lubricant effect is not fully up to expectations, the wire drawing that is difficult to meet various metals line is drawn and is dialled processing requirement, therefore for improve enterprise machining level, reduce production costs, need to improve wire drawing oil formula and technique, make it reach good use properties.
Summary of the invention
The object of the invention is to, a kind of magnalium lubricating oil for wire drawing is provided, to improve wire-drawing effect, to achieve these goals, the technical solution used in the present invention is as follows:
A kind of magnalium lubricating oil for wire drawing, it is characterized in that, material of the present invention is made by the raw material of following weight part: machinery oil 50-60, tricarboxymethyl propane oleate 80-100, fatty alcohol-polyoxyethylene ether 10-12, petroleum sodium sulfonate 2-3, Zinic stearas 1-3, butylated hydroxytoluene 1-2, tritolyl phosphate 1-2, SULFURIZED CALCIUM ALKYL PHENATE WITH HIGH BASE NUMBER 1-2, auxiliary agent 2-3; Described auxiliary agent is made by the raw material of following weight part: Graphene 1-2, silane coupling agent KH560 0.1-0.2, Unimac 5680 15-18, xanthan gum 10-12, sorbester p17 4-5, deionized water are appropriate; Preparation method is: first by Graphene and silane coupling agent mixed grinding 10-15min, the powder obtaining mixes with Unimac 5680, sorbester p17, under the rotating speed of 1000-1500 rev/min, stir 20-30min, make emulsion standby, then xanthan gum is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion are mixed, continuation is stirred 15-20min with 1000-1500 rev/min of rotating speed, stirs and finishes rear standing 2-4h, obtains.
Described a kind of magnalium lubricating oil for wire drawing, its preparation technology is: first machinery oil is mixed with tricarboxymethyl propane oleate, be heated to 50-60 ℃, add fatty alcohol-polyoxyethylene ether, abundant mix and blend 20-30min, then add other remaining component, continue to stir 50-60min, stir and finish by naturally cooling to room temperature, get product.
The wire drawing oil advantage that the present invention prepares is: because magnesium-aluminium alloy material hardness is larger, in wire drawing, drawing process, accelerated the loss of mould, and wire-drawing effect is also not fully up to expectations, product is easy-formation not, in order to improve wire-drawing effect, to improve drawing mould on the one hand, need on the other hand wire drawing oil to carry out compositional refinements, improve its oilness, help metal to slide and moulding; Wire drawing oil of the present invention is usingd machinery oil and synthesizing ester oil and is mixed as base oil, this class base oil has good thermostability, make it in drawing process at a high speed, still can keep good lubricity, again in conjunction with additives such as petroleum sodium sulfonate, Zinic stearas, SULFURIZED CALCIUM ALKYL PHENATE WITH HIGH BASE NUMBER, make wire drawing oil of the present invention there is tough oil film, can effectively reduce the frictional coefficient between wire rod and mould, thus effectively reduce break, the phenomenon such as cut, improve wire-drawing effect.
Embodiment
Embodiment
The present embodiment wire drawing oil by following weight part (kilogram) raw material make: machinery oil 60, tricarboxymethyl propane oleate 100, fatty alcohol-polyoxyethylene ether 12, petroleum sodium sulfonate 2, Zinic stearas 2, butylated hydroxytoluene 1, tritolyl phosphate 2, SULFURIZED CALCIUM ALKYL PHENATE WITH HIGH BASE NUMBER 2, auxiliary agent 3; Described auxiliary agent is made by the raw material of following weight part: Graphene 1, silane coupling agent KH560 0.2, Unimac 5680 15, xanthan gum 10, sorbester p17 4, deionized water are appropriate; Preparation method is: first by Graphene and silane coupling agent mixed grinding 15min, the powder obtaining mixes with Unimac 5680, sorbester p17, under the rotating speed of 1500 revs/min, stir 20min, make emulsion standby, then xanthan gum is mixed with appropriate deionized water, be mixed with mass concentration and be 60% xanthan gum solution, finally the aqueous solution, emulsion are mixed, continuation is stirred 15min with 1500 revs/min of rotating speeds, stirs and finishes rear standing 2h, obtains.
Described a kind of magnalium lubricating oil for wire drawing, its preparation technology is: first machinery oil is mixed with tricarboxymethyl propane oleate, be heated to 50-60 ℃, add fatty alcohol-polyoxyethylene ether, abundant mix and blend 30min, then add other remaining component, continue to stir 60min, stir and finish by naturally cooling to room temperature, get product.
Wire drawing oil of the present invention can stablize at ambient temperature deposit at least one year, during without precipitation, demixing phenomenon; Concrete each performance index are as follows:
| Project | Index |
| Kinematic viscosity (100 ℃) | 15-18mm 2/s |
| Condensation point | ≤-4℃ |
| Flash-point (opening) | ≥240℃ |
| 5% emulsion pH value | 6.8 |
| 5% emulsion corrosion (55 ± 2) ℃, soaks aluminium flake 24h entirely | Corrosion-free |
| Rust-preventing characteristic (35 ± 2) ℃, aluminium bits 2h | Qualified |
| 5% emulsion stability (15-35 ℃) 4h | Without layering, without precipitation, without soap, oil, separate out |
| P BValue/N | 608 |
Claims (2)
1. a magnalium lubricating oil for wire drawing, it is characterized in that, this wire drawing oil is made by the raw material of following weight part: machinery oil 50-60, tricarboxymethyl propane oleate 80-100, fatty alcohol-polyoxyethylene ether 10-12, petroleum sodium sulfonate 2-3, Zinic stearas 1-3, butylated hydroxytoluene 1-2, tritolyl phosphate 1-2, SULFURIZED CALCIUM ALKYL PHENATE WITH HIGH BASE NUMBER 1-2, auxiliary agent 2-3; Described auxiliary agent is made by the raw material of following weight part: Graphene 1-2, silane coupling agent KH560 0.1-0.2, Unimac 5680 15-18, xanthan gum 10-12, sorbester p17 4-5, deionized water are appropriate; Preparation method is: first by Graphene and silane coupling agent mixed grinding 10-15min, the powder obtaining mixes with Unimac 5680, sorbester p17, under the rotating speed of 1000-1500 rev/min, stir 20-30min, make emulsion standby, then xanthan gum is mixed with appropriate deionized water, be mixed with the xanthan gum solution that mass concentration is 60-70%, finally the aqueous solution, emulsion are mixed, continuation is stirred 15-20min with 1000-1500 rev/min of rotating speed, stirs and finishes rear standing 2-4h, obtains.
2. a kind of magnalium lubricating oil for wire drawing as claimed in claim 1, its preparation technology is: first machinery oil is mixed with tricarboxymethyl propane oleate, be heated to 50-60 ℃, add fatty alcohol-polyoxyethylene ether, abundant mix and blend 20-30min, then add other remaining component, continue to stir 50-60min, stir and finish by naturally cooling to room temperature, get product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410170075.4A CN104046419A (en) | 2014-04-25 | 2014-04-25 | Lubricating oil for magnesuim-aluminium alloy wire-drawing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410170075.4A CN104046419A (en) | 2014-04-25 | 2014-04-25 | Lubricating oil for magnesuim-aluminium alloy wire-drawing |
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| Publication Number | Publication Date |
|---|---|
| CN104046419A true CN104046419A (en) | 2014-09-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201410170075.4A Pending CN104046419A (en) | 2014-04-25 | 2014-04-25 | Lubricating oil for magnesuim-aluminium alloy wire-drawing |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105414225A (en) * | 2015-11-04 | 2016-03-23 | 无锡翱天钢丝制品有限公司 | Novel cold heading wire coating process |
| CN107603707A (en) * | 2017-09-27 | 2018-01-19 | 深圳市奥科宝特种油剂有限公司 | A kind of water-soluble cold-heading oil and preparation method thereof |
| CN111778093A (en) * | 2020-08-05 | 2020-10-16 | 陕西高精尖新材料科技有限责任公司 | Titanium alloy wire high-temperature drawing oil-based lubricant and preparation method thereof |
| CN112048357A (en) * | 2020-09-22 | 2020-12-08 | 广州南星精细化工有限公司 | Preparation method of high-resistance alloy wire drawing lubricating oil |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2139321C1 (en) * | 1998-02-09 | 1999-10-10 | Институт проблем сверхпластичности металлов РАН | Process lubricant concentrate "mekor 1" for metal cord wire drawing |
| CN103589491A (en) * | 2013-11-29 | 2014-02-19 | 广州机械科学研究院有限公司 | Lubricating material for cold rolling and its preparation method and use |
| CN103710123A (en) * | 2013-12-05 | 2014-04-09 | 马鞍山市恒毅机械制造有限公司 | Environmentally friendly cutting fluid containing graphene and preparation method therefor |
-
2014
- 2014-04-25 CN CN201410170075.4A patent/CN104046419A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2139321C1 (en) * | 1998-02-09 | 1999-10-10 | Институт проблем сверхпластичности металлов РАН | Process lubricant concentrate "mekor 1" for metal cord wire drawing |
| CN103589491A (en) * | 2013-11-29 | 2014-02-19 | 广州机械科学研究院有限公司 | Lubricating material for cold rolling and its preparation method and use |
| CN103710123A (en) * | 2013-12-05 | 2014-04-09 | 马鞍山市恒毅机械制造有限公司 | Environmentally friendly cutting fluid containing graphene and preparation method therefor |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105414225A (en) * | 2015-11-04 | 2016-03-23 | 无锡翱天钢丝制品有限公司 | Novel cold heading wire coating process |
| CN107603707A (en) * | 2017-09-27 | 2018-01-19 | 深圳市奥科宝特种油剂有限公司 | A kind of water-soluble cold-heading oil and preparation method thereof |
| CN107603707B (en) * | 2017-09-27 | 2020-09-18 | 深圳市奥科宝特种油剂有限公司 | Water-soluble cold heading oil and preparation method thereof |
| CN111778093A (en) * | 2020-08-05 | 2020-10-16 | 陕西高精尖新材料科技有限责任公司 | Titanium alloy wire high-temperature drawing oil-based lubricant and preparation method thereof |
| CN112048357A (en) * | 2020-09-22 | 2020-12-08 | 广州南星精细化工有限公司 | Preparation method of high-resistance alloy wire drawing lubricating oil |
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Application publication date: 20140917 |