CN103865746A - Preparation method of cynomorium songaricum and medlar vinegar - Google Patents

Preparation method of cynomorium songaricum and medlar vinegar Download PDF

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CN103865746A
CN103865746A CN201410055123.5A CN201410055123A CN103865746A CN 103865746 A CN103865746 A CN 103865746A CN 201410055123 A CN201410055123 A CN 201410055123A CN 103865746 A CN103865746 A CN 103865746A
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vinegar
saccharification
temperature
water
cynomorium songaricum
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孙钰家
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Abstract

The invention discloses a preparation method of cynomorium songaricum and medlar vinegar, belonging to the field of non-staple food processing. The cynomorium songaricum and medlar vinegar comprises the following main materials: 1000-1500 parts of wheat flour, 270-400 parts of corn, 30-60 parts of wheat bran, 65-90 parts of soybean and the balance of water and auxiliary materials including 50-75 parts of cynomorium songaricum, 50-75 parts of medlar, 80-120 parts of table salt, 0.007-0.015 part of acetic bacteria, 0.15-0.5 part of saccharifying enzyme and 0.15-0.5 part of amylase. The preparation method comprises the following processing steps: making a starter, saccharifying, boiling grains, extracting, fermenting, carrying out vinegar infiltration and carrying out vinegar aging. The cynomorium songaricum and medlar vinegar prepared by the preparation method disclosed by the invention has the efficacies of tonifying liver and kidney, relaxing bowels, improving the immunity and delaying senescence.

Description

A kind of cynomorium songaricum medlar vinegar preparation method
Technical field
The present invention relates to a kind of preparation method of vinegar, particularly a kind of cynomorium songaricum medlar vinegar preparation method, belongs to food processing field.
Background technology
Vinegar is the requisite in daily life, is widely used in the aspects such as seasoning, sterilization, medical treatment.Mass-produced vinegar has edible vinegar and beverage vinegar etc. in the market.These beverage vinegars, as cider vinegar, medlar vinegar, onion vinegar etc. only form through zymamsis, acetic fermentation with certain raw material, as beverage, though given prominence to mouthfeel, cause the nutritive ingredient of vinegar single, function reduction.And edible vinegar aspect nutrition and health care aspect be all better than beverage vinegar.The present invention cereal is combined with the Chinese medicine of the integration of drinking and medicinal herbs such as cynomorium songaricum, matrimony vine produce cynomorium songaricum medlar vinegar, not only utilize to greatest extent the various nutritive ingredients in cereal, bring into play the function itself having, and because the utilization of cynomorium songaricum, matrimony vine has increased nourishing function, as tonify the liver and kidney, relax bowel, improve immunizing power, delay senility etc.Record the pharmacological action of cynomorium songaricum: the 1. impact on immunity and sexual function according to " Chinese herbal cynomorium songaricum ".Cynomorium songaricum all has regulating effect for body non-specific immune function and cellular immune function, and it acts under immune suppressed state particularly evident: humoral immune function is also had to enhancement, and have the maturing of the animality of promotion.2. the impact on intestinal function.Cynomorium songaricum solution is the excited intestinal tube of energy under finite concentration, increases intestinal peristalsis, has the effect relaxing bowel.The traditional Chinese medical science thinks, cynomorium songaricum has effect of kidney invigorating and YANG supporting, beneficial intestines defaecation, main impotence due to deficiency of the kidney; Seminal emission premature ejaculation; Flaccidity and weakness of the lower limbs; Empty people's constipation.Matrimony vine is a kind of nutritious fruit, contain the nutritive ingredients such as betaine, polysaccharide, crude fat, crude protein, carotene, vitamin A, vitamins C, VITMAIN B1, Lin Suanna Vitamin B2 Sodium Phosphate and calcium, phosphorus, iron, zinc, manganese, linolic acid, hemopoietic function is had to promoter action, can also be anti-ageing, anti-mutation, antitumor, anti-fatty liveranti-fatty liver and the effect such as hypoglycemic.Matrimony vine is famous and precious medicinal material and invigorant, and the traditional Chinese medical science has the saying of " medlar health preserving " very early.Pharmaceutical use and the health-care effect of research in the past to cynomorium songaricum, matrimony vine do not give due attention, and the present invention can widen the purposes of cynomorium songaricum, matrimony vine, enriches the kind of edible vinegar, makes up cynomorium songaricum not yet for this blank of production of vinegar.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of cynomorium songaricum medlar vinegar preparation method.For achieving the above object, a kind of cynomorium songaricum medlar vinegar preparation method of the present invention, realizes by following steps: comprise koji, saccharification, boil paddy, extraction, ferment, ooze vinegar, heavy vinegar.Concrete steps and method are: (1) is by the water of the wheat bran of the wheat-flour of 40--60 part, 30--40 part and 12--15 part, add edible starter, bent material is 30--40:1 with edible starter weight ratio, stir, put into jar fermenter, encase with wet cloth, temperature is controlled at the koji 5-7 days that ferments between 35-40 ℃.(2) by corn 300--350 part, soybean 50--70 part is ground into coarse particles, adds water afterwards while burning to 85-95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stirs, and boils 50 minutes, until boil, the weight ratio of water and material is 1--5:1.(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 35-40 ℃ of hot water of 400--600 part to stir evenly into saccharification slurry.(4) material the 2nd step being boiled is in the time that temperature drops to 35-38 ℃, admix 0.2-0.45 part, saccharifying enzyme, 0.15-0.3 part of amylase, the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 35--38 ℃ and carries out the saccharification of 6 days, obtains saccharification song after maturation.(5) 60--70 part cynomorium songaricum and 50--75 part matrimony vine are rinsed well, add water, the weight ratio of water and raw material is 10--15:1, after smashing, be warming up to 33-38 ℃, add the complex enzyme zymohydrolysis 3-5 hour being made up of by 1--5:1--5 weight ratio polygalacturonase and cellulase, prozyme consumption is 80-150mL/t.Be warming up to again 90-100 ℃ of decoction, time 1-1.5 hour.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1200--1400 part wheat-flour, after mixing with the saccharification song after saccharification maturation, 70--100 part salt, 0.001-0.015 part of acetic bacteria, put into jar fermenter and make real gently, temperature is controlled between 31-40 degree, fermentation 10-15 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 31-40 ℃, in the time that temperature is high, stirs, and makes it be cooled to 31-40 ℃, guarantees that fermentation evenly.(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:2--5, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
Described a kind of cynomorium songaricum medlar vinegar preparation method, realizes by following steps: comprise koji, boil paddy, mixing, saccharification, extraction, ferment, ooze vinegar, heavy vinegar.Concrete steps and method are: (1) is by the water of the wheat bran of the wheat-flour of 40--60 part, 30--40 part and 12--15 part, add edible starter, bent material is 30--40:1 with edible starter weight ratio, stir, put into jar fermenter, encase with wet cloth, temperature is controlled at the koji 5-7 days that ferments between 35-40 ℃.(2) by corn 300--350 part, soybean 50--70 part is ground into coarse particles, adds water afterwards while burning to 85-95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stirs, and boils 50 minutes, until boil, the weight ratio of water and material is 1--5:1.(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 35-40 ℃ of hot water of 400--600 part to stir evenly into saccharification slurry.(4) material the 2nd step being boiled is in the time that temperature drops to 35-38 ℃, admix 0.2-0.45 part, saccharifying enzyme, 0.15-0.3 part of amylase, the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 35--38 ℃ and carries out the saccharification of 6 days, obtains saccharification song after maturation.(5) 60--70 part cynomorium songaricum and 50--75 part matrimony vine are rinsed well, add water, the weight ratio of water and raw material is 10--15:1, after smashing, be warming up to 33-38 ℃, add the complex enzyme zymohydrolysis 3-5 hour being made up of by 1--5:1--5 weight ratio polygalacturonase and cellulase, prozyme consumption is 80-150mL/t.Be warming up to again 90-100 ℃ of decoction, time 1-1.5 hour.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1200--1400 part wheat-flour, after mixing with the saccharification song after saccharification maturation, 70--100 part salt, 0.001-0.015 part of acetic bacteria, put into jar fermenter and make real gently, temperature is controlled between 31-40 degree, fermentation 10-15 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 31-40 ℃, in the time that temperature is high, stirs, and makes it be cooled to 31-40 ℃, guarantees that fermentation evenly.(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:2--5, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
Described a kind of cynomorium songaricum medlar vinegar preparation method, realizes by following steps: comprise koji, boil paddy, mixing, saccharification, extraction, ferment, ooze vinegar, heavy vinegar.Concrete steps and method are: (1) is by the water of the wheat bran of the wheat-flour of 40--50 part, 50--60 part and 10--15 part, add edible starter, bent material is 10--20:1 with edible starter weight ratio, stir, put into jar fermenter, encase with wet cloth, temperature is controlled at the koji 5 days of fermenting between 35--40 ℃.(2) by corn 300--380 part, soybean 65--85 part is ground into coarse particles, adds water afterwards while burning to 85-95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stirs, and boils 60 minutes, until boil, the weight ratio of water and material is 2--4:1.(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 600--1000 part 35-40 degree hot water to stir evenly into saccharification slurry.(4) material the 2nd step being boiled, in the time that temperature drops to 35-38 ℃, is admixed 0.2-0.4 part, saccharifying enzyme, 0.2-0.5 part of amylase, and the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 35-38 ℃ and carries out the saccharification of 5 days, obtains saccharification song after maturation.(5) 55--65 part cynomorium songaricum and 50--70 part matrimony vine are rinsed well, add water, the weight ratio of water and raw material is 15--30:1, after smashing, be warming up to 33-38 ℃, add the complex enzyme zymohydrolysis 3-5 hour being made up of by 2--5:1 weight ratio polygalacturonase and cellulase, prozyme consumption is 80-150mL/t.Be warming up to again 90-100 ℃ of decoction, time 1-2 hour.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1100--1500 part wheat-flour, after mixing with the saccharification song after saccharification maturation, 100--120 part salt, 0.009-0.013 part of acetic bacteria, put into jar fermenter and make real gently, temperature is controlled between 31-40 ℃, ferments 10 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 31-40 ℃, in the time that temperature is high, stirs, and makes it be cooled to 31-40 ℃, guarantees that fermentation evenly.(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:3-5, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
The property of medicine below in conjunction with combined composition further illustrates.
Cynomorium songaricum, beneficial able-bodied sun, moisturizes laxation, nourishing the muscle and tendon.Function: kidney invigorating and YANG supporting controlling nocturnal emission with astringent drugs, ease constipation, strong waist knee.Cure mainly: impotence and premature ejaculation, blood depletion constipation, a little less than the thin impotence of waist, the diseases such as infertilitas feminis.
Wolfberry fruit, nourishing the liver; Nourshing kidney; Moistening lung.Main caused by liver and kidney deficiency; Have a dizzy spell; Soreness of the waist and knees; The expensive essence of impotence; Cough due to consumptive disease; Quench one's thirst and draw drink.Lose for consumptive disease essence, soreness of waist and knee joint, dizzy tinnitus, interior heat is quenched one's thirst, and the deficiency of blood is sallow, and blurred vision is not clear.
The present invention compared with prior art has the following advantages:
It is 15 main seed amino acids that the high acid environment of the cynomorium songaricum medlar vinegar that the present invention makes can make anthocyanin, triterpenoid saponin and aspartic acid in cynomorium songaricum, proline(Pro), Serine etc., anthocyanogen in matrimony vine, organic acid, VITAMIN, VC isoreactivity composition are preserved to greatest extent, thereby its inherent composition, nourishing function are played a role easily in daily diet.
The present invention is by cynomorium songaricum, matrimony vine reasonable compatibility, and product has certain effect that tonifies the liver and kidney, relaxes bowel, improves immunizing power, delays senility, and its taste is slightly micro-sweet, and mouthfeel is soft, is better than general edible vinegar.
Product price of the present invention is cheap, easy to use, can escort to enduringly people's health.
Preparation process of the present invention is simple and easy to do, and production cost is low, stable and controllable for quality, is easy to realize mechanized operation, can meet suitability for industrialized production demand.
Embodiment
Embodiment 1
A kind of cynomorium songaricum medlar vinegar preparation method, is made by following proportioning raw materials and step:
(1) by the wheat-flour of 30 parts, the wheat bran of 40 parts and the water of 10 parts, add edible starter, bent material is 30:1 with edible starter weight ratio, stirs, and puts into jar fermenter, encases with wet cloth, and temperature is controlled at 35 ℃ of kojis 5 days of fermenting.
(2) by 270 parts of corns, 65 parts of soybean are ground into coarse particles, add water afterwards while burning to 85 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stir, and boil 40 minutes, until boil, the weight ratio of water and material is 2:1.
(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 500 parts of 35 ℃ of hot water to stir evenly into saccharification slurry.
(4) material the 2nd step being boiled, in the time that temperature drops to 35 ℃, is admixed 0.2 part, saccharifying enzyme, 0.15 part of amylase, and the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 35 ℃ and carries out the saccharification of 6 days, obtains saccharification song after maturation.
(5) 50 parts of cynomorium songaricums and 50 portions of matrimony vines are rinsed well, added water, the weight ratio of water and raw material is 15:1, is warming up to 33 ℃ after smashing, and adds the complex enzyme zymohydrolysis that is made up of by 3:1 weight ratio polygalacturonase and cellulase 5 hours, and prozyme consumption is 80mL/t.Be warming up to again 90-100 ℃ of decoction, 1 hour time.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.
(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1000 portions of wheat-flours, after mixing with the saccharification song after saccharification maturation, 80 portions of salt, 0.007 part of acetic bacteria, to put into jar fermenter and make real gently, temperature is controlled at 33 ℃, ferments 10 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 31-36 ℃, in the time that temperature is high, stirs, and makes it be cooled to 32 ℃, guarantees that fermentation evenly.
(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:1.5, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.
(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
Embodiment 2
A kind of cynomorium songaricum medlar vinegar preparation method, is made by following proportioning raw materials and step:
(1) by the wheat-flour of 40 parts, the wheat bran of 50 parts and the water of 15 parts, add edible starter, bent material is 25:1 with edible starter weight ratio, stirs, and puts into jar fermenter, encases with wet cloth, and temperature is controlled at 36 ℃ of kojis 7 days of fermenting.
(2) by 350 parts of corns, 80 parts of soybean are ground into coarse particles, add water afterwards while burning to 88 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stir, and boil 50 minutes, until boil, the weight ratio of water and material is 4:1.
(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 700 parts of 38 ℃ of hot water to stir evenly into saccharification slurry.
(4) material the 2nd step being boiled drops to 36 while spending in temperature, admixes 0.5 part, saccharifying enzyme, 0.5 part of amylase, and the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at the saccharification that 35 degree carry out 6 days, after maturation saccharification song.
(5) 60 parts of cynomorium songaricums and 60 portions of matrimony vines are rinsed well, added water, the weight ratio of water and raw material is 20:1, is warming up to 37 ℃ after smashing, and adds the complex enzyme zymohydrolysis that is made up of by 1:1 weight ratio polygalacturonase and cellulase 3 hours, and prozyme consumption is 110mL/t.Be warming up to again 90 ℃ of decoctions, time 2 h.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.
(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1300 portions of wheat-flours, after mixing with the saccharification song after saccharification maturation, 100 portions of salt, 0.012 part of acetic bacteria, to put into jar fermenter and make real gently, temperature is controlled at 36 ℃, ferments 10 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 34-37 ℃, in the time that temperature is high, stirs, and makes it be cooled to 35 ℃, guarantees that fermentation evenly.
(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:3, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.
(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
Embodiment 3
A kind of cynomorium songaricum medlar vinegar preparation method, is made by following proportioning raw materials and step:
(1) by the wheat-flour of 40 parts, the wheat bran of 30 parts and the water of 12 parts, add edible starter, bent material is 40:1 with edible starter weight ratio, stirs, and puts into jar fermenter, encases with wet cloth, and temperature is controlled at 40 ℃ of kojis 7 days of fermenting.
(2) by 300 parts of corns, 50 parts of soybean are ground into coarse particles, add water afterwards while burning to 90 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stir, and boil 50 minutes, until boil, the weight ratio of water and material is 1:1.
(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 400 parts of 40 ℃ of hot water to stir evenly into saccharification slurry.
(4) material the 2nd step being boiled, in the time that temperature drops to 38 ℃, is admixed 0.5 part, saccharifying enzyme, 0.3 part of amylase, and the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 8 ℃ and carries out the saccharification of 6 days, obtains saccharification song after maturation.
(5) 70 parts of cynomorium songaricums and 50 portions of matrimony vines are rinsed well, added water, the weight ratio of water and raw material is 12:1, is warming up to 36 ℃ after smashing, and adds the complex enzyme zymohydrolysis that is made up of by 3:1 weight ratio polygalacturonase and cellulase 5 hours, and prozyme consumption is 150mL/t.Be warming up to again 94 ℃ of decoctions, 1.5 hours time.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.
(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1200 portions of wheat-flours, after mixing with the saccharification song after saccharification maturation, 70 portions of salt, 0.001 part of acetic bacteria, to put into jar fermenter and make real gently, temperature is controlled at 40 ℃, ferments 15 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 38 ℃, in the time that temperature is high, stirs, and makes it be cooled to 40 ℃, guarantees that fermentation evenly.
(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:2, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.
(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
Embodiment 4
A kind of cynomorium songaricum medlar vinegar preparation method, is made by following proportioning raw materials and step:
(1) by the wheat-flour of 60 parts, the wheat bran of 40 parts and the water of 10 parts, add edible starter, bent material is 25:1 with edible starter weight ratio, stirs, and puts into jar fermenter, encases with wet cloth, and temperature is controlled at the koji 7 days of fermenting between 38 ℃.
(2) by 350 parts of corns, 60 parts of soybean are ground into coarse particles, add water afterwards while burning to 95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stir, and boil 40 minutes, until boil, the weight ratio of water and material is 3:1.
(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 500 parts of 36 ℃ of hot water to stir evenly into saccharification slurry.
(4) material the 2nd step being boiled, in the time that temperature drops to 35-38 ℃, is admixed 0.3 part, saccharifying enzyme, 0.3 part of amylase, and the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 36 ℃ and carries out the saccharification of 6 days, obtains saccharification song after maturation.
(5) 65 parts of cynomorium songaricums and 60 portions of matrimony vines are rinsed well, add water, the weight ratio of water and raw material is 10:1, is warming up to 34 ℃ after smashing, add the complex enzyme zymohydrolysis that is made up of by 2.5:1 weight ratio polygalacturonase and cellulase 3.5 hours, prozyme consumption is 120mL/t.Be warming up to again 96 ℃ of decoctions, 1.2 hours time.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.
(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1400 portions of wheat-flours, after mixing with the saccharification song after saccharification maturation, 80 portions of salt, 0.01 part of acetic bacteria, to put into jar fermenter and make real gently, temperature is controlled at 36 ℃, ferments 10 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 40 ℃, in the time that temperature is high, stirs, and makes it be cooled to 36 ℃, guarantees that fermentation evenly.
(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:3, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.
(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
Embodiment 5
A kind of cynomorium songaricum medlar vinegar preparation method, is made by following proportioning raw materials and step:
(1) by the wheat-flour of 50 parts, the wheat bran of 50 parts and the water of 15 parts, add edible starter, bent material is 20:1 with edible starter weight ratio, stirs, and puts into jar fermenter, encases with wet cloth, and temperature is controlled at 37 ℃ of kojis 5 days of fermenting.
(2) by 380 parts of corns, 80 parts of soybean are ground into coarse particles, add water afterwards while burning to 85 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stir, and boil 55 minutes, until boil, the weight ratio of water and material is 3:1.
(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 600 parts of 36 ℃ of hot water to stir evenly into saccharification slurry.
(4) material the 2nd step being boiled drops to 37 while spending in temperature, admixes 0.3 part, saccharifying enzyme, 0.2 part of amylase, and the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 38 ℃ and carries out the saccharification of 5 days, after maturation saccharification song.
(5) 50 parts of cynomorium songaricums and 70 portions of matrimony vines are rinsed well, added water, the weight ratio of water and raw material is 15:1, is warming up to 34 ℃ after smashing, and adds the complex enzyme zymohydrolysis that is made up of by 2:1 weight ratio polygalacturonase and cellulase 4 hours, and prozyme consumption is 100mL/t.Be warming up to again 95 ℃ of decoctions, 1.5 hours time.Then mash is left standstill to 2 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.
(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1500 portions of wheat-flours, after mixing with the saccharification song after saccharification maturation, 100 portions of salt, 0.0014 part of acetic bacteria, to put into jar fermenter and make real gently, temperature is controlled at 35 ℃, ferments 10 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 36 ℃, in the time that temperature is high, stirs, and makes it be cooled to 34 ℃, guarantees that fermentation evenly.
(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:3, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.
(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
Embodiment 6
A kind of cynomorium songaricum medlar vinegar preparation method, is made by following proportioning raw materials and step:
(1) by the wheat-flour of 40 parts, the wheat bran of 60 parts and the water of 10 parts, add edible starter, bent material is 15:1 with edible starter weight ratio, stirs, and puts into jar fermenter, encases with wet cloth, and temperature is controlled at 37 ℃ of kojis 5 days of fermenting.
(2) by 300 parts of corns, 70 parts of soybean are ground into coarse particles, add water afterwards while burning to 95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stir, and boil 65 minutes, until boil, the weight ratio of water and material is 4:1.
(3) song material step 1 being fermented is put into saccharification pond, then it is for subsequent use to add 800 parts of 40 ℃ of hot water to stir evenly into saccharification slurry.
(4) material the 2nd step being boiled, in the time that temperature drops to 37 ℃, is admixed 0.4 part, saccharifying enzyme, 0.5 part of amylase, and the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 45 ℃ and carries out the saccharification of 3 days, obtains saccharification song after maturation.
(5) 55 parts of cynomorium songaricums and 50 portions of matrimony vines are rinsed well, added water, the weight ratio of water and raw material is 20:1, is warming up to 38 ℃ after smashing, and adds the complex enzyme zymohydrolysis that is made up of by 4:1 weight ratio polygalacturonase and cellulase 4 hours, and prozyme consumption is 100mL/t.Be warming up to again 100 ℃ of decoctions, time 2 h.Then mash is left standstill to 3 hours, get supernatant liquor and leach, take out oxygen airtight for subsequent use; The dregs of a decoction are for subsequent use.
(6) by the cynomorium songaricum matrimony vine dregs of a decoction and 1400 portions of wheat-flours, after mixing with the saccharification song after saccharification maturation, 110 portions of salt, 0.001 part of acetic bacteria, to put into jar fermenter and make real gently, temperature is controlled at 38 ℃, ferments 10 days.In yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 38 ℃, in the time that temperature is high, stirs, and makes it be cooled to 37 ℃, guarantees that fermentation evenly.
(7) material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:5, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation.
(8) the vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.

Claims (3)

1. a cynomorium songaricum medlar vinegar preparation method, is characterized in that, comprises following proportioning raw materials and step:
By the water of the wheat bran of the wheat-flour of 30--45 part, 40--50 part and 10--15 part, add edible starter, bent material is 20--30:1 with edible starter weight ratio, stir, put into jar fermenter, encase with wet cloth, temperature is controlled at the koji 5-7 days that ferments between 35-40 ℃; By corn 270--400 part, soybean 65--90 part is ground into coarse particles, adds water afterwards while burning to 85-95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stirs, and boils 40-60min, until boil, the weight ratio of water and material is 2--5:1; The song material fermenting is put into saccharification pond, then it is for subsequent use to add 35-40 ℃ of hot water of 500--750 part to stir evenly into saccharification slurry; Corn that the 2nd step is boiled, soybean material are in the time that temperature drops to 35-38 ℃, admix 0.15-0.5 part, saccharifying enzyme, 0.15-0.5 part of amylase, the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 35-38 ℃ and carries out the saccharification of 6-8 days, obtains saccharification song after maturation; 50--75 part cynomorium songaricum and 60--50 part matrimony vine are rinsed well, add water, the weight ratio of water and raw material is 15--20:1, after smashing, is warming up to 33--38 ℃, add the complex enzyme zymohydrolysis 3-5h being formed by 1--3:1--5 weight ratio by polygalacturonase and cellulase, prozyme consumption is 80-150mL/t, then slurries are warming up to 90-100 ℃ of decoction, time 1-1.5h, mash leaves standstill 2h, get supernatant liquor and leach, take out oxygen airtight for subsequent use, the dregs of a decoction are for subsequent use; By the cynomorium songaricum matrimony vine dregs of a decoction and 1000--1500 part wheat-flour, after mixing with the saccharification song after saccharification maturation, 80--120 part salt, 0.007-0.015 part of acetic bacteria, put into jar fermenter and make real gently, temperature is controlled between 31-40 ℃, fermentation 10-15 days, in yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 31-40 ℃, in the time that temperature is high, stir, make it be cooled to 31-40 ℃, guarantee that fermentation evenly; The material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:1.5--3, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation; The vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
2. a cynomorium songaricum medlar vinegar preparation method, is characterized in that, comprises following proportioning raw materials and step:
By the water of the wheat bran of the wheat-flour of 40--60 part, 30--40 part and 12--15 part, add edible starter, bent material is 30--40:1 with edible starter weight ratio, stir, put into jar fermenter, encase with wet cloth, temperature is controlled at the koji 5-7 days that ferments between 35-40 ℃; By corn 300--350 part, soybean 50--70 part is ground into coarse particles, adds water afterwards while burning to 85-95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stirs, and boils 50min, until boil, the weight ratio of water and material is 1--5:1; The song material fermenting is put into saccharification pond, then it is for subsequent use to add 35-40 ℃ of hot water of 400--600 part to stir evenly into saccharification slurry; Corn that the 2nd step is boiled, soybean material are in the time that temperature drops to 35-38 ℃, admix 0.2-0.45 part, saccharifying enzyme, 0.15-0.3 part of amylase, the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 35--38 ℃ and carries out the saccharification of 6 days, obtains saccharification song after maturation; 60--70 part cynomorium songaricum and 50--75 part matrimony vine are rinsed well, add water, the weight ratio of water and raw material is 10--15:1, after smashing, is warming up to 33-38 ℃, add the complex enzyme zymohydrolysis 3-5h being formed by 1--5:1--5 weight ratio by polygalacturonase and cellulase, prozyme consumption is 80-150mL/t, then slurries are warming up to 90-100 ℃ of decoction, time 1-1.5h, mash leaves standstill 2h, get supernatant liquor and leach, take out oxygen airtight for subsequent use, the dregs of a decoction are for subsequent use; By the cynomorium songaricum matrimony vine dregs of a decoction and 1200--1400 part wheat-flour, after mixing with the saccharification song after saccharification maturation, 70--100 part salt, 0.001-0.015 part of acetic bacteria, put into jar fermenter and make real gently, temperature is controlled between 31-40 degree, fermentation 10-15 days, in yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 31-40 ℃, in the time that temperature is high, stir, make it be cooled to 31-40 ℃, guarantee that fermentation evenly; The material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:2--5, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation; The vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
3. a cynomorium songaricum medlar vinegar preparation method, is characterized in that, comprises following proportioning raw materials and step:
By the water of the wheat bran of the wheat-flour of 40--50 part, 50--60 part and 10--15 part, add edible starter, bent material is 10--20:1 with edible starter weight ratio, stir, put into jar fermenter, encase with wet cloth, temperature is controlled at the koji 5 days of fermenting between 35--40 ℃; By corn 300--380 part, soybean 65--85 part is ground into coarse particles, adds water afterwards while burning to 85-95 ℃ in steam cooker, and the corn processing, soybean are put into pot and boil, and constantly stirs, and boils 60min, until boil, the weight ratio of water and material is 2--4:1; The song material fermenting is put into saccharification pond, then it is for subsequent use to add 600--1000 part 35-40 degree hot water to stir evenly into saccharification slurry; Corn that the 2nd step is boiled, soybean material are in the time that temperature drops to 35-38 ℃, admix 0.2-0.4 part, saccharifying enzyme, 0.2-0.5 part of amylase, the saccharification slurry of pouring in saccharification pond and pond is mixed evenly, and temperature is controlled at 35-38 ℃ and carries out the saccharification of 5 days, obtains saccharification song after maturation; 55--65 part cynomorium songaricum and 50--70 part matrimony vine are rinsed well, add water, the weight ratio of water and raw material is 15--30:1, after smashing, is warming up to 33-38 ℃, add the complex enzyme zymohydrolysis 3-5h being formed by 2--5:1 weight ratio by polygalacturonase and cellulase, prozyme consumption is 80-150mL/t, then slurries are warming up to 90-100 ℃ of decoction, time 1-2h, mash leaves standstill 2h, get supernatant liquor and leach, take out oxygen airtight for subsequent use, the dregs of a decoction are for subsequent use; By the cynomorium songaricum matrimony vine dregs of a decoction and 1100--1500 part wheat-flour, after mixing with the saccharification song after saccharification maturation, 100--120 part salt, 0.009-0.013 part of acetic bacteria, put into jar fermenter and make real gently, temperature is controlled between 31-40 ℃, ferment 10 days, in yeast phase, the moment is observed the temperature of fermented product in jar fermenter, and fermented product temperature is controlled at 31-40 ℃, in the time that temperature is high, stir, make it be cooled to 31-40 ℃, guarantee that fermentation evenly; The material fermenting is taken out in jar fermenter, pack into and ooze in vinegar cylinder, cynomorium songaricum matrimony vine supernatant liquor that step 5 is made is boiled is cooled to 15 ℃ naturally afterwards, add and infiltrate in vinegar cylinder, the weight ratio of material and water is 1:3-5, starts to ooze vinegar, ooze vinegar 2-3 days, obtain the vinegar liquid of diacolation; The vinegar liquid of diacolation is put into pretipitatin jar and precipitate 2-3 days, disgorging, obtains cynomorium songaricum medlar vinegar.
CN201410055123.5A 2014-02-19 2014-02-19 Preparation method of cynomorium songaricum and medlar vinegar Pending CN103865746A (en)

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Application publication date: 20140618