CN104031403B - A kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof - Google Patents
A kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof Download PDFInfo
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- CN104031403B CN104031403B CN201410269204.5A CN201410269204A CN104031403B CN 104031403 B CN104031403 B CN 104031403B CN 201410269204 A CN201410269204 A CN 201410269204A CN 104031403 B CN104031403 B CN 104031403B
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Abstract
The present invention relates to a kind of preparation method and application thereof of tender Folium Evodiae trichotomae natural dyestuff, this preparation method, comprising: the tender Folium Evodiae trichotomae collected utilizes clear water to clean, dries by (1), utilizes mechanical disintegration to obtain tender Folium Evodiae trichotomae powder; (2) tender Folium Evodiae trichotomae powder is joined in the aqueous ethanolic solution of pH value 8 ~ 10, leave standstill after utilizing wooden stick to stir; (3) carry out refluxing extraction, extracting solution is warmed up to 75 ~ 95 DEG C, carry out filtering also; (4) method of underpressure distillation is utilized to obtain the tender Folium Evodiae trichotomae natural dyestuff concentrated.The leaching process of this tender Folium Evodiae trichotomae natural dyestuff can not shine into environmental pollution; Fabric touch after dyeing is soft, wears safety, does not have reaction that is carcinogenic, teratogenesis, no longer needs to worry that on fabric, dyestuff is to the injury of child after infant's dress; And tender Folium Evodiae trichotomae abundant raw material, extract simple, steady quality.
Description
Technical field
The field that the present invention relates to natural dyestuff and apply, particularly a kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff and application thereof.
Background technology
Now society be no matter science and technology or social economy all in develop rapidly, the standard of living of people is constantly improving, and the quality of life is also in the change that matter occurs, and the health that hope is not only eaten by increasing people, that wears also wants healthy.But what wear in life is nearly all the dyestuff of chemosynthesis, this dyestuff not only by the process of producing to the Nature, damage the health of people, after textile dyeing, the color and luster of fabric seems unnatural, it is also very uncomfortable that people wear, particularly infant, they like what being taken just toward putting in the mouth, very dangerous.
Summary of the invention
The object of the invention is to overcome above deficiency, a kind of preparation method and application thereof of tender Folium Evodiae trichotomae natural dyestuff are provided, the present invention can effectively utilize natural resources, not pollute in preparation process, very economical and practical, and the fabric color nature applied, healthy practical, there is anti-microbial property.
Technical scheme provided by the invention is: a kind of preparation method of tender Folium Evodiae trichotomae natural dyestuff, comprises the following steps:
(1) the tender Folium Evodiae trichotomae collected is utilized clear water to clean, dries, utilize machinery to be pulverized by the tender Folium Evodiae trichotomae dried and obtain tender Folium Evodiae trichotomae powder;
(2) tender Folium Evodiae trichotomae powder is joined concentration of volume percent and be 40 ~ 80% and in the aqueous ethanolic solution of pH value 8 ~ 10, the mass ratio of tender Folium Evodiae trichotomae powder and aqueous ethanolic solution is 1:10 ~ 50, after utilizing wooden stick to stir, leave standstill 3 ~ 5 minutes;
(3) carry out refluxing extraction, extracting solution is warmed up to 75 ~ 95 DEG C, insulation 30 ~ 90min, carries out filtering also;
(4) liquid volume after utilizing the method for underpressure distillation to make filtration is concentrated to 1/5 ~ 1/3 of original volume, obtains the tender Folium Evodiae trichotomae natural dyestuff concentrated.
Further improvement is, the invention provides a kind ofly to utilize aforementioned tender Folium Evodiae trichotomae natural dyestuff to the method for fabric substantive dyeing, comprises step:
(1) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:10 ~ 60, and dyestuff pH value is adjusted to 7 ~ 8;
(2) treating that dye thing is put in water and soak into by real silk or wool material, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 ~ 60 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing in 1:20 ~ 60, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min;
(3), after having dyeed, washing, dries.
Further improve and be, the invention provides a kind of method utilizing the application of aforementioned tender Folium Evodiae trichotomae natural dyestuff fabric to be carried out to antimicrobial treatment, comprise the following steps:
(1) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:20 ~ 40, and dyestuff pH value is adjusted to 7.5 ~ 8;
(2) treating that dye thing is put in water and soak into by real silk or wool material, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 ~ 60 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing in 1:20 ~ 60, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min;
(3), after having dyeed, washing, dries.
The invention has the advantages that: the present invention extracts natural dyestuff from tender Folium Evodiae trichotomae, and dye to real silk, wool fabric, colour fastness is high, and dye uptake is high, and natural in color is characteristic, and natural environmental protection; Real silk simultaneously after tender maple leaf dyeing, wool fabric have excellent germ resistance and reach 90.95%, 85.72% respectively to streptococcus aureus, colibacillary bacteriostasis rate.The leaching process of whole tender Folium Evodiae trichotomae dyestuff can not shine into environmental pollution; Fabric touch after dyeing is soft, wears safety, does not have reaction that is carcinogenic, teratogenesis, no longer needs to worry that on fabric, dyestuff is to the injury of child after infant's dress; And tender Folium Evodiae trichotomae abundant raw material, extract simple, steady quality.
embodiment:
Embodiment 1:
Tender Folium Evodiae trichotomae is cleaned, dried, mechanical disintegration, take 1 kilogram, powder, with the aqueous ethanolic solution that 50 kilograms of pH value are 10 40%, after stirring, at 95 DEG C of temperature, soak into 30min, after filtration, remove solid matter, liquid after filtration carries out underpressure distillation and is concentrated into 5 liters, is tender Folium Evodiae trichotomae natural dyestuff.
Embodiment 2:
Tender Folium Evodiae trichotomae is cleaned, dried, mechanical disintegration, take 1 kilogram, powder, with the aqueous ethanolic solution that 10 kilograms of pH value are 8 80%, after stirring, at 75 DEG C of temperature, soak into 90min, after filtration, remove solid matter, liquid after filtration carries out underpressure distillation and is concentrated into 10 liters, is tender Folium Evodiae trichotomae natural dyestuff.
Embodiment 3:
Tender Folium Evodiae trichotomae is cleaned, dried, mechanical disintegration, take 1 kilogram, powder, with the aqueous ethanolic solution that 30 kilograms of pH value are 9 80%, after stirring, at 85 DEG C of temperature, soak into 45min, after filtration, remove solid matter, liquid after filtration carries out underpressure distillation and is concentrated into 5 liters, is tender Folium Evodiae trichotomae natural dyestuff.
Embodiment 4:
(1) treat that dye thing is put in water and soaked into by real silk material, take out directly extract stand-by;
(2) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:60, and dyestuff pH value is adjusted to 7, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing at 1:60, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min, after having dyeed, washing, dries.
(3) above-mentioned dyeing sample is oyster.
Embodiment 5:
(1) treat that dye thing is put in water and soaked into by real silk material, take out directly extract stand-by;
(2) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:40, and dyestuff pH value is adjusted to 7.5, control the temperature of tender Folium Evodiae trichotomae dyestuff at 55 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing at 1:40, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min, after having dyeed, washing, dries.
(3) above-mentioned dyeing sample is yellow-green colour.
Embodiment 6:
(1) treat that dye thing is put in water and soaked into by real silk material, take out directly extract stand-by;
(2) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:10, and dyestuff pH value is adjusted to 8, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing at 1:20, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min, after having dyeed, washing, dries.
(3) above-mentioned dyeing sample is dark yellow-green.
Embodiment 7:
(1) treat that dye thing is put in water and soaked into by real silk material, take out directly extract stand-by;
(2) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:40, and dyestuff pH value is adjusted to 8, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing at 1:20, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min, after having dyeed, washing, dries.
(3) with reference to E2149-01 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record DYED FABRICS and 92.10%, 86.35% is respectively to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 8:
(1) treat that dye thing is put in water and soaked into by real silk material, take out directly extract stand-by;
(2) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:30, and dyestuff pH value is adjusted to 7.8, control the temperature of tender Folium Evodiae trichotomae dyestuff at 55 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing at 1:40, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min, after having dyeed, washing, dries.
(3) with reference to E2149-01 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record DYED FABRICS and 93.05%, 87.65% is respectively to streptococcus aureus, colibacillary bacteriostasis rate.
Embodiment 9:
(1) treat that dye thing is put in water and soaked into by real silk material, take out directly extract stand-by;
(2) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:20, and dyestuff pH value is adjusted to 7.5, control the temperature of tender Folium Evodiae trichotomae dyestuff at 60 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing at 1:60, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min, after having dyeed, washing, dries.
(3) with reference to E2149-01 " fixing the standard test methods of antibacterial antiplaque agent determination of activity under dynamic Contact condition ", record DYED FABRICS and 91.25%, 86.85% is respectively to streptococcus aureus, colibacillary bacteriostasis rate.
Claims (2)
1. tender Folium Evodiae trichotomae natural dyestuff is to a method for fabric substantive dyeing, comprises the following steps:
(1) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:10 ~ 60, and dyestuff pH value is adjusted to 7 ~ 8, the tender Folium Evodiae trichotomae collected utilizes clear water to clean by the preparation method of described concentrated tender Folium Evodiae trichotomae natural dyestuff, dry, utilize machinery to be pulverized by the tender Folium Evodiae trichotomae dried and obtain tender Folium Evodiae trichotomae powder, tender Folium Evodiae trichotomae powder is joined concentration of volume percent and be 40 ~ 80% and in the aqueous ethanolic solution of pH value 8 ~ 10, the mass ratio of tender Folium Evodiae trichotomae powder and aqueous ethanolic solution is 1:10 ~ 50, 3 ~ 5 minutes are left standstill after utilizing wooden stick to stir, carry out refluxing extraction, extracting solution is warmed up to 75 ~ 95 DEG C, insulation 30 ~ 90min, filter, liquid volume after utilizing the method for underpressure distillation to make filtration is concentrated to 1/5 ~ 1/3 of original volume,
(2) treating that dye thing is put in water and soak into by real silk or wool material, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 ~ 60 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing in 1:20 ~ 60, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min;
(3), after having dyeed, washing, dries.
2. utilize tender Folium Evodiae trichotomae natural dyestuff application described in claim 1 fabric to be carried out to the method for antimicrobial treatment, comprise the following steps:
(1) quality of concentrated tender Folium Evodiae trichotomae natural dyestuff and water is hybridly prepared into tender Folium Evodiae trichotomae dyestuff with the ratio of 1:20 ~ 40, and dyestuff pH value is adjusted to 7.5 ~ 8, , the tender Folium Evodiae trichotomae collected utilizes clear water to clean by the preparation method of described concentrated tender Folium Evodiae trichotomae natural dyestuff, dry, utilize machinery to be pulverized by the tender Folium Evodiae trichotomae dried and obtain tender Folium Evodiae trichotomae powder, tender Folium Evodiae trichotomae powder is joined concentration of volume percent and be 40 ~ 80% and in the aqueous ethanolic solution of pH value 8 ~ 10, the mass ratio of tender Folium Evodiae trichotomae powder and aqueous ethanolic solution is 1:10 ~ 50, 3 ~ 5 minutes are left standstill after utilizing wooden stick to stir, carry out refluxing extraction, extracting solution is warmed up to 75 ~ 95 DEG C, insulation 30 ~ 90min, filter, liquid volume after utilizing the method for underpressure distillation to make filtration is concentrated to 1/5 ~ 1/3 of original volume,
(2) treating that dye thing is put in water and soak into by real silk or wool material, control the temperature of tender Folium Evodiae trichotomae dyestuff at 50 ~ 60 DEG C, take out and put it in the tender Folium Evodiae trichotomae dyestuff mixed up after directly extracting, make the fixing fabric structure of the volume and tender Folium Evodiae trichotomae dyestuff waiting to contaminate thing in 1:20 ~ 60, whole waiting contaminates thing needs at tender Folium Evodiae trichotomae dyestuff placement 90min;
(3), after having dyeed, washing, dries.
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| CN106235326A (en) * | 2016-07-21 | 2016-12-21 | 天峨县全盛蜂业科技有限公司 | The extracting method of a kind of Folium Alangii juice and application |
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| CN102454119A (en) * | 2010-10-18 | 2012-05-16 | 南通曙光染织有限公司 | Extraction of tea-leaf natural dye and dyeing method for silk broadcloth |
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| CN102454119A (en) * | 2010-10-18 | 2012-05-16 | 南通曙光染织有限公司 | Extraction of tea-leaf natural dye and dyeing method for silk broadcloth |
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