CN103980693B - A kind of garage floor material and preparation method thereof - Google Patents
A kind of garage floor material and preparation method thereof Download PDFInfo
- Publication number
- CN103980693B CN103980693B CN201410206929.XA CN201410206929A CN103980693B CN 103980693 B CN103980693 B CN 103980693B CN 201410206929 A CN201410206929 A CN 201410206929A CN 103980693 B CN103980693 B CN 103980693B
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- parts
- floor material
- garage
- preparation
- garage floor
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- 239000000463 material Substances 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000000203 mixture Substances 0.000 claims abstract description 37
- XHXUANMFYXWVNG-ADEWGFFLSA-N (-)-Menthyl acetate Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@H]1OC(C)=O XHXUANMFYXWVNG-ADEWGFFLSA-N 0.000 claims abstract description 26
- DROMNWUQASBTFM-UHFFFAOYSA-N dinonyl benzene-1,2-dicarboxylate Chemical compound CCCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCCC DROMNWUQASBTFM-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000001605 (5-methyl-2-propan-2-ylcyclohexyl) acetate Substances 0.000 claims abstract description 13
- XHXUANMFYXWVNG-UHFFFAOYSA-N D-menthyl acetate Natural products CC(C)C1CCC(C)CC1OC(C)=O XHXUANMFYXWVNG-UHFFFAOYSA-N 0.000 claims abstract description 13
- WVWZECQNFWFVFW-UHFFFAOYSA-N methyl 2-methylbenzoate Chemical compound COC(=O)C1=CC=CC=C1C WVWZECQNFWFVFW-UHFFFAOYSA-N 0.000 claims abstract description 13
- -1 polyethylene Polymers 0.000 claims abstract description 13
- 229920005749 polyurethane resin Polymers 0.000 claims abstract description 12
- 239000004698 Polyethylene Substances 0.000 claims abstract description 11
- 229920000573 polyethylene Polymers 0.000 claims abstract description 11
- 239000003822 epoxy resin Substances 0.000 claims abstract description 9
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 9
- 239000004111 Potassium silicate Substances 0.000 claims abstract description 7
- NNHHDJVEYQHLHG-UHFFFAOYSA-N potassium silicate Chemical compound [K+].[K+].[O-][Si]([O-])=O NNHHDJVEYQHLHG-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052913 potassium silicate Inorganic materials 0.000 claims abstract description 7
- 235000019353 potassium silicate Nutrition 0.000 claims abstract description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 6
- 229920005989 resin Polymers 0.000 claims description 6
- 239000011347 resin Substances 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 150000002148 esters Chemical class 0.000 claims description 5
- 230000006641 stabilisation Effects 0.000 claims description 5
- 238000011105 stabilization Methods 0.000 claims description 5
- VPWNQTHUCYMVMZ-UHFFFAOYSA-N 4,4'-sulfonyldiphenol Chemical compound C1=CC(O)=CC=C1S(=O)(=O)C1=CC=C(O)C=C1 VPWNQTHUCYMVMZ-UHFFFAOYSA-N 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- QPJVMBTYPHYUOC-UHFFFAOYSA-N Methyl benzoate Natural products COC(=O)C1=CC=CC=C1 QPJVMBTYPHYUOC-UHFFFAOYSA-N 0.000 claims 1
- 229910021529 ammonia Inorganic materials 0.000 claims 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 1
- XNGIFLGASWRNHJ-UHFFFAOYSA-N o-dicarboxybenzene Natural products OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 claims 1
- ZWLPBLYKEWSWPD-UHFFFAOYSA-N o-toluic acid Chemical compound CC1=CC=CC=C1C(O)=O ZWLPBLYKEWSWPD-UHFFFAOYSA-N 0.000 claims 1
- 238000001816 cooling Methods 0.000 abstract 1
- 230000029087 digestion Effects 0.000 abstract 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000004166 bioassay Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
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- Floor Finish (AREA)
Abstract
The present invention relates to a kind of garage floor material and preparation method thereof, garage floor material is made up of according to weight ratio following composition: dinonyl phthalate is that 13～17 parts, menthyl acetate are that 5～9 parts, o-methyl benzoic acid methyl ester are that 4～7 parts, polyurethane resin are that 16～18 parts, potassium silicate are that 11～16 parts, bisphenol-s epoxy resin are that 9～12 parts, polyethylene are 5～8 parts. The preparation method of garage floor material comprises high-temperature digestion, mixes, the step such as cooling. The garage floor material scuff resistance and the high-temperature capability that prepare are higher.
Description
Technical field
The present invention relates to a kind of floor material and preparation method thereof, particularly relate to ground, a kind of garageTerrace material and preparation method thereof.
Background technology
The use approach of floor material is more, classifies also a lot. Wherein garage floor material is itIn a very important application. Underground garage, conventionally need to be to earth's surface after construction completesLay floor material. Lay after floor material, owing to having for a long time vehicle operating, thereforeThe floor material of laying need to have good wearability. In addition, in more hot area,Car storehouse temperature is very high, if floor material be heated after state labile, change, can shadowThe flatness of ringing terrace, therefore floor material also needs to have higher resistance to elevated temperatures.
Summary of the invention
The technical problem solving: conventional garage floor material resistance to elevated temperatures and anti-wear performancePoor problem.
Technical scheme: the invention discloses a kind of garage floor material, garage floor material by withLower composition forms according to weight ratio: dinonyl phthalate is 13～17 parts, acetic acid peppermintEster is that 5～9 parts, o-methyl benzoic acid methyl ester are that 4～7 parts, polyurethane resin are 16～18Part, potassium silicate is that 11～16 parts, bisphenol-s epoxy resin are that 9～12 parts, polyethylene are5～8 parts.
A preparation method for garage floor material, preparation method comprises the following steps: (1) willTemperature Setting is 85 DEG C～95 DEG C, and after temperature stabilization, getting dinonyl phthalate is 13～17Part, menthyl acetate is that 5～9 parts, o-methyl benzoic acid methyl ester are 4～7 parts, polyurethane treeFat is 16～18 parts, by dinonyl phthalate, menthyl acetate, o-toluic acidMethyl esters, four kinds of compositions of polyurethane resin mix; (2) in mixture, add successively silicon againAcid potassium is that 11～16 parts, bisphenol-s epoxy resin are that 9～12 parts, polyethylene are 5～8 parts;(3) finally carry out again mix and blend, after stirring, be cooled to room temperature, prepare garage terraceMaterial.
A preparation method for garage floor material, in floor material composition, polyurethane resin is preferredIt is 17 parts.
A preparation method for garage floor material, bisphenol S type ring in garage floor material compositionEpoxy resins is preferably 12 parts.
A preparation method for garage floor material, in garage floor material composition, polyethylene is preferredIt is 5 parts.
Beneficial effect: the garage floor material that the present invention prepares has good heat-resisting quantityCan and anti-wear performance, the garage floor material preparing dry at can resistance to 80 DEG C 12h to 36h withoutDistortion, the anti-wear performance of garage floor material is 0.015～0.018g/cm2 (750g, 500r).
Detailed description of the invention
Embodiment 1
(1) be 85 DEG C by Temperature Setting, after temperature stabilization, get dinonyl phthalate and be15kg, menthyl acetate are that 7kg, o-methyl benzoic acid methyl ester are that 4kg, polyurethane resin are18kg, by dinonyl phthalate, menthyl acetate, o-methyl benzoic acid methyl ester, poly-ammoniaFour kinds of compositions of ester resin mix; (2) again to add successively in mixture potassium silicate be 11kg,Bisphenol-s epoxy resin is that 12kg, polyethylene are 8kg; (3) finally carry out again mix and blend,After stirring, be cooled to room temperature, prepare garage floor material.
Embodiment 2
(1) be 95 DEG C by Temperature Setting, after temperature stabilization, get dinonyl phthalate and be17kg, menthyl acetate are that 5kg, o-methyl benzoic acid methyl ester are that 7kg, polyurethane resin are16kg, by dinonyl phthalate, menthyl acetate, o-methyl benzoic acid methyl ester, poly-ammoniaFour kinds of compositions of ester resin mix; (2) again to add successively in mixture potassium silicate be 16kg,Bisphenol-s epoxy resin is that 9kg, polyethylene are 5kg; (3) finally carry out again mix and blend,After stirring, be cooled to room temperature, prepare garage floor material.
Embodiment 3
(1) be 90 DEG C by Temperature Setting, after temperature stabilization, get dinonyl phthalate and be13kg, menthyl acetate are that 9kg, o-methyl benzoic acid methyl ester are that 6kg, polyurethane resin are17kg, by dinonyl phthalate, menthyl acetate, o-methyl benzoic acid methyl ester, poly-ammoniaFour kinds of compositions of ester resin mix; (2) again to add successively in mixture potassium silicate be 14kg,Bisphenol-s epoxy resin is that 11kg, polyethylene are 6kg; (3) finally carry out again mix and blend,After stirring, be cooled to room temperature, prepare garage floor material.
The scuff resistance bioassay standard of the embodiment preparing is GB/T1768-1979. High temperature resistant surveyThe method of determining is placed on respectively at 80 DEG C for embodiment 1 to 3 is prepared to garage floor materialDry 12h, 24h, 36h. Embodiment 1, embodiment 2, embodiment 3 after placement finishesThat garage floor material does not all have is softening, the phenomenon of distortion. The scuff resistance of embodiment 1 to 3 asUnder.
Claims (5)
1. a garage floor material, it is characterized in that garage floor material by following composition byForm according to weight ratio: dinonyl phthalate is that 13～17 parts, menthyl acetate are 5～9Part, o-methyl benzoic acid methyl ester is that 4～7 parts, polyurethane resin are 16～18 parts, potassium silicateBe that 11～16 parts, bisphenol-s epoxy resin are that 9～12 parts, polyethylene are 5～8 parts;
Described garage floor material preparation method comprises the following steps: (1) by Temperature Setting is85 DEG C～95 DEG C, after temperature stabilization, get dinonyl phthalate and be 13～17 parts, acetic acid thinLotus ester be 5～9 parts, o-methyl benzoic acid methyl ester be 4～7 parts, polyurethane resin be 16～18 parts, by dinonyl phthalate, menthyl acetate, o-methyl benzoic acid methyl ester, poly-Four kinds of compositions of ammonia ester resin mix; (2) in mixture, add successively potassium silicate to be again11～16 parts, bisphenol-s epoxy resin are that 9～12 parts, polyethylene are 5～8 parts; (3)Finally carry out again mix and blend, after stirring, be cooled to room temperature, prepare garage floor material.
2. the preparation method of a kind of garage according to claim 1 floor material, its spyLevy and be that preparation method comprises the following steps: (1) is 85 DEG C～95 DEG C by Temperature Setting, temperatureAfter degree is stable, get dinonyl phthalate and be 13～17 parts, menthyl acetate and be 5～9 parts,O-methyl benzoic acid methyl ester is that 4～7 parts, polyurethane resin are 16～18 parts, by O-phthalicAcid ester in two ninth of the ten Heavenly Stems, menthyl acetate, o-methyl benzoic acid methyl ester, four kinds of compositions of polyurethane resin mixClose evenly; (2) be 11～16 parts, bisphenol S type to adding successively potassium silicate in mixture againEpoxy resin is that 9～12 parts, polyethylene are 5～8 parts; (3) finally carry out again mix and blend,After stirring, be cooled to room temperature, prepare garage floor material.
3. the preparation method of a kind of garage according to claim 2 floor material, its spyLevy and be that in garage floor material composition, polyurethane resin is 17 parts.
4. the preparation method of a kind of garage according to claim 2 floor material, its spyLevy and be that in garage floor material composition, bisphenol-s epoxy resin is 12 parts.
5. the preparation method of a kind of garage according to claim 2 floor material, its spyLevy and be that in garage floor material composition, polyethylene is 5 parts.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410206929.XA CN103980693B (en) | 2014-05-16 | 2014-05-16 | A kind of garage floor material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410206929.XA CN103980693B (en) | 2014-05-16 | 2014-05-16 | A kind of garage floor material and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103980693A CN103980693A (en) | 2014-08-13 |
| CN103980693B true CN103980693B (en) | 2016-05-04 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410206929.XA Expired - Fee Related CN103980693B (en) | 2014-05-16 | 2014-05-16 | A kind of garage floor material and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN103980693B (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101343400A (en) * | 2008-09-02 | 2009-01-14 | 中南大学 | MG filled polyurethane modified epoxy resin embedding material and preparation thereof |
| CN101654583A (en) * | 2009-09-24 | 2010-02-24 | 北京红狮漆业有限公司 | Compound epoxy flooring coating and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI431031B (en) * | 2009-10-02 | 2014-03-21 | Mitsubishi Rayon Co | Fabricating method of fiber reinforced composition and heat-resistant die and heat-resistant structural material using fiber reinforced composition |
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2014
- 2014-05-16 CN CN201410206929.XA patent/CN103980693B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101343400A (en) * | 2008-09-02 | 2009-01-14 | 中南大学 | MG filled polyurethane modified epoxy resin embedding material and preparation thereof |
| CN101654583A (en) * | 2009-09-24 | 2010-02-24 | 北京红狮漆业有限公司 | Compound epoxy flooring coating and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN103980693A (en) | 2014-08-13 |
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Granted publication date: 20160504 |