CN103859060A - Refreshing and eyesight improving type peony seed blend oil and preparation method - Google Patents
Refreshing and eyesight improving type peony seed blend oil and preparation method Download PDFInfo
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- CN103859060A CN103859060A CN201410080077.4A CN201410080077A CN103859060A CN 103859060 A CN103859060 A CN 103859060A CN 201410080077 A CN201410080077 A CN 201410080077A CN 103859060 A CN103859060 A CN 103859060A
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Abstract
The invention relates to blending oil and particularly relates to refreshing and eyesight improving type peony seed blend oil and a preparation method. The blend oil provided by the invention comprises following components in parts by mass: 15-30 parts of peony seed oil, 69-84 parts of peanut oil, 0.1-0.9 part of a chrysanthemum extract and 0.1-0.9 part of a mulberry leaf extract. The blend oil is prepared according to the refreshing and eyesight improving requirements completely; nutritional ingredients are comprehensive and reasonable and the mouth feel is very good; the blend oil is very good for health of a human body; according to the preparation method of the blend oil provided by the invention, peony seeds are immersed by water and then are frozen; the peony seeds are crushed at a low temperature and then are dried by microwave in vacuum so as to be good for extracting the peony seed oil, reducing the loss of active ingredients and improving the oil yield.
Description
Technical field
The present invention relates to a kind of ready-mixed oil, specifically a kind of clear gods order type peony seeds ready-mixed oil and preparation method.
Background technology
Peony seeds nutrition is very abundant, and as novel oil crops, not only nontoxic but also nutritious comprehensive, the elements such as protein, fat, potassium, calcium, magnesium, phosphorus, selenium and vitamin B1, B2, carotene carotene content enrich, and are rich in 18 seed amino acids.And contain odd-carbon fatty acid that active anticancer is very strong as C15, C17 etc., and the aliphatic acid that contains in addition a small amount of circulus is as sad in 2-hexyl cyclopropane, and these compositions are very rare in vegetable oil.In peony seed oil, be rich in unrighted acid and account for 92.69% of total oil mass, as leukotrienes, linoleic acid, eicosatrienoic acid, eicosenoic acid and gaidic acid etc., wherein linolenic content reaches 66.85%, secondly for linoleic acid is 23.34%.Research shows, linolenic and linoleic is essential fatty acid, can in human body, change arachidonic acid into, for synthetic phospholipid, forms eucaryotic cell structure, maintains the normal function of all tissues.
Experiment discovery, the disappearance of essential fatty acid can cause that growth eases up, and causes central nervous system, retina and platelet function abnormality pathology, supplementary linoleic acid plus linolenic acid can prevent and improve these symptoms.
China is maximum in the world tree peony plantation country, and the annual production of peony seeds ranks first in the world, however peony seeds utilization rate is lower so far, at present, adopt supercritical CO
2the method of extraction is extracted and is collected grease, obtains peony seed oil, adopt the method to extract its recovery rate 27% of peony seed oil obtaining, but the method cost is very high, and higher to the requirement of equipment, is not preferred manner for suitability for industrialized production.
Chrysanthemum is the dry capitulum of feverfew chrysanthemum, and main effect of its extract has loose wind heat-clearing, flat liver improving eyesight, and removing toxic substances, step-downs etc., cure mainly anemopyretic cold, have a headache dizzy, red eye, swell pain, improving eyesight is dim-sighted.
Mulberry leaf are dry leaves of moraceae plants mulberry, and its extract has effect of dispelling wind, heat-clearing, clearing liver, improving eyesight.
Existing edible oil mainly contains peanut oil, rapeseed oil, sesame oil, sunflower oil, safflower oil, corn oil, peanut oil and the ready-mixed oil that is primary raw material by these edible oils, the contained nutritional labeling of the vegetable oil of single kind is all comprehensive not, and the ready-mixed oil on market is not also prepared according to clear gods object demand completely.
Summary of the invention
The defect low for peony seeds utilization rate in prior art and peony seeds ready-mixed oil does not still have the clear gods object demand of complete basis to prepare, the invention provides a kind of clear gods order type peony seeds ready-mixed oil and preparation method.
For solving the problems of the technologies described above, the technical solution used in the present invention is:
A preparation method for clear gods order type peony seeds ready-mixed oil, comprises the following steps:
Step 1: after shelling without the peony seeds of disease and pest, the 5 ~ 10h that is soaked in water, drains, freezing 8 ~ 10h under-20 ~-10 DEG C of conditions is then ground into the tree peony seed that particle diameter is 0.5 ~ 1mm at this temperature, for subsequent use;
Step 2: the tree peony seed that step 1 is made joins in microwave drying oven, vacuum drying 30-60min under the condition of microwave drying power 6-9W/g, then stop microwave drying, adopt heat pump dehumidification system to carry out the dry 60 ~ 90min of circulating dehumidification, stop heat pump dehumidifying, again carry out after microwave drying 20-40min, stop microwave drying, again adopt heat pump dehumidification system to carry out circulating dehumidification to tree peony seed dry, be down to below 5% to water content, for subsequent use;
Step 3: step 2 gained tree peony seed is sent into squeezer, under 20 ~ 25 DEG C, 50MPa ~ 60MPa pressure condition, squeeze 8 ~ 10h, obtain peony seeds crude oil, for subsequent use;
Step 4: adding mass concentration to gained peony seeds crude oil is 10%NaOH solution alkali refining, add again afterwards the water of 50 ~ 60 DEG C to come unstuck, the addition of water is 5% of peony seeds crude oil weight, speed with 500 ~ 600rpm when adding water stirs 30min, precipitate afterwards 5 ~ 10h, isolate oil reservoir, adsorbed film filters to obtain peony seed oil after filtration, for subsequent use;
Step 5: according to the ratio of quality and the number of copies of 15 ~ 30 parts of peony seed oils, 69 ~ 84 parts of peanut oil, chrysanthemum extract 0.1-0.9 part, mulberry-leaf extract 0.1-0.9 part, take peony seed oil, peanut oil, chrysanthemum extract and mulberry-leaf extract;
Step 6: the chrysanthemum extract taking and mulberry-leaf extract are heated to respectively to 70 ~ 80 DEG C, under 70 ~ 80 DEG C, 800 ~ 1000rpm condition, join in peony seed oil, stir 2 ~ 4h, then add the peanut oil weighing up, under 100 ~ 110 DEG C, 800 ~ 1000rpm condition, stir 2 ~ 4h, make remaining moisture evaporation, membrane filtration obtains gods order type peony seeds ready-mixed oil clearly after filtration.
As a clear gods order type peony seeds ready-mixed oil prepared by said method, comprise the component of following mass fraction: 15 ~ 30 parts of peony seed oils, 69 ~ 84 parts of peanut oil, chrysanthemum extract 0.1-0.9 part and mulberry-leaf extract 0.1-0.9 part;
As a clear gods order type peony seeds ready-mixed oil prepared by said method, comprise the component of following mass fraction: 0.5 part of 30 parts of peony seed oils, 69 parts of peanut oil, 0.5 part of chrysanthemum extract and mulberry-leaf extract.
A kind of for the preparation of as the device of above-mentioned clear gods order type peony seeds ready-mixed oil, comprise the pulverizer for pulverizing peony seeds benevolence and pulverize the squeezer of peony seeds benevolence afterwards for squeezing, pulverizer is positioned at the top of squeezer, also be provided with the tank for soaking the peony seeds that shells, for the refrigerating chamber of peony seeds after freezing immersion, for the microwave dryer of tree peony seed after drying and crushing, batch mixing filter chamber and evaporation mixing chamber, microwave dryer is arranged between pulverizer and squeezer, batch mixing filter chamber is connected with the bottom of squeezer by oil guide pipe, batch mixing filter chamber upper surface is provided with the charge door I for adding alkali lye, inside, batch mixing filter chamber is provided with filtration adsorbed film, evaporation mixing chamber is connected with the bottom of batch mixing filter chamber by oil guide pipe, evaporation mixing chamber upper surface is provided with for adding chrysanthemum extract, the charge door II of mulberry-leaf extract and peanut oil, the top of evaporation mixing chamber sidewall is provided with steam vent,
The Oil Guide pipeline that described squeezer is connected with batch mixing filter chamber is provided with flowmeter;
Described evaporation mixing chamber is provided with outlet, and the pipeline of outlet is provided with filter membrane;
Filler in described filtration adsorbed film is active carbon.
Beneficial effect of the present invention:
Ready-mixed oil provided by the invention, prepares according to clear gods object demand completely, nutritional labeling comprehensive and reasonable, and excellent taste, and useful to health;
Ready-mixed oil preparation method provided by the invention, after employing water soaking, the method for freezing tree peony seed, fully absorbs after moisture tree peony seed, and under low-temperature condition, cell breaks, and is conducive to squeeze in subsequent technique fuel-displaced; Select to pulverize at low temperatures, compared with pulverizing with direct normal temperature, the tree peony seed brittleness after cryogenic freezing becomes large on the one hand, more easily pulverizes, and pulverizes on the other hand after tree peony seed cryogenic freezing, fuel-displaced can avoid pulverizing time, reduces the loss of active ingredient;
Ready-mixed oil preparation method provided by the invention, tree peony seed after adopting the micro-wave vacuum method of being combined with heat pump drying to freezing and pulverizing is dried, vacuum environment reduces the boiling point of its contained humidity, be beneficial to dry, microwave treatment has not only improved rate of drying and efficiency, also helps the fuel-displaced of follow-up expressing process, has reduced the technology difficulty of squeezing, improved squeezing efficiency and oil yield, oil yield can reach 28-34%.Microwave process discontinuous is used the mode of heat pump drying can avoid long-time microwave and destroy material nutritional labeling, is conducive to improve oil quality; Adopt microwave drying and heat pump dehumidifying to hocket, have the features such as quick, efficient, greatly reduce energy consumption simultaneously, operating cost and production cost are reduced greatly, its technique is simple, easy to operate, and effect highly significant, is more suitable for industrialized production;
Ready-mixed oil preparation method provided by the invention, under 70 ~ 80 DEG C, 800 ~ 1000rpm condition, in peony seed oil, add chrysanthemum extract and mulberry-leaf extract, evidence, the modest viscosity of peony seed oil under this temperature conditions, and mixing speed is suitable for, more be conducive to chrysanthemum extract and mulberry-leaf extract dispersing and dissolving to oil phase, to prepare the ready-mixed oil of homogeneous phase;
Ready-mixed oil preparation method provided by the invention, adopts filtration adsorbed film that filtration and adsorption bleaching are synchronously carried out, and has simplified preparation technology, has improved production efficiency;
Ready-mixed oil preparation facilities provided by the invention, reasonable in design, can make technique carry out under closed state, can effectively avoid outside contamination;
Ready-mixed oil preparation facilities provided by the invention, simple in structure, handled easily, is easy to realize suitability for industrialized production.
Brief description of the drawings
Fig. 1 preparation facilities structure chart of the present invention;
Reference numeral: 1, housing, 2, microwave dryer, 3, pulverizer, 4, squeezer, 5, batch mixing filter chamber, 6, filter adsorbed film, 7, evaporation mixing chamber, 8, charge door I, 9, charge door II, 10, steam vent, 11, outlet, 12, flowmeter, 13, filter membrane, 14, charging aperture.
Detailed description of the invention
Below in conjunction with detailed description of the invention, the present invention is further elaborated.
A preparation method for clear gods order type peony seeds ready-mixed oil, comprises the following steps:
Step 1: after shelling without the peony seeds of disease and pest, the 5 ~ 10h that is soaked in water, drains, freezing 8 ~ 10h under-20 ~-10 DEG C of conditions is then ground into the tree peony seed that particle diameter is 0.5 ~ 1mm at this temperature, for subsequent use;
Step 2: the tree peony seed that step 1 is made joins in microwave drying oven, vacuum drying 30-60min under the condition of microwave drying power 6-9W/g, then stop microwave drying, adopt heat pump dehumidification system to carry out the dry 60 ~ 90min of circulating dehumidification, stop heat pump dehumidifying, again carry out after microwave drying 20-40min, stop microwave drying, again adopt heat pump dehumidification system to carry out circulating dehumidification to tree peony seed dry, be down to below 5% to water content, for subsequent use;
Step 3: step 2 gained tree peony seed is sent into squeezer, under 20 ~ 25 DEG C, 50MPa ~ 60MPa pressure condition, squeeze 8 ~ 10h, obtain peony seeds crude oil, for subsequent use;
Step 4: adding mass concentration to gained peony seeds crude oil is 10%NaOH solution alkali refining, add again afterwards the water of 50 ~ 60 DEG C to come unstuck, the addition of water is 5% of peony seeds crude oil weight, speed with 500 ~ 600rpm when adding water stirs 30min, precipitate afterwards 5 ~ 10h, isolate oil reservoir, adsorbed film filters to obtain peony seed oil after filtration, for subsequent use;
Step 5: according to the ratio of quality and the number of copies of 15 ~ 30 parts of peony seed oils, 69 ~ 84 parts of peanut oil, chrysanthemum extract 0.1-0.9 part, mulberry-leaf extract 0.1-0.9 part, take peony seed oil, peanut oil, chrysanthemum extract and mulberry-leaf extract;
Step 6: the chrysanthemum extract taking and mulberry-leaf extract are heated to respectively to 70 ~ 80 DEG C, under 70 ~ 80 DEG C, 800 ~ 1000rpm condition, join in peony seed oil, stir 2 ~ 4h, then add the peanut oil weighing up, under 100 ~ 110 DEG C, 800 ~ 1000rpm condition, stir 2 ~ 4h, make remaining moisture evaporation, membrane filtration obtains gods order type peony seeds ready-mixed oil clearly after filtration.
As a clear gods order type peony seeds ready-mixed oil prepared by said method, comprise the component of following mass fraction: 15 ~ 30 parts of peony seed oils, 69 ~ 84 parts of peanut oil, chrysanthemum extract 0.1-0.9 part and mulberry-leaf extract 0.1-0.9 part;
As a clear gods order type peony seeds ready-mixed oil prepared by said method, comprise the component of following mass fraction: 0.5 part of 30 parts of peony seed oils, 69 parts of peanut oil, 0.5 part of chrysanthemum extract and mulberry-leaf extract.
A kind of as the preparation facilities of above-mentioned clear gods order type peony seeds ready-mixed oil, comprise the pulverizer 3 for pulverizing peony seeds benevolence and pulverize the squeezer 4 of peony seeds benevolence afterwards for squeezing, pulverizer 3 is positioned at the top of squeezer 4, also be provided with the tank for soaking the peony seeds that shells, for the refrigerating chamber of peony seeds after freezing immersion, for the microwave dryer 2 of tree peony seed after drying and crushing, batch mixing filter chamber 5 and evaporation mixing chamber 7, microwave dryer 2 is arranged between pulverizer 3 and squeezer 4, batch mixing filter chamber 5 is connected with the bottom of squeezer 4 by oil guide pipe, batch mixing filter chamber 5 upper surfaces are provided with the charge door I 8 for adding alkali lye, 5 inside, batch mixing filter chamber are provided with filters adsorbed film 6, evaporation mixing chamber 7 is connected with the bottom of batch mixing filter chamber 5 by oil guide pipe, evaporation mixing chamber 7 upper surfaces are provided with for adding chrysanthemum extract, the charge door II 9 of mulberry-leaf extract and peanut oil, the top of evaporation mixing chamber 7 sidewalls is provided with steam vent 10,
The Oil Guide pipeline that described squeezer 4 is connected with batch mixing filter chamber 5 is provided with flowmeter 12;
Described evaporation mixing chamber 7 is provided with outlet 11, and the pipeline of outlet 11 is provided with filter membrane 13;
Filler in described filtration adsorbed film 6 is active carbon.
A preparation method for clear gods order type peony seeds ready-mixed oil, comprises the following steps:
Step 1: after shelling without the peony seeds of disease and pest, water soaks 5h in tank, drains, under-10 DEG C of conditions in refrigerating chamber freezing 8h, then at this temperature, add pulverizer 3 to be ground into the tree peony seed that particle diameter is 0.5mm by charging aperture 14, for subsequent use;
Step 2: the tree peony seed that step 1 is made joins microwave drying oven 2, vacuum drying 30min under the condition of microwave drying power 6W/g, then stop microwave drying, adopt heat pump dehumidification system to carry out the dry 60min of circulating dehumidification, stop heat pump dehumidifying, again carry out after microwave drying 40min, stop microwave drying, again adopt heat pump dehumidification system to carry out circulating dehumidification to tree peony seed dry, be down to below 5% to water content, for subsequent use;
Step 3: step 2 gained tree peony seed is sent into squeezer 4, under 20 ~ 25 DEG C, 50MPa ~ 60MPa pressure condition, squeeze 8h, obtain peony seeds crude oil and flow into batch mixing filter chamber 5, for subsequent use;
Step 4: be 10%NaOH solution alkali refining to adding concentration in gained peony seeds crude oil by charge door I 8, add again afterwards the water of 50 ~ 60 DEG C to come unstuck, the addition of water is 5% of peony seeds crude oil weight, speed with 500 ~ 600rpm when adding water stirs 30min, precipitate afterwards 5h, isolate oil reservoir, adsorbed film 6 filters to obtain peony seed oil after filtration, for subsequent use;
Step 5: according to mass fraction: the ratio of quality and the number of copies of 15 parts of peony seed oils, 84 parts of peanut oil, 0.1 part of chrysanthemum extract, 0.9 part of mulberry-leaf extract takes chrysanthemum extract, mulberry-leaf extract and peanut oil;
Step 6: the chrysanthemum extract taking and mulberry-leaf extract are heated to respectively to 70 ~ 80 DEG C, under 70 ~ 80 DEG C, 800 ~ 1000rpm condition, joined in peony seed oil by charge door II 9, stir 2 ~ 4h, then add the peanut oil weighing up, under 100 ~ 110 DEG C, 800 ~ 1000rpm condition, stir 2 ~ 4h, residual moisture in oil reservoir is discharged by steam vent 10, obtains gods order type peony seeds ready-mixed oil clearly through exporting filter membrane 13 membrane filtrations that arrange on 11 pipelines.
A clear gods order type peony seeds ready-mixed oil of being prepared by above method, comprises the component of following mass fraction: 15 parts of peony seed oils, 84 parts of peanut oil, 0.1 part of chrysanthemum extract, 0.9 part of mulberry-leaf extract.
Embodiment 2
A preparation method for clear gods order type peony seeds ready-mixed oil, comprises the following steps:
Step 1: after shelling without the peony seeds of disease and pest, water soaks 10h in tank, drains, under-20 DEG C of conditions in refrigerating chamber freezing 10h, then at this temperature, add pulverizer 3 to be ground into the tree peony seed that particle diameter is 1mm by charging aperture 14, for subsequent use;
Step 2: the tree peony seed that step 1 is made joins microwave drying oven 2, vacuum drying 60min under the condition of microwave drying power 9W/g, then stop microwave drying, adopt heat pump dehumidification system to carry out the dry 90min of circulating dehumidification, stop heat pump dehumidifying, again carry out after microwave drying 20min, stop microwave drying, again adopt heat pump dehumidification system to carry out circulating dehumidification to tree peony seed dry, be down to below 5% to water content, for subsequent use;
Step 3: step 2 gained tree peony seed is sent into squeezer 4, under 20 ~ 25 DEG C, 50MPa ~ 60MPa pressure condition, squeeze 10h, obtain peony seeds crude oil and flow into batch mixing filter chamber 5, for subsequent use;
Step 4: be 10%NaOH solution alkali refining to adding concentration in gained peony seeds crude oil by charge door I 8, add again afterwards the water of 50 ~ 60 DEG C to come unstuck, the addition of water is 5% of peony seeds crude oil weight, speed with 500 ~ 600rpm when adding water stirs 30min, precipitate afterwards 5h, isolate oil reservoir, adsorbed film 6 filters to obtain peony seed oil after filtration, for subsequent use;
Step 5: according to mass fraction: the ratio of quality and the number of copies of 30 parts of peony seed oils, 69 parts of peanut oil, 0.5 part of Flos Chrysanthemi Indici extract, 0.5 part of mulberry-leaf extract takes chrysanthemum extract, mulberry-leaf extract and peanut oil;
Step 6: the chrysanthemum extract taking and mulberry-leaf extract are heated to respectively to 70 ~ 80 DEG C, under 70 ~ 80 DEG C, 800 ~ 1000rpm condition, slowly joined in peony seed oil by charge door II 9, stir 2 ~ 4h, then add the peanut oil weighing up, under 100 ~ 110 DEG C, 800 ~ 1000rpm condition, stir 2 ~ 4h, residual moisture in oil reservoir is discharged by steam vent 10, obtains gods order type peony seeds ready-mixed oil clearly through exporting filter membrane 13 membrane filtrations that arrange on 11 pipelines.
A clear gods order type peony seeds ready-mixed oil of being prepared by above method, comprises the component of following mass fraction: 30 parts of peony seed oils, 69 parts of peanut oil, 0.5 part of Flos Chrysanthemi Indici extract, 0.5 part of mulberry-leaf extract.
Claims (7)
1. a preparation method for clear gods order type peony seeds ready-mixed oil, is characterized in that, comprises the following steps:
Step 1: after shelling without the peony seeds of disease and pest, the 5 ~ 10h that is soaked in water, drains, freezing 8 ~ 10h under-20 ~-10 DEG C of conditions is then ground into the tree peony seed that particle diameter is 0.5 ~ 1mm at this temperature, for subsequent use;
Step 2: the tree peony seed that step 1 is made joins in microwave drying oven, vacuum drying 30-60min under the condition of microwave drying power 6-9W/g, then stop microwave drying, adopt heat pump dehumidification system to carry out the dry 60 ~ 90min of circulating dehumidification, stop heat pump dehumidifying, again carry out after microwave drying 20-40min, stop microwave drying, again adopt heat pump dehumidification system to carry out circulating dehumidification to tree peony seed dry, be down to below 5% to water content, for subsequent use;
Step 3: step 2 gained tree peony seed is sent into squeezer, under 20 ~ 25 DEG C, 50MPa ~ 60MPa pressure condition, squeeze 8 ~ 10h, obtain peony seeds crude oil, for subsequent use;
Step 4: adding mass concentration to gained peony seeds crude oil is 10%NaOH solution alkali refining, add again afterwards the water of 50 ~ 60 DEG C to come unstuck, the addition of water is 5% of peony seeds crude oil weight, speed with 500 ~ 600rpm when adding water stirs 30min, precipitate afterwards 5 ~ 10h, isolate oil reservoir, adsorbed film filters to obtain peony seed oil after filtration, for subsequent use;
Step 5: according to the ratio of quality and the number of copies of 15 ~ 30 parts of peony seed oils, 69 ~ 84 parts of peanut oil, chrysanthemum extract 0.1-0.9 part, mulberry-leaf extract 0.1-0.9 part, take peony seed oil, peanut oil, chrysanthemum extract and mulberry-leaf extract;
Step 6: the chrysanthemum extract taking and mulberry-leaf extract are heated to respectively to 70 ~ 80 DEG C, under 70 ~ 80 DEG C, 800 ~ 1000rpm condition, join in peony seed oil, stir 2 ~ 4h, then add the peanut oil weighing up, under 100 ~ 110 DEG C, 800 ~ 1000rpm condition, stir 2 ~ 4h, make remaining moisture evaporation, membrane filtration obtains gods order type peony seeds ready-mixed oil clearly after filtration.
2. the clear gods order type peony seeds ready-mixed oil that as claimed in claim 1 prepared by method, it is characterized in that, comprise the component of following mass fraction: 15 ~ 30 parts of peony seed oils, 69 ~ 84 parts of peanut oil, chrysanthemum extract 0.1-0.9 part and mulberry-leaf extract 0.1-0.9 part.
3. clear gods order type peony seeds ready-mixed oil as claimed in claim 2, is characterized in that, comprises the component of following mass fraction: 0.5 part of 30 parts of peony seed oils, 69 parts of peanut oil, 0.5 part of chrysanthemum extract and mulberry-leaf extract.
4. the device for the preparation of clear gods order type peony seeds ready-mixed oil as claimed in claim 1, comprise the pulverizer (3) for pulverizing peony seeds benevolence and pulverize the squeezer (4) of peony seeds benevolence afterwards for squeezing, pulverizer (3) is positioned at the top of squeezer (4), it is characterized in that: be also provided with the tank for soaking the peony seeds that shells, for the refrigerating chamber of peony seeds after freezing immersion, for the microwave dryer (2) of tree peony seed after drying and crushing, batch mixing filter chamber (5) and evaporation mixing chamber (7), microwave dryer (2) is arranged between pulverizer (3) and squeezer (4), batch mixing filter chamber (5) is connected with the bottom of squeezer (4) by oil guide pipe, batch mixing filter chamber (5) upper surface is provided with the charge door I (8) for adding alkali lye, inside, batch mixing filter chamber (5) is provided with filters adsorbed film (6), evaporation mixing chamber (7) is connected with the bottom of batch mixing filter chamber (5) by oil guide pipe, evaporation mixing chamber (7) upper surface is provided with for adding chrysanthemum extract, the charge door II (9) of mulberry-leaf extract and peanut oil, the top of evaporation mixing chamber (7) sidewall is provided with steam vent (10).
5. the preparation facilities of clear gods order type peony seeds ready-mixed oil as claimed in claim 4, is characterized in that: the Oil Guide pipeline that described squeezer (4) is connected with batch mixing filter chamber (5) is provided with flowmeter (12).
6. the preparation facilities of clear gods order type peony seeds ready-mixed oil as claimed in claim 4, is characterized in that: described evaporation mixing chamber (7) is provided with outlet (11), and the pipeline of outlet (11) is provided with filter membrane (13).
7. the preparation facilities of clear gods order type peony seeds ready-mixed oil as claimed in claim 4, is characterized in that: the filler in described filtration adsorbed film (6) is active carbon.
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CN112940839A (en) * | 2021-01-28 | 2021-06-11 | 江苏国色天香油用牡丹科技发展有限公司 | High-yield peony seed oil and processing technology thereof |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101548705A (en) * | 2008-04-03 | 2009-10-07 | 李松健 | Muberry beaf and chrysanthemum tea |
CN101812370A (en) * | 2010-03-29 | 2010-08-25 | 甘肃省轻工研究院 | Method and device for extracting peony seed oil from peony seeds |
CN101653174B (en) * | 2009-09-07 | 2012-05-02 | 兰州牡丹园艺开发公司 | Method for preparing blend oil and cold-pressing and extracting peony seed oil |
CN103416490A (en) * | 2012-05-25 | 2013-12-04 | 洛阳花瓣舞生物技术有限公司 | Preparation method of peony seed oil |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN101548705A (en) * | 2008-04-03 | 2009-10-07 | 李松健 | Muberry beaf and chrysanthemum tea |
CN101653174B (en) * | 2009-09-07 | 2012-05-02 | 兰州牡丹园艺开发公司 | Method for preparing blend oil and cold-pressing and extracting peony seed oil |
CN101812370A (en) * | 2010-03-29 | 2010-08-25 | 甘肃省轻工研究院 | Method and device for extracting peony seed oil from peony seeds |
CN103416490A (en) * | 2012-05-25 | 2013-12-04 | 洛阳花瓣舞生物技术有限公司 | Preparation method of peony seed oil |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN112940839A (en) * | 2021-01-28 | 2021-06-11 | 江苏国色天香油用牡丹科技发展有限公司 | High-yield peony seed oil and processing technology thereof |
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