CN103766361B - Insecticide of a kind of containing chlorantraniliprole and carbosulfan and preparation method thereof - Google Patents
Insecticide of a kind of containing chlorantraniliprole and carbosulfan and preparation method thereof Download PDFInfo
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- CN103766361B CN103766361B CN201410060279.2A CN201410060279A CN103766361B CN 103766361 B CN103766361 B CN 103766361B CN 201410060279 A CN201410060279 A CN 201410060279A CN 103766361 B CN103766361 B CN 103766361B
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- carbosulfan
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Abstract
The invention provides insecticide of a kind of containing chlorantraniliprole and carbosulfan and preparation method thereof, belong to technical field of pesticide.Active ingredient contained by this insecticide is Rynaxypyr 10 ~ 20%, carbosulfan 5 ~ 10%.This insecticide is had complementary advantages, and synergy is remarkable, and overcome pest resistance to insecticide, expand insecticidal spectrum, decrease times for spraying and pesticide dosage, reduce production cost, can effectively control sugarcane moth borer and woolly aphid, preventive effect reaches more than more than 85% and 95% respectively.
Description
Technical field
The invention belongs to technical field of pesticide, be specifically related to insecticide of a kind of containing chlorantraniliprole and carbosulfan and preparation method thereof.
Background technology
Rynaxypyr is O-formammidotiazol-benzamide broad spectrum pesticide, there is stomach toxicity and action of contace poison, can in stem, leaf surface infiltration plant corpus, also move by root absorption with at xylem, there is excellent control efficiency to the lepidoptera pest of various crop, also have good preventive effect to other insects.Its mechanism of action activates blue Buddhist nun's alkali acceptor, the calcium of release smooth muscle and the interior storage of striated muscle cell, causes muscle to regulate weak, fiber crops illness, until insect is dead.
Carbosulfan belongs to carbamate insecticide, be that poisonous Furadan plays insecticidal action at insect bodies intracellular metabolite, its toxicity mechanism is the activity suppressing insect enzyme acetylcholine (Ache) and carboxy-lesterase, cause the accumulation of acetylcholine (Ach) and carboxylate, affect the normal nerve conduction of insect and lethal.Its lethality is strong, and instant effect, has stomach toxicity and action of contace poison.Fat-soluble, interior absorption is good, penetration is strong, effect rapidly, residual low, have longer residual effect, use safety, to adult and larva all effective.The various crop insects such as sugarcane, corn, cotton, paddy rice can be prevented and treated, particularly excellent to the control efficiency of aphid.
Sugarcane moth borer is that the first insect the most general, harm is the most serious occurs sugarcane district of China at present.Sugarcane moth borer has harm sugarcane whole vegetative period, and endanger growing point seedling stage and cause withered heart seedling, what withered heart rate was heavy reaches 31.16% ~ 61.82%; The middle and late growth stage bores moth harm sugarcane stem (borer pest strain rate serious up to more than 80%), and destroy sugarcane stem tissue, hinder sugarcane production, reduction output and sugar, cause windbreak.
Sugar cane cottony aphid (CeratovacunalanigeraZehntner) is the important pests in sugarcane jointing vegetative period, and occurring area can reach more than 80% of cultivated area.Particularly sugarcane implementation fall planting in recent years or winter plant, complicated cropping system, make woolly aphid obtain sufficient foodstuff and shift to cause harm, add year after year hot drought, be conducive to its Fast-propagation and the develop of the population, have and increase the weight of harm trend year by year.The general underproduction 13.7%-24.6% of killed sugarcane, heavy reaches more than 50%, and Sucrose reduces 10%-40%.Prevent and treat not in place not in time, normal harm is caused disaster, and it is serious that the underproduction subtracts sugar.
Production prevents and treats Sugarcane Pests mainly based on chemical control, chemical pesticide instant effect, but conventional pesticide controlling object is single, various pests needs repeatedly dispenser to prevent and treat, not only time-consuming, recruitment shipwreck, cost accounting is high, but also easily cause insect to develop immunity to drugs, residue of pesticide, contaminated environment and killed natural enemies, increase difficulty of prevention and cure.Therefore, development composite highly effective low toxicity novel agrochemical formula is the harm of science bridle Sugarcane Pests, guarantees sugared industry sustainable and stable development problem demanding prompt solution.
Summary of the invention
The object of the invention is to occur for sugarcane moth borer, woolly aphid mixing, emergence period is long, harm is rampant and lack again the industrial technology problem of the novel pesticide control of high-efficiency low-toxicity, and provides a kind of prevention and control sugarcane moth borer, woolly aphid remarkably productive and economic benefit, composite highly effective insecticide profitable on ecology and preparation method thereof.
For realizing the object of the invention, technical scheme of the present invention is as follows:
1. the insecticide of a containing chlorantraniliprole and carbosulfan, its active ingredient is Rynaxypyr and carbosulfan, and described Rynaxypyr is 10 ~ 20%, and carbosulfan is 5 ~ 10%, all the other are auxiliary agent, described auxiliary agent is respectively wetting agent 2 ~ 5%, dispersant 3 ~ 8%, anticaking agent 1 ~ 2%, defoamer 1 ~ 2%, suspending agent 0.5 ~ 1%, filler 64 ~ 66%, described percentage is mass fraction.
2, a kind of containing chlorantraniliprole described in technical scheme 1 and the insecticide of carbosulfan, wetting agent described in it is lauryl sodium sulfate, dodecyl sodium sulfate or pulls open powder, described dispersant is calcium lignosulfonate, sodium lignin sulfonate, polyvinyl alcohol or sodium phosphate trimer, described anticaking agent is white carbon, described defoamer is organosilicon, described suspending agent is JY-3, and described filler is kaolin, potter's clay or diatomite.
3, a method for producing insecticide for containing chlorantraniliprole and carbosulfan, comprises the following steps:
(1), after weighing by each component in the insecticide of the containing chlorantraniliprole described in technique scheme 1 or 2 and carbosulfan and proportioning consumption thereof, each component to be added in mixer just mixing 30 minutes;
(2) mixed material is added in airslide disintegrating mill make 300 ~ 400 order fine powders;
(3) add again in mixer and mix 30 minutes, namely make mixed powder quantitative package and namely obtain described containing chlorantraniliprole and the insecticide of carbosulfan.
4, a kind of containing chlorantraniliprole described in technical scheme 1 or 2 and the insecticide of carbosulfan are in the application preventing and treating sugarcane moth borer and sugar cane cottony aphid.
5, the insecticide of a kind of containing chlorantraniliprole and carbosulfan described in technical scheme 4 is in the application preventing and treating sugarcane moth borer and sugar cane cottony aphid, it is characterized in that: respectively at 3 ~ April 1st generation, 2nd generation snout moth's larva egg hatching contains phase and the sugarcane grand period of growth in 7 ~ August, evenly sprays in sugarcane foliage each once with insecticide 1500 times of liquid of a kind of containing chlorantraniliprole described in technical scheme 1 or 2 and carbosulfan.
Compared with prior art, the invention has the beneficial effects as follows:
1, two kinds of active ingredient Rynaxypyrs contained by insecticide of the present invention and carbosulfan are had complementary advantages, preparation rationally, overcome pest resistance to insecticide, expand insecticidal spectrum, but also significantly reducing times for spraying and pesticide dosage, spraying times reduces by 50%, reduces production cost, compared with prior art, unforeseeable technique effect is created to the control of sugarcane borer pest and sugar cane cottony aphid.Adopt insecticide of the present invention only need use twice, in 3 ~ April 1st generation, 2nd generation snout moth's larva egg hatching contain the phase, evenly spray in sugarcane foliage with insecticide of the present invention 1500 times of liquid, can effectively control Seedling of Sugarcane Under Water Stress borer pest, control efficiency reaches more than 85%, field insect population radix can be forced down simultaneously, alleviate later stage harm; Spray in the 7-8 month sugarcane grand period of growth, effectively can control sugar cane cottony aphid, preventive effect reaches more than 95%, simultaneously double controlled the 3rd generation, the 4th generation sugarcane moth borer bore moth harm sugarcane stem, control efficiency reaches more than 85%.The spraying times of prior art control sugarcane borer pest is 2 times, the spraying times of control sugar cane cottony aphid is 2 times, totally 4 dispensers, compare, present invention significantly reduces spraying times and pesticide dosage, spraying times reduces by 50%, save production cost, decrease the pollution to environment, create significant economic benefit and ecological benefits, also improve control efficiency simultaneously, efficiently solve sugarcane moth borer, woolly aphid mixing occurs, emergence period is long, endangers industrial technology problem that is rampant and the novel pesticide control of shortage high-efficiency low-toxicity again.
2, not only a medicine is multiplex for product of the present invention, prevents, controls and take into account, decrease spraying times, and easy to use, saves labour, to the infringement of ecotope with pollute little.
3, raw material of the present invention is sufficient, and production method is simple, produces, energy saving standard in production of the present invention without waste water, waste residue, waste gas, has efficient, low toxicity, economy, environmental protection, safe superperformance.
Embodiment
In each insecticidal formulation of the present invention of following examples, each component all can buy from commercial channel.
Embodiment 1 insecticidal formulation of the present invention
See Table 1-Table 3 for insecticidal formulation of the present invention.
Table 120% Rynaxypyr carbosulfan wettable powder agent prescription 1
| Component | Content (mass percent %) |
| Rynaxypyr | 10 |
| Carbosulfan | 10 |
| Lauryl sodium sulfate | 5 |
| Sodium lignin sulfonate | 8 |
| White carbon | 1.5 |
| Organosilicon | 1 |
| JY-3 | 0.5 |
| Kaolin | 64 |
Table 223% Rynaxypyr carbosulfan wettable powder agent prescription 2
| Component | Content (mass percent %) |
| Rynaxypyr | 16 |
| Carbosulfan | 7 |
| Dodecyl sodium sulfate | 3.7 |
| Calcium lignosulfonate | 5 |
| White carbon | 1 |
| Organosilicon | 1.5 |
| JY-3 | 0.8 |
| Potter's clay | 65 |
Table 325% Rynaxypyr carbosulfan wettable powder agent prescription 3
| Component | Content (mass percent %) |
| Rynaxypyr | 20 |
| Carbosulfan | 5 |
| Lauryl sodium sulfate | 2 |
| Polyvinyl alcohol | 3 |
| White carbon | 2 |
| Organosilicon | 1 |
| JY-3 | 1 |
| Diatomite | 66 |
Embodiment 2 preparation method of the present invention
The method for producing insecticide of a kind of containing chlorantraniliprole of the present invention and carbosulfan, comprises the following steps:
(1) after in the Rynaxypyr carbosulfan wettable powder agent prescription of filling a prescription described in 1 by table 1 in embodiment 1, each component and proportioning consumption thereof weigh, by the just mixing 30 minutes in mixer of each component;
(2) mixed material is added in airslide disintegrating mill make 300 ~ 400 order fine powders;
(3) add again in mixer and mix 30 minutes, namely make the insecticide that namely mixed powder quantitative package obtains described containing chlorantraniliprole and carbosulfan.
Fill a prescription in embodiment 12 and the preparation method of the Rynaxypyr carbosulfan wetting powder of formula described in 3 except respectively by except each component in each formula and proportioning consumption thereof, all the other methods are identical with above-mentioned preparation method.
The application of sugarcane moth borer and sugar cane cottony aphid prevented and treated by embodiment 3 insecticide of the present invention.
Experimental field: Sugarcane Inst., Yunnan Prov. Agriculture Academy proving ground is carried out, 1 year perennial root, sugar cane breed ROC25, Planting Row Distance 1m.
Plot soil property, fertility, irrigation, management and sugarcane strain growing way are all more consistent.Sugarcane moth borer over the years, sugar cane cottony aphid endanger heavier.
Test medicine is that table 1 in embodiment 1,2,3 is filled a prescription the preparation made, and often process 4 times and repeat, random district group arranges, plot area 66m
2(6m × 10 row).
In March 1st generation, 2nd generation snout moth's larva egg hatching contains the phase, evenly spray in sugarcane foliage once with insecticide of the present invention 1500 times of liquid, can effectively control Seedling of Sugarcane Under Water Stress borer pest, control efficiency reaches more than 85%, simultaneously can force down field insect population radix, alleviates later stage harm; Spray once in the sugarcane grand period of growth in July, effectively can control sugar cane cottony aphid, preventive effect reaches more than 95%, simultaneously double controlled the 3rd generation, the 4th generation sugarcane moth borer bore moth harm sugarcane stem.Insecticide of the present invention is total to dispenser 2 times, within 30 days after each medicine, carries out preventive effect investigation.
Seedling of Sugarcane Under Water Stress borer pest: investigation records each community sugarcane seedling sum and borer pest withered heart seedling number respectively, then calculates the withered heart rate of borer pest and control efficiency;
3rd, the 4th generation sugarcane moth borer brill moth harm sugarcane stem: every community random searching 30 strain, records the total joint number of every strain and borer pest joint number respectively, then calculates borer pest strain rate, borer pest joint rate and control efficiency.
The withered heart rate of borer pest in seedling stage (%)=[borer pest withered heart seedling number/investigate total seedling number] × 100
Later stage borer pest strain rate (%)=[borer pest strain number/investigate total strain number] × 100
Later stage borer pest joint rate (%)=[borer pest joint number/investigate total joint number] × 100
Sugar cane cottony aphid: investigation records each community sugarcane strain sum and have aphid strain number respectively, calculates having worm strain rate and control efficiency.
Woolly aphid having worm strain rate (%)=[have worm strain number/investigate total strain number] × 100
Experimental result is as shown in table 4:
Table 4 insecticide of the present invention and the test effect contrasted
As can be seen from Table 4, insecticide of the present invention 1500 times of liquid evenly spray in sugarcane foliage, prevent, control and take into account, only need 3 ~ April 1st generation, 2nd generation snout moth's larva egg hatching contains the phase and the sugarcane grand period of growth in 7 ~ August respectively sprays once, to Seedling of Sugarcane Under Water Stress borer pest, sugar cane cottony aphid and the 3rd generation, the 4th generation sugarcane moth borer bore moth harm sugarcane stem all there is special control efficiency significantly.Product one medicine of the present invention is multiplex, spraying times 50% is reduced than prior art, save production cost, decrease the pollution to environment, create significant economic benefit and ecological benefits, efficiently solve sugarcane moth borer, woolly aphid mixing occurs, the emergence period is long, endangers industrial technology problem that is rampant and the novel pesticide control of shortage high-efficiency low-toxicity again.
Claims (6)
1. the insecticide of a containing chlorantraniliprole and carbosulfan, it is characterized in that: its active ingredient is Rynaxypyr 10% and carbosulfan 10%, auxiliary agent is: lauryl sodium sulfate 5%, sodium lignin sulfonate 8%, white carbon 1.5%, organosilicon 1%, JY-3 is 0.5%, kaolin 64%, described percentage is mass fraction.
2. the insecticide of a containing chlorantraniliprole and carbosulfan, it is characterized in that: its active ingredient is Rynaxypyr 16% and carbosulfan 7%, auxiliary agent is: dodecyl sodium sulfate 3.7%, calcium lignosulfonate 5%, white carbon 1%, organosilicon 1.5%, JY-3 is 0.8%, potter's clay 65%, described percentage is mass fraction.
3. the insecticide of a containing chlorantraniliprole and carbosulfan, it is characterized in that: its active ingredient is Rynaxypyr 20% and carbosulfan 5%, auxiliary agent is: lauryl sodium sulfate 2%, polyvinyl alcohol 3%, white carbon 2%, organosilicon 1%, JY-3 is 1%, diatomite 66%, described percentage is mass fraction.
4. a method for producing insecticide for containing chlorantraniliprole and carbosulfan, comprises the following steps:
(1), after weighing by each component in the insecticide of a kind of containing chlorantraniliprole described in claim 1 or 2 or 3 and carbosulfan and proportioning consumption thereof, each component to be added in mixer just mixing 30 minutes;
(2) mixed material is added in airslide disintegrating mill make 300 ~ 400 order fine powders;
(3) add again in mixer and mix 30 minutes, namely make mixed powder quantitative package and namely obtain described containing chlorantraniliprole and the insecticide of carbosulfan.
5. a kind of containing chlorantraniliprole described in claim 1 or 2 or 3 and the insecticide of carbosulfan are in the application preventing and treating sugarcane moth borer and sugar cane cottony aphid.
6. the insecticide of a kind of containing chlorantraniliprole according to claim 5 and carbosulfan is in the application preventing and treating sugarcane moth borer and sugar cane cottony aphid, it is characterized in that: respectively at 3 ~ April 1st generation, 2nd generation snout moth's larva egg hatching contains phase and the sugarcane grand period of growth in 7 ~ August, sprays in sugarcane foliage each once with insecticide 1500 times of liquid of the containing chlorantraniliprole described in claim 1 or 2 or 3 and carbosulfan.
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| CN106614675A (en) * | 2016-12-16 | 2017-05-10 | 张宗斌 | Pesticide composition for preventing and controlling thrips of mangoes |
| CN108812651A (en) * | 2018-08-29 | 2018-11-16 | 南通汇平高分子新材料有限公司 | Dedicated low-foam wetting agents composition and preparation method thereof for pesticide WDG/WP |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008072783A1 (en) * | 2006-12-14 | 2008-06-19 | Ishihara Sangyo Kaisha, Ltd. | Pesticidal compositions |
| CN101366388A (en) * | 2008-09-25 | 2009-02-18 | 浙江省农业科学院 | Complex insecticide of fipronil and carbosulfan |
| CN102626068A (en) * | 2012-03-29 | 2012-08-08 | 广西田园生化股份有限公司 | Ultra-low-volume liquid containing cyantraniliprole and carbamate pesticide |
| CN103503896A (en) * | 2012-12-05 | 2014-01-15 | 江苏辉丰农化股份有限公司 | Insecticide composition having synergistic effect |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2008072783A1 (en) * | 2006-12-14 | 2008-06-19 | Ishihara Sangyo Kaisha, Ltd. | Pesticidal compositions |
| CN101366388A (en) * | 2008-09-25 | 2009-02-18 | 浙江省农业科学院 | Complex insecticide of fipronil and carbosulfan |
| CN102626068A (en) * | 2012-03-29 | 2012-08-08 | 广西田园生化股份有限公司 | Ultra-low-volume liquid containing cyantraniliprole and carbamate pesticide |
| CN103503896A (en) * | 2012-12-05 | 2014-01-15 | 江苏辉丰农化股份有限公司 | Insecticide composition having synergistic effect |
Non-Patent Citations (1)
| Title |
|---|
| 双酰胺类杀虫剂应用现状;郑雪松 等;《农药》;20120810;第51卷(第8期);参见第554-557页 * |
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