CN104030613B - A kind of porcelain tendre and preparation method thereof - Google Patents
A kind of porcelain tendre and preparation method thereof Download PDFInfo
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- CN104030613B CN104030613B CN201410238703.8A CN201410238703A CN104030613B CN 104030613 B CN104030613 B CN 104030613B CN 201410238703 A CN201410238703 A CN 201410238703A CN 104030613 B CN104030613 B CN 104030613B
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- 229910052573 porcelain Inorganic materials 0.000 title claims abstract description 95
- 238000002360 preparation method Methods 0.000 title claims abstract description 43
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 60
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims abstract description 31
- 235000013312 flour Nutrition 0.000 claims abstract description 31
- 239000004575 stone Substances 0.000 claims abstract description 31
- 239000006004 Quartz sand Substances 0.000 claims abstract description 30
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 30
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims abstract description 29
- 239000004743 Polypropylene Substances 0.000 claims abstract description 29
- HCWCAKKEBCNQJP-UHFFFAOYSA-N magnesium orthosilicate Chemical compound [Mg+2].[Mg+2].[O-][Si]([O-])([O-])[O-] HCWCAKKEBCNQJP-UHFFFAOYSA-N 0.000 claims abstract description 29
- 229910052919 magnesium silicate Inorganic materials 0.000 claims abstract description 29
- 235000019792 magnesium silicate Nutrition 0.000 claims abstract description 29
- 239000000391 magnesium silicate Substances 0.000 claims abstract description 29
- 229920001155 polypropylene Polymers 0.000 claims abstract description 29
- 239000000843 powder Substances 0.000 claims abstract description 29
- 229910052500 inorganic mineral Inorganic materials 0.000 claims abstract description 15
- 239000011707 mineral Substances 0.000 claims abstract description 15
- 239000002994 raw material Substances 0.000 claims description 48
- 239000006096 absorbing agent Substances 0.000 claims description 17
- 239000003963 antioxidant agent Substances 0.000 claims description 17
- 230000003078 antioxidant effect Effects 0.000 claims description 17
- 239000000463 material Substances 0.000 claims description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 8
- 238000012986 modification Methods 0.000 claims description 6
- 230000004048 modification Effects 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 4
- 238000004090 dissolution Methods 0.000 claims description 3
- 238000005516 engineering process Methods 0.000 abstract description 20
- 238000005265 energy consumption Methods 0.000 abstract description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N iron oxide Inorganic materials [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 16
- NDLPOXTZKUMGOV-UHFFFAOYSA-N oxo(oxoferriooxy)iron hydrate Chemical compound O.O=[Fe]O[Fe]=O NDLPOXTZKUMGOV-UHFFFAOYSA-N 0.000 description 16
- 230000032683 aging Effects 0.000 description 7
- 238000002474 experimental method Methods 0.000 description 6
- 238000005034 decoration Methods 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 230000003245 working effect Effects 0.000 description 3
- 239000002253 acid Substances 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 239000004816 latex Substances 0.000 description 2
- 229920000126 latex Polymers 0.000 description 2
- 230000014759 maintenance of location Effects 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000178 monomer Substances 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 238000005245 sintering Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 206010019909 Hernia Diseases 0.000 description 1
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
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- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000009422 external insulation Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 230000009970 fire resistant effect Effects 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 150000001282 organosilanes Chemical class 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000004078 waterproofing Methods 0.000 description 1
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- Compositions Of Oxide Ceramics (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
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Abstract
The invention discloses a kind of porcelain tendre, comprise the component of following weight proportion: Magnesium Silicate q-agent 5-15 part, Calucium Silicate powder 5-15 part, earth 10-30 part, stone flour 10-25 part, quartz sand 20-40 part, vinylformic acid 5-15 part, mineral dye 1-2 part, water-resisting agent 0.2-0.8 part and polypropene staple 1-3 part.The present invention also discloses a kind of preparation method of porcelain tendre.Porcelain tendre of the present invention has the weathering resistance of good water-repellancy, flexibility and overlength, and its preparation technology is simple, and burns till link without the need to high temperature, only need under the environment of 180-200 DEG C baking-curing, energy consumption reduces greatly.
Description
Technical field
The present invention relates to building and decoration material field, particularly relate to a kind of porcelain tendre with and preparation method thereof.
Background technology
Porcelain tendre (MCM material) is a kind of novel energy-saving low-carbon finishing material.Explain according to " porcelain tendre building decoration engineering technology code " that Guangdong Province formulates: be main raw material by modification earth (MCM), use that special temperature control moulding system is shaping, baking, a kind of of cross-linking radiation have flexible building decoration plane materiel.
Porcelain tendre, as decorative material for wall surface, has light weight, flexible, appearance and modeling is various, the feature such as good weatherability; It is used as floor decorative material, has the features such as wear-resisting, anti-skidding, comfortable foot feeling; Easy construction is quick, than the traditional material reduction of erection time, saves space, cost-saving, and difficult drop-off.Be applicable to the building decorations such as exterior wall, interior wall, ground, be specially adapted to Highrise buildings exterior finish engineering, facade decorative engineering, Old City Reconstruction exterior wall plane materiel, the finish coat of external insulation system and the surface-veneer engineered of the opposite sex such as curved wall, arch post building.
Although soft ceramic tile has above-mentioned advantage, it need to improve in water resistance, ageing-resistant performance etc., and the preparation technology of existing porcelain tendre needs high temperature sintering mostly, and energy consumption is higher.
Summary of the invention
For this reason, the invention provides a kind of new porcelain tendre at least partially that at least can solve the problem with and preparation method thereof.
One aspect of the present invention provides a kind of porcelain tendre, comprise the component of following weight proportion: Magnesium Silicate q-agent 5-15 part, Calucium Silicate powder 5-15 part, earth 10-30 part, stone flour 10-25 part, quartz sand 20-40 part, vinylformic acid 5-15 part, mineral dye 1-2 part, water-resisting agent 0.2-0.8 part and polypropene staple 1-3 part.
Alternatively, according to porcelain tendre of the present invention, described porcelain tendre also includes the antioxidant of 0.2-0.8 weight part.
Alternatively, according to porcelain tendre of the present invention, described porcelain tendre also includes the UV light absorber of 0.2-0.8 weight part.
Alternatively, according to porcelain tendre of the present invention, in described porcelain tendre, the weight proportion of each component is: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, mineral dye 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.5 part, UV light absorber 0.5 part.
Alternatively, porcelain tendre of the present invention, described earth is the modification earth obtained for microwave treatment 20-50 minute at 350-450 DEG C by earth.
The present invention provides a kind of preparation method of porcelain tendre on the other hand, comprises the steps:
Material preparation step: the raw material preparing following weight proportion: Magnesium Silicate q-agent 5-15 part, Calucium Silicate powder 5-15 part, earth 10-30 part, stone flour 10-25 part, quartz sand 20-40 part, vinylformic acid 5-15 part, mineral dye 1-2 part, water-resisting agent 0.2-0.8 part and polypropene staple 1-3 part;
Mixing step: the water adding raw material gross weight 10-20% in described raw material, then adopt stirrer carry out being uniformly mixed until material dissolution, gel;
Steam-cured step: mixed raw material is poured in mould, then sends into drying room, steam-cured 30-50 minute at 180-200 DEG C, obtains initial porcelain tendre;
Curing step: by described initial porcelain tendre cooling, natural curing 7-15 days.
Alternatively, preparation in accordance with the present invention, described porcelain tendre also includes the antioxidant of 0.2-0.8 weight part.
Alternatively, preparation in accordance with the present invention, described porcelain tendre also includes the UV light absorber of 0.2-0.8 weight part.
Alternatively, preparation in accordance with the present invention, in described porcelain tendre, the weight proportion of each component is: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, mineral dye 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.5 part, UV light absorber 0.5 part.
Alternatively, preparation method of the present invention, described earth is the modification earth obtained for microwave treatment 20-50 minute at 350-450 DEG C by earth.
Porcelain tendre of the present invention has the weathering resistance of good water-repellancy, flexibility and overlength, and its preparation technology is simple, and without the need to high temperature sintering link, only need under the environment of 180-200 DEG C baking-curing, energy consumption reduces greatly.
Accompanying drawing explanation
By reading hereafter detailed description of the preferred embodiment, various other advantage and benefit will become cheer and bright for those of ordinary skill in the art.Accompanying drawing only for illustrating the object of preferred implementation, and does not think limitation of the present invention.In the accompanying drawings:
Fig. 1 is the schematic flow sheet of porcelain tendre preparation method of the present invention.
Embodiment
Below in conjunction with accompanying drawing and concrete embodiment, the invention will be further described.
One aspect of the present invention provides a kind of porcelain tendre, it comprises the component of following weight proportion: Magnesium Silicate q-agent 5-15 part, Calucium Silicate powder 5-15 part, earth 10-30 part, stone flour 10-25 part, quartz sand 20-40 part, vinylformic acid 5-15 part, mineral dye 1-2 part, water-resisting agent 0.2-0.8 part and polypropene staple 1-3 part.Preferably, the weight proportion of each component is: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, mineral dye 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts.
In above-mentioned each component, described earth is through the earth of modification, particularly, earth is placed in microwave oven, at 350-450 DEG C of temperature, process 20-50 minute.The stone flour product that described stone flour can adopt such as Paris white etc. commercially available.Described quartz sand generally adopts particle diameter to be 80-200 object product.Described vinylformic acid preferably uses organosilicon crylic acid latex, and it is that the organosilane monomer containing unsaturated link(age) and acrylic monomer are added suitable auxiliary agent, the emulsion be polymerized by the coated polymerization technique of nucleocapsid.Organosilicon crylic acid latex combines organosilicon fire-resistant, weathering resistance, chemical-resistant, high tint retention, snappiness, the tack of the low not v ulnerability of hydrophobic, surface energy and acrylic resin, it can be used as the raw material preparing porcelain tendre, the weathering resistance of porcelain tendre finished product, water tolerance and resistance to crocking can be improved.Described mineral dye generally adopts ferric oxide, because it has good opacifying power and tinting strength, chemical resistant properties, tint retention, dispersiveness, price is more honest and cleaner.Described water-resisting agent preferably uses waterproofing agent of organosilicon.
According to porcelain tendre of the present invention, described porcelain tendre also includes the antioxidant of 0.2-0.8 weight part; And described porcelain tendre also includes the UV light absorber of 0.2-0.8 weight part.By adding appropriate antioxidant and UV light absorber, thus effectively preventing porcelain tendre finished product from reducing its work-ing life because of oxygenizement or uviolizing or fading, ensureing work-ing life and the quality of product.Described oxygenant and UV light absorber adopt various product well known in the prior art, such as antioxidant 1010, oxidation inhibitor 164, UV light absorber UV-O, UV light absorber UV-9 etc.
The present invention provides the preparation method of above-mentioned porcelain tendre on the other hand, and Fig. 1 illustrates the schematic flow sheet of porcelain tendre preparation method of the present invention.As shown in Figure 1, first described preparation method enters material preparation step S1100, namely the various raw materials prepared needed for porcelain tendre are prepared, the weight proportion of raw material is as follows: Magnesium Silicate q-agent 5-15 part, Calucium Silicate powder 5-15 part, earth 10-30 part, stone flour 10-25 part, quartz sand 20-40 part, vinylformic acid 5-15 part, mineral dye 1-2 part, water-resisting agent 0.2-0.8 part and polypropene staple 1-3 part.Preferably, the weight proportion of described each raw material is: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, mineral dye 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts.The antioxidant of 0.2-0.8 weight part (being preferably 0.5 weight part) can also be included in described raw material, and comprise the UV light absorber of 0.2-0.8 weight part (being preferably 0.5 weight part) further.
After having got the raw materials ready, by described various raw material mixing, namely enter mixing step S1200.Particularly, in described raw material, add the water of raw material gross weight 10-20%, then adopt stirrer to be uniformly mixed by each raw material, until raw material fully dissolves, gel.After raw material gel, also need to carry out steam-cured step S1300, concrete operations are: the raw material after gel is poured into die for molding by transferpump, then sending into drying room carries out steam-cured, steam curing temperature is 180-200 DEG C, and the time is 30-50 minute, steam-cured complete after obtain initial porcelain tendre.Finally, enter curing step S1400, by described initial porcelain tendre cooling, natural curing 7-15 days.Wherein, so-called natural curing, be exactly by initial porcelain tendre after steam-cured, be placed on outdoor, give free rein to development.Before carrying out natural curing, the preliminary treatment such as carving, cutting can be carried out by specific equipment to initial porcelain tendre.After completing natural curing, namely obtain porcelain tendre finished product.
More according to the porcelain tendre that the present invention proposes and preparation method thereof optional element, can design various embodiments, therefore specific embodiment is only as the exemplary illustration of specific implementation of the present invention, and does not form limitation of the scope of the invention.In order to concrete description the present invention, following examples are selected to carry out exemplary illustration.
Embodiment 1
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 5 parts, Calucium Silicate powder 5 parts, 10 parts, earth, stone flour 10 parts, quartz sand 20 parts, 5 parts, vinylformic acid, mineral dye 1 part, water-resisting agent 0.2 part and polypropene staple 1 part.
The preparation technology of the porcelain tendre of above-mentioned formula is as follows:
First the raw material prepared needed for porcelain tendre is prepared according to following weight proportion: Magnesium Silicate q-agent 5 parts, Calucium Silicate powder 5 parts, 10 parts, earth, stone flour 10 parts, quartz sand 20 parts, 5 parts, vinylformic acid, ferric oxide 1 part, water-resisting agent 0.2 part and polypropene staple 1 part.In described raw material, add the water of raw material gross weight 10%, then adopt stirrer carry out being uniformly mixed until material dissolution, gel; Be poured in mould by mixed raw material, then send into drying room and then send into drying room and carry out steam-cured, steam curing temperature is 180 DEG C, and the time is 30 minutes, steam-cured complete after obtain initial porcelain tendre; By described initial porcelain tendre cooling, natural curing 7 days, obtains porcelain tendre finished product.
Embodiment 2
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 5 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1.
Embodiment 3
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 5 parts, 10 parts, earth, stone flour 20 parts, quartz sand 20 parts, 15 parts, vinylformic acid, ferric oxide 2 parts, water-resisting agent 0.2 part and polypropene staple 1 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1, and difference is, the weight of the water added in mixing step is 15% of raw material gross weight, and steam curing temperature is 190 DEG C.
Embodiment 4
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1, and difference is, the weight of the water added in mixing step is 15% of raw material gross weight, and steam curing temperature is 190 DEG C, and the steam-cured time is 40 minutes.
Embodiment 5
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 5 parts, Calucium Silicate powder 15 parts, 30 parts, earth, stone flour 25 parts, quartz sand 40 parts, 15 parts, vinylformic acid, ferric oxide 2 parts, water-resisting agent 0.8 part and polypropene staple 3 parts.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1, and difference is, the steam-cured time is 40 minutes.
Embodiment 6
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 15 parts, 30 parts, earth, stone flour 25 parts, quartz sand 40 parts, 5 parts, vinylformic acid, ferric oxide 1 part, water-resisting agent 0.8 part and polypropene staple 3 parts.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1, and difference is, the weight of the water added in mixing step is 15% of raw material gross weight, and steam curing temperature is 200 DEG C, and the steam-cured time is 40 minutes.
Embodiment 7
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 15 parts, Calucium Silicate powder 5 parts, 20 parts, earth, stone flour 15 parts, quartz sand 40 parts, 10 parts, vinylformic acid, ferric oxide 2 parts, water-resisting agent 0.5 part and polypropene staple 2 parts.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 4, and difference is, the steam-cured time is 50 minutes.
Embodiment 8
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 15 parts, Calucium Silicate powder 10 parts, 30 parts, earth, stone flour 25 parts, quartz sand 20 parts, 5 parts, vinylformic acid, ferric oxide 1 part, water-resisting agent 0.8 part and polypropene staple 1 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1, and difference is, the steam-cured time is 50 minutes.
Embodiment 9
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 15 parts, Calucium Silicate powder 15 parts, 10 parts, earth, stone flour 10 parts, quartz sand 30 parts, 15 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.2 part and polypropene staple 3 parts.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1, and difference is, the weight of the water added in mixing step is 25% of raw material gross weight, and steam curing temperature is 190 DEG C, and the steam-cured time is 40 minutes.
Embodiment 10
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.5 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 4.
Embodiment 11
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.2 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1.
Embodiment 12
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.8 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1.
Embodiment 13
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.8 part, UV light absorber 0.2 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1.
Embodiment 14
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.5 part, UV light absorber 0.5 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 4.
Embodiment 15
The present embodiment porcelain tendre is made up of the raw material of following weight proportion: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, ferric oxide 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.2 part, UV light absorber 0.8 part.
The preparation technology of the porcelain tendre of above-mentioned formula is with embodiment 1.
The porcelain tendre prepared through above-described embodiment 1-15 has the weathering resistance of good water-repellancy, flexibility and overlength.In order to the These parameters performance of porcelain tendre of the present invention is described better, applicant has carried out water-repellancy experiment, flexible experiment and ageing-resistant experiment respectively to the porcelain tendre product prepared.Wherein, what water-repellancy was tested is operating as: the porcelain tendre prepared is placed in water and soaks, measure the water-intake rate of porcelain tendre after 1 month; Being operating as of flexible experiment: be wrapped on the right cylinder that diameter is 20cm by the porcelain tendre prepared, observes it whether occur cracking; Whether the concrete operations of ageing-resistant experiment are: irradiate 2500 hours to porcelain tendre finished product in hernia lamp ageing oven, observe it occur aging.Experimental result shows, the porcelain tendre water-intake rate prepared by embodiment of the present invention 1-15 is all less than 5%, and water resistance is good; All occur without cracking phenomena in flexible experiment, its flexility is also better; Ageing-resistant test is simultaneously after 2500 hours, and product does not occur catabiosis, has the ageing-resistant time of overlength, ensures that it has longer work-ing life.
It should be noted, the present invention will be described instead of limit the invention for above-described embodiment, and those skilled in the art can design alternative embodiment when not departing from the scope of claims.In the claims, any reference symbol between bracket should be configured to limitations on claims.Word " comprises " not to be got rid of existence and does not arrange element in the claims or step.Word first, second and third-class use do not represent any order, can be title by these word explanations.
Claims (8)
1. a porcelain tendre, comprise the component of following weight proportion: Magnesium Silicate q-agent 5-15 part, Calucium Silicate powder 5-15 part, earth 10-30 part, stone flour 10-25 part, quartz sand 20-40 part, vinylformic acid 5-15 part, mineral dye 1-2 part, water-resisting agent 0.2-0.8 part and polypropene staple 1-3 part; Wherein, described earth is the modification earth obtained for microwave treatment 20-50 minute at 350-450 DEG C by earth.
2. porcelain tendre according to claim 1, wherein, described porcelain tendre also includes the antioxidant of 0.2-0.8 weight part.
3. porcelain tendre according to claim 2, wherein, described porcelain tendre also includes the UV light absorber of 0.2-0.8 weight part.
4. porcelain tendre according to claim 3, wherein, in described porcelain tendre, the weight proportion of each component is: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, mineral dye 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.5 part, UV light absorber 0.5 part.
5. a preparation method for porcelain tendre, comprises the steps:
Material preparation step (S1100): the raw material preparing following weight proportion: Magnesium Silicate q-agent 5-15 part, Calucium Silicate powder 5-15 part, earth 10-30 part, stone flour 10-25 part, quartz sand 20-40 part, vinylformic acid 5-15 part, mineral dye 1-2 part, water-resisting agent 0.2-0.8 part and polypropene staple 1-3 part; Wherein, described earth is the modification earth obtained for microwave treatment 20-50 minute at 350-450 DEG C by earth;
Mixing step (S1200): the water adding raw material gross weight 10-20% in described raw material, then adopt stirrer carry out being uniformly mixed until material dissolution, gel;
Steam-cured step (S1300): mixed raw material is poured in mould, then sends into drying room, steam-cured 30-50 minute at 180-200 DEG C, obtains initial porcelain tendre;
Curing step (S1400): by described initial porcelain tendre cooling, natural curing 7-15 days.
6. preparation method according to claim 5, wherein, in described material preparation step (S1100), described raw material also comprises the antioxidant of 0.2-0.8 weight part.
7. preparation method according to claim 6, wherein, in described material preparation step (S1100), described raw material also includes the UV light absorber of 0.2-0.8 weight part.
8. preparation method according to claim 7, wherein, in described material preparation step (S1100), the weight proportion of described raw material is: Magnesium Silicate q-agent 10 parts, Calucium Silicate powder 10 parts, 20 parts, earth, stone flour 15 parts, quartz sand 30 parts, 10 parts, vinylformic acid, mineral dye 1.5 parts, water-resisting agent 0.5 part and polypropene staple 2 parts, antioxidant 0.5 part, UV light absorber 0.5 part.
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| CN104446177A (en) * | 2014-11-03 | 2015-03-25 | 湖北垚美软瓷有限公司 | Method for preparing soft porcelain archaized brick by utilizing manganese residue tailings |
| CN107298277A (en) * | 2016-01-18 | 2017-10-27 | 孙欣 | A kind of travelling belt |
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| CN106830789A (en) * | 2017-01-13 | 2017-06-13 | 高春 | A kind of porcelain tendre preparation method |
| CN106939678B (en) * | 2017-03-17 | 2021-01-19 | 潘长海 | Automatic production method of soft bricks |
| CN108275961A (en) * | 2018-01-26 | 2018-07-13 | 海宁市大众建材有限公司 | A kind of processing technology of porcelain tendre |
| CN108505705A (en) * | 2018-03-29 | 2018-09-07 | 安徽巨力新型环保材料有限公司 | Soft stone insulation and decoration integrated plate |
| CN108569882A (en) * | 2018-04-24 | 2018-09-25 | 吴刚 | A kind of preparation method of the energy saving porcelain tendre of microvesicle |
| CN108609911A (en) * | 2018-04-28 | 2018-10-02 | 无锡市辰元科技有限公司 | Heat insulating mortar and preparation method thereof, heat-insulated porcelain tendre and preparation method thereof and construction material |
| CN112500044A (en) * | 2020-12-04 | 2021-03-16 | 姚智 | Soft ceramic tile and preparation method thereof |
| CN112723851B (en) * | 2020-12-23 | 2022-08-09 | 宝润达新型材料股份有限公司 | Light flexible soft porcelain and preparation method thereof |
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