CN103932945A - Natural moisturizing mask and preparation method thereof - Google Patents
Natural moisturizing mask and preparation method thereof Download PDFInfo
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- CN103932945A CN103932945A CN201410154947.8A CN201410154947A CN103932945A CN 103932945 A CN103932945 A CN 103932945A CN 201410154947 A CN201410154947 A CN 201410154947A CN 103932945 A CN103932945 A CN 103932945A
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- angelicae dahuricae
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Abstract
The invention discloses a natural moisturizing mask. The natural moisturizing mask comprises the following components in parts by weight: 10 to 20 parts of pollen extracting liquid, 10 to 15 parts of radix angelicae extracting liquid, 5 to 10 parts of sodium alga acid, 5 to 10 parts of glycerinum, 1 to 5 parts of citric acid, 0.5 to 1 part of moisturizing chitosan oligosaccharide, and 40 to 70 parts of deionized water. The invention also discloses a preparation method of the natural moisturizing mask. The natural moisturizing mask composed of natural components has high safety coefficient, is suitable for any skin, and has a plurality of skin protection effects, such as moisturizing, tendering skin, whitening, and removing stain and whelk.
Description
Technical field
The present invention relates to cosmetic field, particularly a kind of natural moisture preserving facial film and preparation method thereof.
Background technology
Along with improving constantly of living standard, and all pollutions of living environment condition, adopt cosmetics to improve the only selection that skin has become people.Facial film is used as the carrier of the face beautifying health keeping product personage that liked to be beautiful widely, especially female consumer.Moisture saver mask is because moistening effect is outstanding, and good absorbing effect, has been subject to the favor of more and more consumers.
At present skin care item taste mainly by contained natural component number and skin effect decide, skin care item more and more trend towards naturalization, synthetic function.What the skin-protection product of the state such as American-European-Japanese contained natural plants accounts for 80%, but the cosmetics that China market contains natural plants are less, and especially composition is single, can not be applicable to various skin problem.Chinese patent CN201210557450.1 discloses a kind of moisture saver mask, although selected Chinese medicine as raw material.Chinese patent CN200710302100.X discloses a kind of pearl vitamin E whitening moisturizing face masque and preparation method thereof, Chinese patent CN200710187487.9 discloses a kind of formula and preparation technology of pure Chinese medicine whitening moisturizing face masque, Chinese patent CN201110103296.6 discloses a kind of moisture saver mask, Chinese patent 200810060551.1 discloses a kind of moisture saver mask and preparation method thereof, and these patents have added chemical antibacterial or the chemical preservatives such as methyl parahydroxybenzoate, two imidazolidinyl urea.In addition, Chinese patent CN201210522031.4, discloses a kind of Flos Inulae facial film, adopts Flos Inulae extract as the Major Nutrient agent of facial film.But all there is certain problem in the preparation process of the facial film of above-mentioned Patent design and facial film: (1) is in order to extend antiseptic (antibacterial) and the synthetic perfume that has added some synthetic in the shelf-life of facial film and the quality facial film raw material of facial film, these materials have a certain impact to skin tool, if life-time service can infiltrate human body by skin, facial skin mucosa is produced to destruction, in addition, some of them material can make skin produce anaphylaxis, is not suitable for all skin quality crowds and uses; (2) facial film adopts expensive natural materials as the main component of facial film, directly carries out composite making, and so not only affects the absorption of skin to nutrient substance, and expensive, and Chinese medicine exists some unjoyful abnormal smells from the patients to have influence on it and uses desire in addition; (3) facial film adopts a kind of natural materials as the nutrient of facial film, and its nutritional labeling kind and content are limited, does not reach the effect of comprehensive solution skin global question.
Summary of the invention
In order to overcome the above-mentioned shortcoming and deficiency of prior art, the object of the present invention is to provide a kind of natural moisture preserving facial film, composition is natural, and safety coefficient is high, the crowd who is suitable for any skin quality uses, and has the multiple skin-care effects such as moisturizing, skin care, whitening and dispelling stain, comedo.
The invention also discloses the preparation method of above-mentioned natural moisture preserving facial film.
Object of the present invention is achieved through the following technical solutions:
A natural moisture preserving facial film, according to weighing scale, comprises pollen extracting liquid 10-20 part, Radix Angelicae Dahuricae extracting solution 10-15 part, sodium alginate 5-10, glycerol 5-10 part, citric acid 1-5 part, moisturizing oligo-chitosan 0.5-1 part, deionized water 40-70 part.
A preparation method for natural moisture preserving facial film, comprises the following steps:
(1) according to weighing scale, by sodium alginate sodium alginate 5-10, glycerol 5-10 part, citric acid 1-5 part, moisturizing oligo-chitosan 0.5-1 part, deionized water 40-70 part is mixed, and is heated to 60-80 ℃, obtains basal liquid;
(2), according to weighing scale, by pollen extracting liquid 10-20 part, Radix Angelicae Dahuricae extracting solution 10-15 part adds in described basal liquid, obtains facial film solution;
(3) opposite coating solution carries out emulsifying operation, rotating speed 1000-12000r/min, and time 1-2h obtains facial film emulsion, is moisture saver mask.
The preparation process of described pollen extracting liquid is as follows:
Choose pollen (processed by breaking wall) dry, remove impurity, carry out ultrasonic assisted extraction, obtain preliminary pollen extracting liquid; Adopt active carbon to decolour, take off taste to the preliminary pollen extracting liquid extracting and process, then pass through centrifugally operated, obtain pollen extracting liquid;
Described ultrasonic assisted extraction is specially: the weight ratio of pollen (processed by breaking wall) and water is 1:10-20, carries out ultrasonic Treatment in the time of extraction; Extraction time is 10-30min, and extraction temperature is 40-60 ℃, and ultrasonic power is 400W-800W.
The preparation method of described Radix Angelicae Dahuricae extracting solution is as follows:
The Radix Angelicae Dahuricae powder that choose dry, remove impurity, pulverizes and sieves, carries out ultrasonic assisted extraction; Obtain preliminary Radix Angelicae Dahuricae extracting solution, adopt active carbon to decolour, take off taste to preliminary Radix Angelicae Dahuricae extracting solution and process, then pass through centrifugally operated, obtain Radix Angelicae Dahuricae extracting solution;
Described ultrasonic assisted extraction is specially: the weight ratio of Radix Angelicae Dahuricae powder and water is 1:10-20, carries out ultrasonic Treatment in the time of extraction; Extraction time is 10-30min, and extraction temperature is 40-60 ℃, and ultrasonic power is 400W-800W.
The preparation method of described moisturizing oligo-chitosan is as follows:
In the chitosan solution that is 1%-5% to mass concentration, adding mass concentration is 30% hydrogen peroxide solution, obtains mixed liquor; Make the mass concentration of hydrogen peroxide in mixed liquor reach 1%-2%; After stirring at room 10-20min, by liquor pump, mixed liquor is sent into high-voltage pulse electric field device and process, time 30-60min, field intensity 10-20kV/cm, carries out spray drying treatment after being warming up to the 60-80 ℃ of hydrogen peroxide of removing in mixed liquor; Described spray process conditions is: 160 ℃-180 ℃ of inlet temperatures, intake 20-30m
3/ h, feed rate 0.2-0.3L/h, obtains moisturizing oligo-chitosan, and its molecular weight is less than 5000Da.
Principle of the present invention is: facial film of the present invention all adopts natural materials, wherein pollen and the Radix Angelicae Dahuricae have abundant aminoacid, vitamin, mineral element, also there is flavone, polysaccharide isoreactivity material, not only for skin provides a large amount of nutritional labelings, and there is the effects such as good antioxidation, defying age, whitening, antiinflammatory.In order to improve the absorption of skin to pollen and Radix Angelicae Dahuricae nutrient substance, the present invention has carried out extraction operation to it, and in order to reach the convenience of application and to increase the desire that user is used, the present invention has also carried out decolouring, de-taste processing to extract.In order further to improve the long moistening effect of facial film, also added moisturizing oligo-chitosan, synergism due to high-pressure pulse electric and hydrogen peroxide, one side degrade chitosan, pass through on the one hand in addition Oxidation, form more unsaturated group and strengthen non-oxidizability, form more hydrophilic group and impel the hydrophilic groups such as more hydroxyl to expose, not only can increase the performance of keeping humidity of facial film, and there is the growth that broad spectrum antibacterial and non-oxidizability can suppress the harmful bacterias such as skin surface fungus, suppress the growth of comedo.In addition, added a certain amount of citric acid solution, pH microenvironment that not only can regulation of skin, and there is softening skin, accelerate the texts that comes off of dermal melanin.
Compared with prior art, the present invention has the following advantages and beneficial effect: facial film composition of the present invention is natural, safety coefficient is high, the crowd who is suitable for any skin quality uses, have the multiple skin-care effects such as coming off of antioxidation, defying age, whitening, antiinflammatory, softening skin, acceleration dermal melanin, and moistening effect is better, skin is fast to the absorption of nutrient substance, simultaneously disposable, easy to use.
The specific embodiment
Below in conjunction with embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited to this.
Embodiment 1
The natural moisture preserving facial film of the present embodiment, according to weight fraction meter, comprises 15 parts of pollen extracting liquids, 10 parts of Radix Angelicae Dahuricae extracting solution, 5 parts of sodium alginates, 5 parts of glycerol, 1 part of citric acid, 0.5 part of moisturizing oligo-chitosan, 70 parts of deionized waters.
The preparation method of the natural moisture preserving facial film of the present embodiment is as follows:
The first step: the preparation of pollen extracting liquid
Choose breaking cellular wall Pollen Brassicae campestris dry, remove impurity, carry out ultrasonic assisted extraction (SB-25-12D ultrasonic washing unit, Ningbo excitement biotechnology joint-stock company) obtain pollen extracting liquid, concrete supersound extraction condition is: pollen: water is than being 1:10, when extracting, carry out ultrasonic Treatment, obtain preliminary pollen extracting liquid; Extraction time is 30min, and extracting temperature is 40 ℃, and ultrasonic power is 600W; Adopt 3% active carbon (Guangzhou Xiang Yuan active carbon company limited) to process 30min to the preliminary pollen extracting liquid extracting, decolouring, take off taste processes, pass through again centrifugally operated (TGL-15B centrifuge, Town in Shanghai booth science and technology instrument plant), obtain pollen extracting liquid.
Second step: the preparation of Radix Angelicae Dahuricae extracting solution
The Radix Angelicae Dahuricae powder of choosing dry, remove impurity and pulverizing and sieving, carries out ultrasonic assisted extraction and obtains Radix Angelicae Dahuricae extracting solution, and concrete supersound extraction condition is: Radix Angelicae Dahuricae powder: water, than being 1:10, carries out ultrasonic Treatment in the time of extraction, obtain preliminary Radix Angelicae Dahuricae extracting solution; Extraction time is 30min, and extracting temperature is 40 ℃, and ultrasonic power is 600W; Adopt 3% active carbon to process 30min to the preliminary Radix Angelicae Dahuricae extracting solution extracting, decolour, take off taste and process, then pass through centrifugally operated (TGL-15B centrifuge, Town in Shanghai booth science and technology instrument plant), obtain Radix Angelicae Dahuricae extracting solution.
The 3rd step: the preparation of moisturizing oligo-chitosan
Moisturizing oligo-chitosan is worked in coordination with high-pressure pulse electric (south China science and engineering light industry and food development) to the chitosan acquisition of degrading by hydrogen peroxide, and its molecular weight is less than 5000Da.Concrete treatment conditions are 30% hydrogen peroxide solution for adding mass concentration in the chitosan solution that is 1% to mass concentration, obtain mixed liquor; Make hydrogen peroxide concentration in mixed liquor reach 1%; After stirring at room 10min, by liquor pump, mixed liquor is sent into high-voltage pulse electric field device and process, time 30min, field intensity 10kV/cm, is warming up to 60 ℃ of hydrogen peroxide of removing in mixed liquor; The drying process (GPQ small-sized spray drier, Qianjiang drying equipment company limited) of spraying after processing, treatment conditions are 180 ℃ of inlet temperatures, intake 30m
3/ h, feed rate 0.3L/h, obtains moisturizing oligo-chitosan.
The 4th step: the preparation of moisture saver mask
According to weight fraction meter, by 5 parts of sodium alginates, 5 parts of glycerol, 1 part of citric acid, 0.5 part of moisturizing oligo-chitosan, 70 parts of mixing of deionized water, and be heated to 80 ℃, obtain basal liquid; According to weighing scale, by 15 parts of pollen extracting liquids, 10 parts of Radix Angelicae Dahuricae extracting solution add in described basal liquid, obtain facial film solution; By described facial film solution emulsifying (SRH-S450 laboratory high-shear emulsion machine, Shanghai Shi He mechanical & electronic equipment corporation, Ltd) rotating speed 10000r/min, time 2h, obtains facial film emulsion.The facial film safety coefficient of gained is high, and the crowd who is suitable for any skin quality uses, and homogeneous, has the good multiple effects such as moisturizing, skin care, whitening and dispelling stain, comedo that have, and moisturizing rate is higher than common facial film 22% left and right, market.
Embodiment 2
The natural moisture preserving facial film of the present embodiment, according to weight fraction meter, comprises 20 parts of pollen extracting liquids, 10 parts of Radix Angelicae Dahuricae extracting solution, 8 parts of sodium alginates, 8 parts of glycerol, 2 parts of citric acids, 1 part of moisturizing oligo-chitosan, 50 parts of deionized waters.
The preparation method of the natural moisture preserving facial film of the present embodiment is as follows:
The first step: the preparation of pollen extracting liquid
Choose breaking cellular wall Pollen Brassicae campestris dry, remove impurity, carry out ultrasonic assisted extraction (SB-25-12D ultrasonic washing unit, Ningbo excitement biotechnology joint-stock company) obtain pollen extracting liquid, concrete supersound extraction condition is: pollen: water is than being 1:20, when extracting, carry out ultrasonic Treatment, obtain preliminary pollen extracting liquid; Extraction time is 15min, and extracting temperature is 60 ℃, and ultrasonic power is 800W; Adopt 1% active carbon (Guangzhou Xiang Yuan active carbon company limited) to process 60min to the preliminary pollen extracting liquid extracting, decolour, take off taste and process, then pass through centrifugally operated (TGL-15B centrifuge, Town in Shanghai booth science and technology instrument plant), obtain pollen extracting liquid.
Second step: the preparation of Radix Angelicae Dahuricae extracting solution
The Radix Angelicae Dahuricae powder of choosing dry, remove impurity and pulverizing and sieving, carries out ultrasonic assisted extraction and obtains Radix Angelicae Dahuricae extracting solution, and concrete supersound extraction condition is: Radix Angelicae Dahuricae powder: water, than being 1:20, carries out ultrasonic Treatment in the time of extraction, obtain preliminary Radix Angelicae Dahuricae extracting solution; Extraction time is 15min, and extracting temperature is 60 ℃, and ultrasonic power is 800W; Adopt 1% active carbon to process 60min to the preliminary Radix Angelicae Dahuricae extracting solution extracting, decolour, take off taste and process, then pass through centrifugally operated (TGL-15B centrifuge, Town in Shanghai booth science and technology instrument plant), obtain Radix Angelicae Dahuricae extracting solution.
The 3rd step: the preparation of moisturizing oligo-chitosan
Moisturizing oligo-chitosan is worked in coordination with high-pressure pulse electric (south China science and engineering light industry and food development) to the chitosan acquisition of degrading by hydrogen peroxide, and its molecular weight is less than 5000Da.Concrete treatment conditions are 30% hydrogen peroxide solution for adding mass concentration in the chitosan solution that is 5% to mass concentration, obtain mixed liquor; Make hydrogen peroxide concentration in mixed liquor reach 2%, after stirring at room 20min, by liquor pump, mixed liquor is sent into high-voltage pulse electric field device and process, time 60min, field intensity 20kV/cm, is warming up to 80 ℃ of hydrogen peroxide of removing in mixed liquor; The drying process (GPQ small-sized spray drier, Qianjiang drying equipment company limited) of spraying after processing, treatment conditions are 160 ℃ of inlet temperatures, intake 20m
3/ h, feed rate 0.2L/h, obtains moisturizing oligo-chitosan.
The 4th step: the preparation of moisture saver mask
According to weight fraction meter, by 8 parts of sodium alginates, 8 parts of glycerol, 2 parts of citric acids, 1 part of moisturizing oligo-chitosan, 50 parts of mixing of deionized water, and be heated to 60 ℃, obtain basal liquid; According to weight fraction meter, by 20 parts of pollen extracting liquids, 10 parts of Radix Angelicae Dahuricae extracting solution add in described basal liquid, obtain facial film solution; By described facial film solution emulsifying (SRH-S450 laboratory high-shear emulsion machine, Shanghai Shi He mechanical & electronic equipment corporation, Ltd) rotating speed 12000r/min, time 1h, obtains facial film emulsion.The facial film safety coefficient of gained is high, and the crowd who is suitable for any skin quality uses, and homogeneous, has the good multiple effects such as moisturizing, skin care, whitening and dispelling stain, comedo that have, and moisturizing rate is higher than common facial film 20% left and right, market.
Above-described embodiment is preferably embodiment of the present invention; but embodiments of the present invention are not limited by the examples; other any do not deviate from change, the modification done under spirit of the present invention and principle, substitutes, combination, simplify; all should be equivalent substitute mode, within being included in protection scope of the present invention.
Claims (5)
1. a natural moisture preserving facial film, is characterized in that, according to weighing scale, comprises pollen extracting liquid 10-20 part, Radix Angelicae Dahuricae extracting solution 10-15 part, sodium alginate 5-10, glycerol 5-10 part, citric acid 1-5 part, moisturizing oligo-chitosan 0.5-1 part, deionized water 40-70 part.
2. a preparation method for natural moisture preserving facial film, is characterized in that, comprises the following steps:
(1) according to weighing scale, by sodium alginate sodium alginate 5-10, glycerol 5-10 part, citric acid 1-5 part, moisturizing oligo-chitosan 0.5-1 part, deionized water 40-70 part is mixed, and is heated to 60-80 ℃, obtains basal liquid;
(2), according to weighing scale, by pollen extracting liquid 10-20 part, Radix Angelicae Dahuricae extracting solution 10-15 part adds in described basal liquid, obtains facial film solution;
(3) opposite coating solution carries out emulsifying operation, rotating speed 1000-12000r/min, and time 1-2h obtains facial film emulsion, is moisture saver mask.
3. the preparation method of natural moisture preserving facial film according to claim 2, is characterized in that, the preparation process of described pollen extracting liquid is as follows:
Choose pollen (processed by breaking wall) dry, remove impurity, carry out ultrasonic assisted extraction, obtain preliminary pollen extracting liquid; Adopt active carbon to decolour, take off taste to the preliminary pollen extracting liquid extracting and process, then pass through centrifugally operated, obtain pollen extracting liquid;
Described ultrasonic assisted extraction is specially: the weight ratio of pollen (processed by breaking wall) and water is 1:10-20, carries out ultrasonic Treatment in the time of extraction; Extraction time is 10-30min, and extraction temperature is 40-60 ℃, and ultrasonic power is 400W-800W.
4. the preparation method of natural moisture preserving facial film according to claim 2, is characterized in that, the preparation method of described Radix Angelicae Dahuricae extracting solution is as follows:
The Radix Angelicae Dahuricae powder that choose dry, remove impurity, pulverizes and sieves, carries out ultrasonic assisted extraction; Obtain preliminary Radix Angelicae Dahuricae extracting solution, adopt active carbon to decolour, take off taste to preliminary Radix Angelicae Dahuricae extracting solution and process, then pass through centrifugally operated, obtain Radix Angelicae Dahuricae extracting solution;
Described ultrasonic assisted extraction is specially: the weight ratio of Radix Angelicae Dahuricae powder and water is 1:10-20, carries out ultrasonic Treatment in the time of extraction; Extraction time is 10-30min, and extraction temperature is 40-60 ℃, and ultrasonic power is 400W-800W.
5. the preparation method of natural moisture preserving facial film according to claim 2, is characterized in that, the preparation method of described moisturizing oligo-chitosan is as follows:
In the chitosan solution that is 1%-5% to mass concentration, adding mass concentration is 30% hydrogen peroxide solution, obtains mixed liquor; Make the mass concentration of hydrogen peroxide in mixed liquor reach 1%-2%; After stirring at room 10-20min, by liquor pump, mixed liquor is sent into high-voltage pulse electric field device and process, time 30-60min, field intensity 10-20kV/cm, carries out spray drying treatment after being warming up to the 60-80 ℃ of hydrogen peroxide of removing in mixed liquor; Described spray process conditions is: 160 ℃-180 ℃ of inlet temperatures, intake 20-30m
3/ h, feed rate 0.2-0.3L/h, obtains moisturizing oligo-chitosan, and its molecular weight is less than 5000Da.
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| CN201410154947.8A CN103932945A (en) | 2014-04-17 | 2014-04-17 | Natural moisturizing mask and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105662914A (en) * | 2016-03-03 | 2016-06-15 | 中山卡丝生物科技有限公司 | Irritation-reducing blackhead acne extraction liquid and blackhead acne extraction film |
| CN106387796A (en) * | 2016-08-30 | 2017-02-15 | 湖北赛纯生物技术有限公司 | Pollen nutrition composition, pollen mask and preparation methods thereof |
| CN107951732A (en) * | 2017-12-26 | 2018-04-24 | 湖南御家化妆品制造有限公司 | Rectorite tearing slurry mask |
| CN110693772A (en) * | 2019-11-12 | 2020-01-17 | 烟台新时代健康产业日化有限公司 | Preparation method of seaweed anti-inflammatory extract applied to cosmetics |
| CN114869811A (en) * | 2021-04-02 | 2022-08-09 | 宿州学院 | Rape bee pollen mask, preparation method and application |
-
2014
- 2014-04-17 CN CN201410154947.8A patent/CN103932945A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105662914A (en) * | 2016-03-03 | 2016-06-15 | 中山卡丝生物科技有限公司 | Irritation-reducing blackhead acne extraction liquid and blackhead acne extraction film |
| CN105662914B (en) * | 2016-03-03 | 2018-04-17 | 中山卡丝生物科技有限公司 | It is a kind of to drop the blackhead export liquid stimulated and blackhead export film |
| CN106387796A (en) * | 2016-08-30 | 2017-02-15 | 湖北赛纯生物技术有限公司 | Pollen nutrition composition, pollen mask and preparation methods thereof |
| CN107951732A (en) * | 2017-12-26 | 2018-04-24 | 湖南御家化妆品制造有限公司 | Rectorite tearing slurry mask |
| CN107951732B (en) * | 2017-12-26 | 2020-10-30 | 湖南御家化妆品制造有限公司 | Rectorite tearing slurry mask |
| CN110693772A (en) * | 2019-11-12 | 2020-01-17 | 烟台新时代健康产业日化有限公司 | Preparation method of seaweed anti-inflammatory extract applied to cosmetics |
| CN110693772B (en) * | 2019-11-12 | 2021-11-23 | 烟台新时代健康产业日化有限公司 | Preparation method of seaweed anti-inflammatory extract applied to cosmetics |
| CN114869811A (en) * | 2021-04-02 | 2022-08-09 | 宿州学院 | Rape bee pollen mask, preparation method and application |
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Application publication date: 20140723 |