CN103865184B - A kind of insulated cable material and preparation method thereof - Google Patents
A kind of insulated cable material and preparation method thereof Download PDFInfo
- Publication number
- CN103865184B CN103865184B CN201410117887.2A CN201410117887A CN103865184B CN 103865184 B CN103865184 B CN 103865184B CN 201410117887 A CN201410117887 A CN 201410117887A CN 103865184 B CN103865184 B CN 103865184B
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- zinc
- powder
- hour
- insulated cable
- zinc oxide
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- 239000000463 material Substances 0.000 title claims abstract description 26
- 238000002360 preparation method Methods 0.000 title claims description 7
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims abstract description 26
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims abstract description 14
- ZFOZVQLOBQUTQQ-UHFFFAOYSA-N Tributyl citrate Chemical compound CCCCOC(=O)CC(O)(C(=O)OCCCC)CC(=O)OCCCC ZFOZVQLOBQUTQQ-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 13
- 239000011787 zinc oxide Substances 0.000 claims abstract description 13
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 10
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 8
- 239000004709 Chlorinated polyethylene Substances 0.000 claims abstract description 8
- 239000004609 Impact Modifier Substances 0.000 claims abstract description 7
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 7
- -1 carbon alcohols ester Chemical class 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 7
- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 claims abstract description 7
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 claims abstract description 7
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims abstract description 4
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 4
- 239000000843 powder Substances 0.000 claims description 12
- 238000005469 granulation Methods 0.000 claims description 9
- 230000003179 granulation Effects 0.000 claims description 9
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 7
- LJRSZGKUUZPHEB-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxypropoxy)propoxy]propyl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COC(C)COC(=O)C=C LJRSZGKUUZPHEB-UHFFFAOYSA-N 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 claims description 3
- 241000628997 Flos Species 0.000 claims description 3
- 244000223014 Syzygium aromaticum Species 0.000 claims description 3
- 235000016639 Syzygium aromaticum Nutrition 0.000 claims description 3
- WHMDKBIGKVEYHS-IYEMJOQQSA-L Zinc gluconate Chemical compound [Zn+2].OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C([O-])=O WHMDKBIGKVEYHS-IYEMJOQQSA-L 0.000 claims description 3
- 238000001354 calcination Methods 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 239000010977 jade Substances 0.000 claims description 3
- 238000002844 melting Methods 0.000 claims description 3
- 230000008018 melting Effects 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000011670 zinc gluconate Substances 0.000 claims description 3
- 229960000306 zinc gluconate Drugs 0.000 claims description 3
- 235000011478 zinc gluconate Nutrition 0.000 claims description 3
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 abstract description 4
- 239000003063 flame retardant Substances 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 230000000694 effects Effects 0.000 abstract description 3
- 239000004800 polyvinyl chloride Substances 0.000 description 4
- 229920006235 chlorinated polyethylene elastomer Polymers 0.000 description 3
- 229920000915 polyvinyl chloride Polymers 0.000 description 3
- 101000831616 Homo sapiens Protachykinin-1 Proteins 0.000 description 2
- 102100024304 Protachykinin-1 Human genes 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 229910052793 cadmium Inorganic materials 0.000 description 1
- BDOSMKKIYDKNTQ-UHFFFAOYSA-N cadmium atom Chemical compound [Cd] BDOSMKKIYDKNTQ-UHFFFAOYSA-N 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 230000003245 working effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/26—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers modified by chemical after-treatment
- C08L23/28—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers modified by chemical after-treatment by reaction with halogens or compounds containing halogen
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/44—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes vinyl resins; acrylic resins
- H01B3/441—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes vinyl resins; acrylic resins from alkenes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/20—Applications use in electrical or conductive gadgets
- C08L2203/202—Applications use in electrical or conductive gadgets use in electrical wires or wirecoating
Landscapes
- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Organic Insulating Materials (AREA)
- Insulated Conductors (AREA)
Abstract
The invention discloses a kind of insulated cable material, it is characterized in that, be made up of the raw material of following weight part: chlorinatedpolyethylene 55-60, zinc borate 4-5, tributyl citrate 14-16, zinc oxide 2-3, two ten four carbon alcohols ester 3-5, Zinc Stearate 3-4, morpholine 1-2, ACR impact modifier 1-2, vinylbenzene 12-15, light calcium carbonate 15-20, wilkinite 12-15, linking agent TAC1-2, auxiliary agent 6-8; The tensile strength of insulated cable material of the present invention is high, and have good flame retardant effect, production cost also reduces, and can save a large amount of production costs.
Description
Technical field
The present invention relates to polymeric material field, particularly a kind of insulated cable material and preparation method thereof.
Background technology
Along with Economic development, the popularity of electrical equipment is more and more higher, and the usage quantity of wire is also increasing.Current wire insulation layer material mainly based on polyvinyl chloride (PVC), and adds corresponding auxiliary agent and makes.But because the thermotolerance of polyvinyl chloride, flame retardant resistance and ageing resistance are all poor, thus the work-ing life of wire is shorter, and security and reliability are all poor.And polyvinyl chloride needs to add leaded, barium, cadmium auxiliary agent in the course of processing, these auxiliary agents containing toxic heavy metal element can dissolve, to environment after wire uses for a long time.In addition, the wire that polyvinyl chloride is made can give off poisonous gas hydrogenchloride in combustion, the health of harm people.Chlorinated polyethylene rubber (CPE) is applied at wire, cable industry on a large scale as a kind of material of good cost performance in recent years, owing at chlorinated polyethylene rubber being the chlorine-containing polymer a kind of main chain not having double bond, so it has excellent chemical stability, ageing resistance, flame retardant resistance and oil-proofness are all better.
Summary of the invention
The object of this invention is to provide a kind of insulated cable material and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of insulated cable material, is made up of the raw material of following weight part: chlorinatedpolyethylene 55-60, zinc borate 4-5, tributyl citrate 14-16, zinc oxide 2-3, two ten four carbon alcohols ester 3-5, Zinc Stearate 3-4, morpholine 1-2, ACR impact modifier 1-2, vinylbenzene 12-15, light calcium carbonate 15-20, wilkinite 12-15, linking agent TAC1-2, auxiliary agent 6-8;
Described auxiliary agent is made up of the raw material of following weight part: diatomite 10-12, tri (propylene glycol) diacrylate 2-3, zinc oxide 5-6, jade powder 4-5,3-aminopropyl trimethoxysilane 2-3, linking agent TAC1-2, Zinc Gluconate 1-2, Zinic stearas 1-2, magnesium nitrate 7-9, Syzygium aromaticum stem oil 1-2, Flos Rosae Rugosae quintessence oil 0.1-0.2; Diatomite in powder is sent in calcining furnace to calcine 3-4 hour at 700-730 DEG C by preparation method, take out, send in 10-15% hydrochloric acid and soak 1-2 hour, filter to obtain filter residue, wash with clear water, dry, be ground into 200-250 order powder, then the powder of drying is mixed with tri (propylene glycol) diacrylate, zinc oxide, linking agent TAC, grinding 1-2 hour, add other remaining component again, mixed grinding 1-2 hour, to obtain final product.
Insulated cable material of the present invention, be made up of following concrete steps:
(1) chlorinatedpolyethylene is heated to molten state, add zinc borate, tributyl citrate, zinc oxide, two ten four carbon alcohols esters, Zinc Stearate, morpholine, ACR impact modifier, auxiliary agent, stir and mediate 15-25 minute, send into twin screw extruder granulation, obtain A material;
(2) by all the other remaining components heating mixed melting, stir 7-10 minute, send on twin screw extruder and melt extrude granulation, obtain B material;
(3), after A, B material being mixed, melt extrude granulation on the twin screw extruder, to obtain final product.
Excellent effect of the present invention is: the tensile strength of insulated cable material of the present invention is high, and have good flame retardant effect, production cost also reduces, and can save a large amount of production costs.
Embodiment
Below by specific examples, the present invention is described in detail.
A kind of insulated cable material, is made up of the raw material of following weight part (kilogram): chlorinatedpolyethylene 55, zinc borate 4, tributyl citrate 14, zinc oxide 2, two ten four carbon alcohols esters 3, Zinc Stearate 3, morpholine 1, ACR impact modifier 1, vinylbenzene 12, light calcium carbonate 15, wilkinite 12, linking agent TAC1, auxiliary agent 6;
Described auxiliary agent is made up of the raw material of following weight part (kilogram): diatomite 10, tri (propylene glycol) diacrylate 3, zinc oxide 5, jade powder 4,3-aminopropyl trimethoxysilane 2, linking agent TAC2, Zinc Gluconate 1, Zinic stearas 2, magnesium nitrate 9, Syzygium aromaticum stem oil 2, Flos Rosae Rugosae quintessence oil 0.1; Diatomite is sent in calcining furnace to calcine 3-4 hour at 700-730 DEG C by preparation method, take out, send in 10-15% hydrochloric acid and soak 1-2 hour, filter to obtain filter residue, wash with clear water, dry, be ground into 200-250 order powder, then the powder of drying is mixed with tri (propylene glycol) diacrylate, zinc oxide, linking agent TAC, grinding 1-2 hour, add other remaining component again, mixed grinding 1-2 hour, to obtain final product.
Insulated cable material of the present invention, be made up of following concrete steps:
(1) chlorinatedpolyethylene is heated to molten state, add zinc borate, tributyl citrate, zinc oxide, two ten four carbon alcohols esters, Zinc Stearate, morpholine, ACR impact modifier, auxiliary agent, stir and mediate 15-25 minute, send into twin screw extruder granulation, obtain A material;
(2) by all the other remaining components heating mixed melting, stir 7-10 minute, send on twin screw extruder and melt extrude granulation, obtain B material;
(3), after A, B material being mixed, melt extrude granulation on the twin screw extruder, to obtain final product.
Carried out performance test to material of the present invention, main condition are as follows:
Claims (2)
1. an insulated cable material, it is characterized in that, be made up of the raw material of following weight part: chlorinatedpolyethylene 55-60, zinc borate 4-5, tributyl citrate 14-16, zinc oxide 2-3, two ten four carbon alcohols ester 3-5, Zinc Stearate 3-4, morpholine 1-2, ACR impact modifier 1-2, vinylbenzene 12-15, light calcium carbonate 15-20, wilkinite 12-15, linking agent TAC1-2, auxiliary agent 6-8;
Described auxiliary agent is made up of the raw material of following weight part: diatomite in powder 10-12, tri (propylene glycol) diacrylate 2-3, zinc oxide 5-6, jade powder 4-5,3-aminopropyl trimethoxysilane 2-3, linking agent TAC1-2, Zinc Gluconate 1-2, Zinic stearas 1-2, magnesium nitrate 7-9, Syzygium aromaticum stem oil 1-2, Flos Rosae Rugosae quintessence oil 0.1-0.2; Diatomite in powder is sent in calcining furnace to calcine 3-4 hour at 700-730 DEG C by preparation method, take out, send in 10-15% hydrochloric acid and soak 1-2 hour, filter to obtain filter residue, wash with clear water, dry, be ground into 200-250 order powder, then the powder of drying is mixed with tri (propylene glycol) diacrylate, zinc oxide, linking agent TAC, grinding 1-2 hour, add other remaining component again, mixed grinding 1-2 hour, to obtain final product.
2. insulated cable material according to claim 1, is characterized in that, be made up of following concrete steps:
(1) chlorinatedpolyethylene is heated to molten state, add zinc borate, tributyl citrate, zinc oxide, two ten four carbon alcohols esters, Zinc Stearate, morpholine, ACR impact modifier, auxiliary agent, stir and mediate 15-25 minute, send into twin screw extruder granulation, obtain A material;
(2) by all the other remaining components heating mixed melting, stir 7-10 minute, send on twin screw extruder and melt extrude granulation, obtain B material;
(3), after A, B material being mixed, melt extrude granulation on the twin screw extruder, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410117887.2A CN103865184B (en) | 2014-03-26 | 2014-03-26 | A kind of insulated cable material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410117887.2A CN103865184B (en) | 2014-03-26 | 2014-03-26 | A kind of insulated cable material and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103865184A CN103865184A (en) | 2014-06-18 |
| CN103865184B true CN103865184B (en) | 2016-03-30 |
Family
ID=50904227
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410117887.2A Active CN103865184B (en) | 2014-03-26 | 2014-03-26 | A kind of insulated cable material and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103865184B (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103509235A (en) * | 2013-10-12 | 2014-01-15 | 绿宝电缆（集团）有限公司 | Environment-friendly polyethylene cable material and preparation method thereof |
-
2014
- 2014-03-26 CN CN201410117887.2A patent/CN103865184B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103509235A (en) * | 2013-10-12 | 2014-01-15 | 绿宝电缆（集团）有限公司 | Environment-friendly polyethylene cable material and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 耐热氯化聚乙烯电缆料的研制与开发;王丽华;《化学工程与装备》;20100630(第6期);第18-19页 * |
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| Publication number | Publication date |
|---|---|
| CN103865184A (en) | 2014-06-18 |
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