CN103866564A - Spinning size and preparation method thereof - Google Patents
Spinning size and preparation method thereof Download PDFInfo
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- CN103866564A CN103866564A CN201410135025.2A CN201410135025A CN103866564A CN 103866564 A CN103866564 A CN 103866564A CN 201410135025 A CN201410135025 A CN 201410135025A CN 103866564 A CN103866564 A CN 103866564A
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- size
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Abstract
The invention relates to a spinning size and a preparation method thereof, and belongs to the technical field of chemical metallurgy. The size comprises the following components: 3%-4% of acrylic acid, 2%-6% of butyl acrylate, 9%-15% of acrylamide, 1%-3% of diphenylmethane, 2%-5% of protein amino acid, 12-18% of auxiliaries and the balance being starch. The energy-saving spinning size and the preparation method are characterized in that all the adopted components are low-toxicity and environment-friendly materials, so that the permeability of the size and the bonding property of fabrics are enhanced, the preparation of the major material and the size and the sizing by using the size both are not required to be implemented under a high temperature condition, and the energy consumption is reduced by omitting the steps of size mixing and cooking.
Description
Technical field
The present invention relates to a kind of slurry and preparation method thereof, belong to chemical metallurgy technical field.
Background technology
Current, starching is the important procedure that fabric is produced.Especially producing when thick high density fabric, all take the technique of high frequency time, little opening, hightension, thwack latitude in weaving process, warp thread suffered frictional force, tensile force and bending force repeatedly in weaving process is large especially.The warp thread of cloth is being subject to very large damage, and the starching of having only had could improve the intensity of fabric.
It is main that current slurry generally adopts converted starch to mix slurry with acrylic size, PVA, and major ingredient need rise to temperature more than 95 DEG C and react with auxiliary agent, finally just can obtain slurry.
Summary of the invention
The technical problem that the present invention solves is: propose the spinning sizing agent that a kind of normal temperature can be prepared.
In order to solve the problems of the technologies described above, the first technical scheme that the present invention proposes is: a kind of spinning sizing agent, its composition comprises: acrylic acid 3 %～4%, butyl acrylate 2%～6%, acrylamide 9%～15%, diphenyl-methane 1%～3%, Argine Monohydrochloride 2%～5%, auxiliary agent 12～18%, surplus is starch.
Technique scheme is further improved and is: the percentage by weight of the composition of described auxiliary agent is, chloroacetic acid 3%～6%, potassium hydroxide 3%～8%, and surplus is methyl alcohol.
In order to solve the problems of the technologies described above, the another kind of technical scheme that the present invention proposes is: the preparation method of above-mentioned spinning sizing agent, comprises the steps:
A, prepare burden according to weight ratio: acrylic acid 3 %～4%, butyl acrylate 2%～6%, acrylamide 9%～15%, diphenyl-methane 1%～3%, Argine Monohydrochloride 2%～5%, auxiliary agent 12～18%, surplus is starch; Then starch is water-soluble and fully stirring;
B, acrylic acid, butyl acrylate, acrylamide, diphenyl-methane, Argine Monohydrochloride are added in the starch solution that upper step makes and fully and stirred;
C, auxiliary agent is added in the solution that upper step makes and fully and stirred.
Technique scheme is further improved and is: in described steps A, water temperature is 55 degrees Celsius to 65 degrees Celsius.
A kind of spinning sizing agent provided by the invention and preparation method thereof, the composition adopting is all low toxicity, ep-type material, and make slurry permeability, with fabric adhesive property strengthen; From preparing major ingredient, slurry, recycle this slurry sizing all without hot conditions, by the minimizing process of hotting plate of sizing mixing, reduce energy consumption.
Detailed description of the invention
Embodiment
A kind of spinning sizing agent that the present embodiment provides, its composition comprises: acrylic acid 3 %～4%, butyl acrylate 2%～6%, acrylamide 9%～15%, diphenyl-methane 1%～3%, Argine Monohydrochloride 2%～5%, auxiliary agent 12～18%, surplus is starch.
Wherein the composition percentage by weight of auxiliary agent is, chloroacetic acid 3%～6%, potassium hydroxide 3%～8%, and surplus is methyl alcohol.
The preparation method of the present embodiment comprises the steps:
A, prepare burden according to weight ratio: acrylic acid 3 %～4%, butyl acrylate 2%～6%, acrylamide 9%～15%, diphenyl-methane 1%～3%, Argine Monohydrochloride 2%～5%, auxiliary agent 12～18%, surplus is starch; By water-soluble starch and fully stirring; Water temperature remains on 55 degrees Celsius to 65 degrees Celsius
B, acrylic acid, butyl acrylate, acrylamide, diphenyl-methane, Argine Monohydrochloride are added in the starch solution that upper step makes and fully and stirred;
C, auxiliary agent is added in the solution that upper step makes and fully and stirred.
The concrete technical scheme that is not limited to above-described embodiment of the present invention, the technical scheme that all employings are equal to replacement formation is the protection domain that the present invention requires.
Claims (4)
1. a spinning sizing agent, is characterized in that, its composition comprises by weight: acrylic acid 3 %～4%, and butyl acrylate 2%～6%, acrylamide 9%～15%, diphenyl-methane 1%～3%, Argine Monohydrochloride 2%～5%, auxiliary agent 12～18%, surplus is starch.
2. according to the spinning sizing agent described in claim 1, it is characterized in that, the percentage by weight of the composition of described auxiliary agent is, chloroacetic acid 3%～6%, potassium hydroxide 3%～8%, and surplus is methyl alcohol.
3. the preparation method of spinning sizing agent according to claim 1, comprises the steps:
A, prepare burden according to weight ratio: acrylic acid 3 %～4%, butyl acrylate 2%～6%, acrylamide 9%～15%, diphenyl-methane 1%～3%, Argine Monohydrochloride 2%～5%, auxiliary agent 12～18%, surplus is starch; Then starch is water-soluble and fully stirring;
B, acrylic acid, butyl acrylate, acrylamide, diphenyl-methane, Argine Monohydrochloride are added in the starch solution that upper step makes and fully and stirred;
C, auxiliary agent is added in the solution that upper step makes and fully and stirred.
4. preparation method according to claim 3, is characterized in that: in described steps A, water temperature is 55 degrees Celsius to 65 degrees Celsius.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410135025.2A CN103866564A (en) | 2014-04-04 | 2014-04-04 | Spinning size and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410135025.2A CN103866564A (en) | 2014-04-04 | 2014-04-04 | Spinning size and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103866564A true CN103866564A (en) | 2014-06-18 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410135025.2A Pending CN103866564A (en) | 2014-04-04 | 2014-04-04 | Spinning size and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103866564A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101935951A (en) * | 2010-09-16 | 2011-01-05 | 湖北达雅化工技术发展有限公司 | Textile size combination |
| CN102050925A (en) * | 2009-10-30 | 2011-05-11 | 成都海旺科技有限责任公司 | Grafted modified starch slurry |
| CN103643515A (en) * | 2013-12-30 | 2014-03-19 | 张海峰 | Textile size and preparation method thereof |
-
2014
- 2014-04-04 CN CN201410135025.2A patent/CN103866564A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102050925A (en) * | 2009-10-30 | 2011-05-11 | 成都海旺科技有限责任公司 | Grafted modified starch slurry |
| CN101935951A (en) * | 2010-09-16 | 2011-01-05 | 湖北达雅化工技术发展有限公司 | Textile size combination |
| CN103643515A (en) * | 2013-12-30 | 2014-03-19 | 张海峰 | Textile size and preparation method thereof |
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Application publication date: 20140618 |