CN103892441A - Tobacco stem soaking water recycling method - Google Patents
Tobacco stem soaking water recycling method Download PDFInfo
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- CN103892441A CN103892441A CN201410115534.9A CN201410115534A CN103892441A CN 103892441 A CN103892441 A CN 103892441A CN 201410115534 A CN201410115534 A CN 201410115534A CN 103892441 A CN103892441 A CN 103892441A
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- soaking water
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Abstract
The invention belongs to the technical field of tobacco production and particularly relates to a tobacco stem soaking water recycling method. The method includes: preprocessing discarded stem soaking water in existing tobacco production, and spraying to 2-4w% of the preprocessed water to stem shreds or leaves to replace existing water used in the stem dampening, leaf dampening or feeding process. The stem soaking water contains various fragrant matters such as nicotine, organic acids, aldoketones, esters and alcohols and. The stem soaking water is directly applied to the dampening or feeding process of the cigarette technique innovatively; the requirements for resource saving and environment protection are met; cost on sewage treatment is greatly saved. The method is simple to operate, regulating cigarette process equipment is not required, no burden is caused to the existing cigarette production process, smoking quality of cigarettes can be significantly improved, operability is high, and application value and economic and social values are significant.
Description
Technical field
The invention belongs to tobacco production technical field, be specifically related to one grow tobacco soak stalk water the method that is recycled.
Background technology
Soaking stalk is a kind of process in cigarette industry stem process processed, and the method is to carry out seasoning in being transported to peduncle-storing cabinet again after washing is soaked approximately 50 seconds in the hot water of 60 degree left and right by dry thick and stiff offal, makes offal obtain washing by soaking, imbibition.Offal moisture content, pliability, resistance to additivity after washing are enhanced.Soaking stalk water is exactly the hot water in the tank for embathing offal.
At present, in production of cigarettes process, generally will soak stalk water and be classified as production waste, and need in addition purified treatment could discard afterwards.Taking 8 production of cigarettes factories of Henan Zhong Yan group as example, every day, stalk water generates amount was only soaked with regard to approximately 2 tons by each factory, had both wasted a large amount of freshwater resources, paid again high sewage disposal expense simultaneously.
Owing to containing a large amount of, diverse chemical substance in offal, soak stalk water by immersion, washing to offal, make to wash in stalk water and contained a large amount of offal extracts, generally speaking, nicotine content is wherein higher, and these materials origin fragrance matter of tobacco just, if directly abandoned, easily cause the waste of a large amount of tobacco flavor resources, thereby the recycling of soaking stalk water about tobacco, there is at present the research work in some early stages, but the not yet simple comparatively ripe technique report that is directly used in production of cigarettes.
Summary of the invention
The object of the invention is to provide one to grow tobacco and soak the recoverying and utilizing method of stalk water, thereby can realize the cycle saving utilization of resource.
The technical solution adopted in the present invention is as follows:
One grows tobacco soaks the recoverying and utilizing method that obstructs water, comprises the following steps:
(1) by the discarded stalk water that soaks, leave standstill cooling, filtration treatment;
(2) in step 1, soaking after filtration obstructed water by 2 ~ 4% mass ratioes, substitutes existing water be applied in stem or blade at stem moisture regain, blade moisture regain or charging process.
Described in step (1), soaking stalk water is waste water after flue-cured tobacco offal soaks 50s in 60 DEG C of hot water.
Contain the multiple fragrance materials such as nicotine, organic acid, aldoketones, ester alcohols owing to soaking in stalk water; the present invention creatively proposes to be applied directly in the moisture regain or charging process of cigarette process soaking stalk water; both met economize on resources, the requirement of protection of the environment, saved a large amount of sewage disposal expenses simultaneously.The present invention is simple to operate, do not need cigarette process equipment to adjust, can not produce burden to existing cigarette producing process yet, and can obviously promote the sucking quality of cigarette, there is stronger operability, thereby there are comparatively significantly using value and economic and social benefits.
Detailed description of the invention
Below in conjunction with specific embodiment the present invention will be further explained explanation.
embodiment 1
For checking actual augmentation effect of the present invention, first inventor has done analyzing and testing to the fragrance matter chemical composition of soaking stalk water, the described stalk water that soaks is the waste water producing after fire-cured tobacco type offal soaks 50s in 60 DEG C of hot water in producing, the program detecting and concise and to the point process are: take 20mL and soak stalk water in 100mL separatory funnel, add 15mL × 3 carrene to extract, merge organic phase, filter after adding anhydrous sodium sulfate drying, be concentrated into 1mL, carry out GC/MS analysis.
Analysis condition is: GC condition, chromatographic column, DP-5MS (m) capillary column of 50 mm × 0.25, m × 0.32 μ; Injector temperature, 250 DEG C; Carrier gas, helium, flow 1 ml/min(constant current mode); Sample size, 1 μ l, temperature programming, 50 DEG C (1 min), 4 DEG C/min, 160 DEG C (5 min), 4 DEG C/min, 260 DEG C (10 min); Split ratio 10: 1.Solvent delay 5 min; Interface temperature, 280 DEG C; Ionization mode, EI; Ionizing energy, 70 eV; Ion source temperature, 230 DEG C; Quadrupole rod temperature, 150 DEG C; Mass scanning scope, 35～350 amu.
Concrete testing result is as following table:
soak fragrance matter chemical composition in stalk water
embodiment 2
Based on to soaking the analysis of stalk Hydrochemical Composition, obstruct water as example taking soaking of fragrance matter chemical composition in the same manner as in Example 1, the recoverying and utilizing method that inventor soaks stalk water to tobacco has done further experimental check.
Detailed process is as follows:
Fire-cured tobacco type offal is soaked in 60 DEG C of hot water and after 50s, soak stalk water, standing cooling, after filtration treatment, respectively according to the ratio of 2wt%, 3wt%, 4wt%, substituting existing water at charging process is applied in fire-cured tobacco type tobacco leaf, apply at charging process, described tobacco leaf is that (because lower tobacco leaf perfume quantity is less, the fragrance matter including is less for lower tobacco leaf, thereby effect is comparatively obvious), make three groups of samples, taking un-added as control sample, throwing rolls into cigarette after drying respectively.
Cigarette, at the climatic chamber inner equilibrium moisture 48h of temperature (20 ± 1) DEG C, relative humidity (60 ± 2) %, is carried out sense organ evaluation and test, and evaluation result sees the following form.
Upper table shows, adds and soaks after stalk water, can obviously improve cigarette flavor matter, increase flue gas perfume quantity, improve flue gas concentration and strength, and along with soaking the increase of stalk water addition, cigarette perfume quantity, plumpness, concentration increase obviously, wherein best with 4% addition effect.
The present invention by soak stalk Hydrochemical Composition detection; find wherein to contain the multiple fragrance materials such as nicotine, organic acid, aldoketones, ester alcohols; in line with economizing on resources, the principle of protection of the environment; creatively propose to be applied directly in the moisture regain or charging process of cigarette process soaking stalk water; not only reduce sewage discharge, and saved a large amount of sewage disposal expenses.The present invention is simple to operate, do not need cigarette process equipment to adjust, can not produce burden to existing cigarette producing process yet, and can obviously promote the sucking quality of cigarette, there is stronger operability, thereby there are comparatively significantly using value and economic and social benefits.
Claims (2)
- One grow tobacco soak stalk water recoverying and utilizing method, it is characterized in that, the method comprises the following steps:(1) by the discarded stalk water that soaks, leave standstill cooling, filtration treatment;(2) in step (1), soaking after filtration obstructed water by 2 ~ 4% mass ratioes, substitutes stem moisture regain in prior art, blade moisture regain or charging process water, is applied in stem or blade.
- 2. tobacco is soaked the recoverying and utilizing method that obstructs water as claimed in claim 1, it is characterized in that, described in step (1), soaking stalk water is that flue-cured tobacco offal soaks the waste water after 50s in 60 DEG C of hot water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410115534.9A CN103892441B (en) | 2014-03-26 | 2014-03-26 | A kind of tobacco leaching stalk Water Sproading Application way |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410115534.9A CN103892441B (en) | 2014-03-26 | 2014-03-26 | A kind of tobacco leaching stalk Water Sproading Application way |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103892441A true CN103892441A (en) | 2014-07-02 |
| CN103892441B CN103892441B (en) | 2016-06-01 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410115534.9A Active CN103892441B (en) | 2014-03-26 | 2014-03-26 | A kind of tobacco leaching stalk Water Sproading Application way |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214087A (en) * | 2008-01-22 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Combined cabo processing technique and special-purpose equipment thereof |
| CN101422276A (en) * | 2008-12-04 | 2009-05-06 | 广东省金叶烟草薄片技术开发有限公司 | Method for adjusting and controlling chlorate and nitrate in tobacco extract |
| CN101433368A (en) * | 2008-12-23 | 2009-05-20 | 陕西科技大学 | Method for producing shredded tobacco of cigarette using cabo |
| CN102440433A (en) * | 2011-09-08 | 2012-05-09 | 上海聚华科技股份有限公司 | Method for manufacturing tobacco cut stems |
| CN102475352A (en) * | 2010-11-29 | 2012-05-30 | 武汉市三骐科技有限公司 | Reconstruction processing method of cut stems |
| CN102907760A (en) * | 2012-09-03 | 2013-02-06 | 上海聚华科技股份有限公司 | Method for regulating chemical components of tobacco material |
| CN202774094U (en) * | 2012-09-10 | 2013-03-13 | 上海聚华科技股份有限公司 | Reproduction system of tobacco stems |
| EP2692247A1 (en) * | 2011-03-31 | 2014-02-05 | Japan Tobacco, Inc. | Tobacco material expansion method and device |
-
2014
- 2014-03-26 CN CN201410115534.9A patent/CN103892441B/en active Active
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101214087A (en) * | 2008-01-22 | 2008-07-09 | 红云烟草(集团)有限责任公司 | Combined cabo processing technique and special-purpose equipment thereof |
| CN101422276A (en) * | 2008-12-04 | 2009-05-06 | 广东省金叶烟草薄片技术开发有限公司 | Method for adjusting and controlling chlorate and nitrate in tobacco extract |
| CN101433368A (en) * | 2008-12-23 | 2009-05-20 | 陕西科技大学 | Method for producing shredded tobacco of cigarette using cabo |
| CN102475352A (en) * | 2010-11-29 | 2012-05-30 | 武汉市三骐科技有限公司 | Reconstruction processing method of cut stems |
| EP2692247A1 (en) * | 2011-03-31 | 2014-02-05 | Japan Tobacco, Inc. | Tobacco material expansion method and device |
| CN102440433A (en) * | 2011-09-08 | 2012-05-09 | 上海聚华科技股份有限公司 | Method for manufacturing tobacco cut stems |
| CN102907760A (en) * | 2012-09-03 | 2013-02-06 | 上海聚华科技股份有限公司 | Method for regulating chemical components of tobacco material |
| CN202774094U (en) * | 2012-09-10 | 2013-03-13 | 上海聚华科技股份有限公司 | Reproduction system of tobacco stems |
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| Publication number | Publication date |
|---|---|
| CN103892441B (en) | 2016-06-01 |
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Address after: 450000 Yulin South Road, Henan, Zheng Dong, No. 16 South Road, Zhengzhou Patentee after: China Tobacco Henan Industrial Co., Ltd. Address before: 450000 Zhengzhou agricultural road, Henan, No. 29 Patentee before: China Tobacco Henan Industrial Co., Ltd. |