CN103815051B - Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil - Google Patents
Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil Download PDFInfo
- Publication number
- CN103815051B CN103815051B CN201410080183.2A CN201410080183A CN103815051B CN 103815051 B CN103815051 B CN 103815051B CN 201410080183 A CN201410080183 A CN 201410080183A CN 103815051 B CN103815051 B CN 103815051B
- Authority
- CN
- China
- Prior art keywords
- oil
- peony
- peony seeds
- peony seed
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 235000006484 Paeonia officinalis Nutrition 0.000 title claims abstract description 95
- 239000003921 oil Substances 0.000 title claims abstract description 36
- 235000019198 oils Nutrition 0.000 title claims abstract description 36
- 235000015112 vegetable and seed oil Nutrition 0.000 title claims abstract description 31
- 239000008157 edible vegetable oil Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000203 mixture Substances 0.000 title abstract 6
- 235000007340 Hordeum vulgare Nutrition 0.000 title abstract 3
- 240000005979 Hordeum vulgare Species 0.000 title 1
- 244000170916 Paeonia officinalis Species 0.000 title 1
- 241000736199 Paeonia Species 0.000 claims abstract description 94
- 238000000034 method Methods 0.000 claims abstract description 22
- 239000010779 crude oil Substances 0.000 claims abstract description 17
- 238000007670 refining Methods 0.000 claims abstract description 15
- 238000002156 mixing Methods 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims description 23
- 241000209140 Triticum Species 0.000 claims description 22
- 235000021307 Triticum Nutrition 0.000 claims description 22
- 239000012266 salt solution Substances 0.000 claims description 22
- 238000005119 centrifugation Methods 0.000 claims description 11
- 230000008014 freezing Effects 0.000 claims description 10
- 238000007710 freezing Methods 0.000 claims description 10
- 230000010355 oscillation Effects 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 7
- 238000004821 distillation Methods 0.000 claims description 2
- 239000004519 grease Substances 0.000 abstract description 6
- 241000209219 Hordeum Species 0.000 abstract 2
- 238000010298 pulverizing process Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 240000005001 Paeonia suffruticosa Species 0.000 description 1
- 235000003889 Paeonia suffruticosa Nutrition 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 229930003451 Vitamin B1 Natural products 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000003925 fat Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- AOJZSYZUFZULLN-UHFFFAOYSA-N hexylcyclopropane Chemical compound CCCCCCC1CC1 AOJZSYZUFZULLN-UHFFFAOYSA-N 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 238000005461 lubrication Methods 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229960003495 thiamine Drugs 0.000 description 1
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 1
- 239000011691 vitamin B1 Substances 0.000 description 1
- 235000010374 vitamin B1 Nutrition 0.000 description 1
Landscapes
- Fats And Perfumes (AREA)
- Edible Oils And Fats (AREA)
Abstract
The invention provides a blend edible oil of peony seed oil and barley oil and a preparation method of the blend edible oil. The blend edible oil is prepared through the following steps: taking shelled peony seeds, conducting physical squeezing to prepare peony seed crude oil after the shelled peony seeds are processed; refining the peony seed crude oil to prepare refined peony seed oil; blending the refined peony seed oil and barley oil sold in market according to the weight ratio of 1:(0.1-0.5), so that the blend edible oil is obtained. According to the invention, after the shelled peony seeds are subjected to a series of processing, the cell structure is destroyed, and the water content of the cells is reduced, so that grease in the cells can be separated from the cells in the process of squeezing conveniently, thereby improving the oil yield.
Description
Technical field
The present invention relates to edible oil field, specifically a kind of peony seed oil and large wheat oil blending edible oil and preparation method thereof.
Background technology
Peony seed oil is edible oil that is emerging, that have edible health double effects, take from peony seed, wherein be rich in the elements such as protein, fat, potassium, calcium, magnesium, phosphorus, selenium and vitamin B1, B2, carrotene etc., and contain the very strong odd-carbon fatty acid of active anticancer as C15, C17 etc., aliphatic acid in addition containing a small amount of circulus is as sad in 2-hexyl cyclopropane, is widely used in medicine, health care, food, superior cosmetics, lubrication wet goods industry.
Two kinds of modes and the respective pluses and minuses of peony seed oil production are as follows:
1) extract technology: the residue tree peony seedcake after squeezing, leaches peony seed oil with chemical solvent.Advantage: oil yield is high, output is large, saves cost.Shortcoming: nutritional labeling reduces, belongs to chemical industry.
2) squeezing process: industrialization squeezing peony seed oil on the basis of ancient method.Advantage: low temperature of controlling well can retain all original nutritional labelings of peony seed oil, physical squeezing.Shortcoming: oil yield is low, cost is high.
Summary of the invention
The object of the invention is to overcome the problem that the oil yield of conventional press method is low, and then utilize commercially available large wheat oil to provide a kind of peony seed oil and large wheat oil blending edible oil and preparation method thereof, the ready-mixed oil prepared by the method is nutritious and balanced, overcome the problem that conventional press technique oil yield is low, make the squeezing oil yield of peony seed oil exceed about 10% than the oil yield of conventional press method.
The technical scheme that the present invention takes for achieving the above object is: a kind of peony seed oil and large wheat oil blending edible oil, to be in harmonious proportion to form by the peony seed oil of large wheat oil and refining by weight the ratio of 0.1-0.5:1.
The method preparing above-mentioned peony seed oil and large wheat oil blending edible oil is: remove shell peony seeds and carry out physical squeezing after treatment and obtain peony seeds crude oil, again the refining peony seed oil obtained after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio and namely obtain product, wherein, the process of peony seeds of shelling described in comprises the following steps:
1) peony seeds after shelling is added to the water soak 2-5h after drain, and put into the freezing 15-20h of environment that temperature is less than-45 DEG C immediately, in sub-zero low temperature environment, be then ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) being taken out and under the environment temperature of 20-25 DEG C, join mass concentration by the peony seeds powder of step 1) is in the salt solution of 15-18%, leaves standstill 17-24h after then passing into supersonic oscillations 3-5min wherein, for subsequent use;
3) adopt centrifugation make step 2) in peony seeds powder be separated with salt solution, be then dry under the condition of 65-70 DEG C to be less than 5% to moisture content in temperature, afterwards peony seeds powder squeezed.
Described step 2) condition of supersonic oscillations is: the ultrasonic wave of the corresponding 120-150W of salt solution of every kilogram, hyperacoustic frequency is 80-110KHz.
The rotating speed of centrifugation in described step 3) is 2500-4000r/min.
Isolate the salt solution after peony seeds powder in described step 3) and isolate peony seeds crude oil by distillation procedure.
In the present invention, first soaked in water by peony seeds is to make the cell of peony seeds fully absorb water, then in the freezing environment below-45 DEG C freezing after and under the environment temperature of 20-25 DEG C, put into salt solution, destroy eucaryotic cell structure like this, be convenient to squeeze time fuel-displaced;
Meanwhile, peony seeds powder is placed in the salt solution that mass concentration is 15-18%, and can make the cell dehydration of peony seeds, cell volume reduces, and is not only convenient to follow-up oven dry, and eliminates moisture unnecessary in cell, improves squeezing oil yield; Introduce supersonic oscillations in the process, not only play stirring action, and the cyto-architectural effect of destruction can be played; In follow-up centrifugation, the grease outer layers of cell interior also can be made to move, be convenient to be extracted in expressing process.
In the present invention, by freezing for peony seeds rear pulverizing, granularity is less, is more conducive to post-processed and improves oil yield, but, in crushing process, have amount of grease to be extracted, the particle of pulverizing is less, and the grease of crushing process loss is more, consider above factor, the particle diameter after pulverizing is that 1-2mm is advisable; And, be compared to and directly pulverize, pulverize in sub-zero low temperature environment immediately after freezing in the freezing environment below-45 DEG C, the loss of grease in crushing process can be effectively reduced.
Beneficial effect: the present invention will shell peony seeds after a series of process, destroys eucaryotic cell structure and decreases the water content of cell, being convenient to intracellular grease like this and separating from cell in expressing process, thus improve oil yield.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further elaborated.
Embodiment 1
A kind of peony seed oil and large wheat oil blending edible oil, formed by weight the ratio mediation of 0.1:1 by the peony seed oil of commercially available large wheat oil and refining;
Its preparation method is, remove shell peony seeds to carry out physical squeezing after treatment and obtain peony seeds crude oil, again the refining peony seed oil obtained after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio i.e. obtained product, wherein, described in the shell process of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak 2h after drain, and put into the freezing 15h of environment that temperature is less than-45 DEG C immediately, in sub-zero low temperature environment, be then ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) being taken out and under the environment temperature of 20-25 DEG C, join mass concentration by the peony seeds powder of step 1) is in the salt solution of 15%, then 17h is left standstill after passing into supersonic oscillations 3min wherein, hyperacoustic frequency is 80KHz, the ultrasonic wave of every kilogram of corresponding 120W power of salt solution, for subsequent use;
3) adopt centrifugation make step 2) in peony seeds powder be separated with salt solution, the rotating speed of centrifugation is 2500r/min, then in temperature is to dry under the condition of 65 DEG C to be less than 5% to moisture content, squeezes afterwards to peony seeds powder;
4) salt solution after being separated distills, and isolates the peony seeds crude oil wherein contained.
Embodiment 2
A kind of peony seed oil and large wheat oil blending edible oil, formed by weight the ratio mediation of 0.5:1 by the peony seed oil of commercially available large wheat oil and refining;
Its preparation method is, remove shell peony seeds to carry out physical squeezing after treatment and obtain peony seeds crude oil, again the refining peony seed oil obtained after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio i.e. obtained product, wherein, described in the shell process of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak 5h after drain, and put into the freezing 20h of environment that temperature is less than-45 DEG C immediately, in sub-zero low temperature environment, be then ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) being taken out and under the environment temperature of 20-25 DEG C, join mass concentration by the peony seeds powder of step 1) is in the salt solution of 18%, then 24h is left standstill after passing into supersonic oscillations 5min wherein, hyperacoustic frequency is 110KHz, the ultrasonic wave of every kilogram of corresponding 150W power of salt solution, for subsequent use;
3) adopt centrifugation make step 2) in peony seeds powder be separated with salt solution, the rotating speed of centrifugation is 4000r/min, then in temperature is to dry under the condition of 70 DEG C to be less than 5% to moisture content, squeezes afterwards to peony seeds powder;
4) salt solution after being separated distills, and isolates the peony seeds crude oil wherein contained.
Embodiment 3
A kind of peony seed oil and large wheat oil blending edible oil, formed by weight the ratio mediation of 0.3:1 by the peony seed oil of commercially available large wheat oil and refining;
Its preparation method is, remove shell peony seeds to carry out physical squeezing after treatment and obtain peony seeds crude oil, again the refining peony seed oil obtained after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion according to the above ratio i.e. obtained product, wherein, described in the shell process of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak 3.5h after drain, and put into the freezing 18h of environment that temperature is less than-45 DEG C immediately, in sub-zero low temperature environment, be then ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) being taken out and under the environment temperature of 20-25 DEG C, join mass concentration by the peony seeds powder of step 1) is in the salt solution of 17%, then 20h is left standstill after passing into supersonic oscillations 4min wherein, hyperacoustic frequency is 95KHz, the ultrasonic wave of every kilogram of corresponding 135W power of salt solution, for subsequent use;
3) adopt centrifugation make step 2) in peony seeds powder be separated with salt solution, the rotating speed of centrifugation is 3300r/min, then in temperature is to dry under the condition of 68 DEG C to be less than 5% to moisture content, squeezes afterwards to peony seeds powder;
4) salt solution after being separated distills, and isolates the peony seeds crude oil wherein contained.
Claims (4)
1. the preparation method of a peony seed oil and large wheat oil blending edible oil, remove shell peony seeds to carry out physical squeezing after treatment and obtain peony seeds crude oil, again the refining peony seed oil that obtains after the refining of peony seeds crude oil and commercially available large wheat oil are in harmonious proportion i.e. obtained product by weight the ratio of 1:0.1-0.5, it is characterized in that: described in the shell process of peony seeds comprise the following steps:
1) peony seeds after shelling is added to the water soak 2-5h after drain, and put into the freezing 15-20h of environment that temperature is less than-45 DEG C immediately, in sub-zero low temperature environment, be then ground into the peony seeds powder that particle diameter is 1-2mm, for subsequent use;
2) being taken out and under the environment temperature of 20-25 DEG C, join mass concentration by the peony seeds powder of step 1) is in the salt solution of 15-18%, leaves standstill 17-24h after then passing into supersonic oscillations 3-5min wherein, for subsequent use;
3) adopt centrifugation make step 2) in peony seeds powder be separated with salt solution, be then dry under the condition of 65-70 DEG C to be less than 5% to moisture content in temperature, afterwards peony seeds powder squeezed.
2. the preparation method of peony seed oil according to claim 1 and large wheat oil blending edible oil, is characterized in that: described step 2) condition of supersonic oscillations is: the ultrasonic wave of the corresponding 120-150W of salt solution of every kilogram, hyperacoustic frequency is 80-110kHz.
3. the preparation method of peony seed oil according to claim 1 and large wheat oil blending edible oil, is characterized in that: the rotating speed of centrifugation in described step 3) is 2500-4000r/min.
4. the preparation method of peony seed oil according to claim 1 and large wheat oil blending edible oil, is characterized in that: isolate the salt solution after peony seeds powder in described step 3) and isolate peony seeds crude oil by distillation procedure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410080183.2A CN103815051B (en) | 2014-03-06 | 2014-03-06 | Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410080183.2A CN103815051B (en) | 2014-03-06 | 2014-03-06 | Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103815051A CN103815051A (en) | 2014-05-28 |
| CN103815051B true CN103815051B (en) | 2015-06-17 |
Family
ID=50750581
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410080183.2A Expired - Fee Related CN103815051B (en) | 2014-03-06 | 2014-03-06 | Blend edible oil of peony seed oil and barley oil and preparation method of blend edible oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103815051B (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1960639A (en) * | 2004-06-14 | 2007-05-09 | 卡拉皮利·佛罗伦萨公开股份有限公司 | Cereal and fruit oil |
| CN101653174A (en) * | 2009-09-07 | 2010-02-24 | 兰州牡丹园艺开发公司 | Method for preparing blend oil and cold-pressing and extracting peony seed oil |
| CN103493908A (en) * | 2013-10-11 | 2014-01-08 | 河南科技大学 | Nut blend oil with lipid lowering and blood glucose reducing effects and preparation method thereof |
-
2014
- 2014-03-06 CN CN201410080183.2A patent/CN103815051B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1960639A (en) * | 2004-06-14 | 2007-05-09 | 卡拉皮利·佛罗伦萨公开股份有限公司 | Cereal and fruit oil |
| CN101653174A (en) * | 2009-09-07 | 2010-02-24 | 兰州牡丹园艺开发公司 | Method for preparing blend oil and cold-pressing and extracting peony seed oil |
| CN103493908A (en) * | 2013-10-11 | 2014-01-08 | 河南科技大学 | Nut blend oil with lipid lowering and blood glucose reducing effects and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103815051A (en) | 2014-05-28 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103815061B (en) | Blend edible oil of peony seed oil and sesame oil and preparation method of blend edible oil | |
| CN102746938A (en) | Method for preparing grease and protein from oil seed kernels by aqueous enzymatic method | |
| CN102321160B (en) | Production technology of sesame protein powder | |
| CN102492537B (en) | Method for extracting krill oil from antarctic krill | |
| CN103254989A (en) | Method for extraction of tea seed oil by ultrasound-assisted enzymatic process | |
| CN102405988B (en) | Method for extracting krill oil with high phospholipid content from krill | |
| CN103815053B (en) | A kind of puerpera is by peony seeds ready-mixed oil and preparation method | |
| CN100358990C (en) | Extraction of aqueous solvent from hickory nut oil | |
| CN104083409A (en) | Preparation method of Mythic Fungus spore oil and its softgel | |
| CN103865632B (en) | A kind of delicate fragrance type seed of Flos Moutan mixed oil and preparation method | |
| CN105602700A (en) | Preparation method of cold-pressed peony seed oil with high oil yield | |
| CN102396677A (en) | Method for preparing jujube perfume, jujube dietary fiber and the like by comprehensive utilization | |
| CN103396878A (en) | Preparation method of low-temperature cold-pressed peanut oil | |
| CN104974071B (en) | A kind of preparation method of luteole | |
| CN104629902A (en) | Method for extracting maize germ oil assisted by ethyl alcohol and steam explosion | |
| CN105018210A (en) | Method for enzymaticly digesting porcine fat tissue and applications thereof | |
| CN103409230B (en) | Method for low temperature extraction of plant oil through n-butane-ethanol-water double phase solvent | |
| CN105132138A (en) | Processing technology for camellia seeds | |
| CN103815055B (en) | Blend cooking oil of peony seed oil and tea seed oil, and preparation method thereof | |
| CN105886108A (en) | Pure camellia oil processing technology | |
| CN102757859A (en) | Low-temperature cold-pressing process for crude maize oil | |
| CN105670796A (en) | Preparation method of lemongrass essential oil | |
| CN108424809A (en) | A kind of production method improving camellia seed oil yield | |
| CN103382412A (en) | Preparation process for low-temperature cold-pressed carotene-rich peanut oil | |
| CN103820212B (en) | Blend edible oil of peony seed oil and peanut oil and preparation method of blend edible oil |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20180306 Address after: No. 4, unit 2, No. 7, courtyard No. 2, Yucai street, old city city, Henan Province, 702 Patentee after: Yang Panpan Address before: 471003 Henan province Luoyang Xigong Mill Road Wangcheng Avenue on the west side of Mill Road 89, two floor No. 01-02001 Patentee before: LUOYANG CHUNKUI AGRICULTURAL DEVELOPMENT Co.,Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20150617 |