CN103741536A - Manufacturing method of ramie paper - Google Patents
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- CN103741536A CN103741536A CN201410020734.6A CN201410020734A CN103741536A CN 103741536 A CN103741536 A CN 103741536A CN 201410020734 A CN201410020734 A CN 201410020734A CN 103741536 A CN103741536 A CN 103741536A
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Abstract
The invention discloses a manufacturing method of ramie paper. The method has the advantages that the ramie (bast) is used as the raw material, and the paper is manufactured by the traditional manual methods of ramie sun and rain bleaching, microorganism fermentation and degumming, processing of natural paper medicines, dying of plant pigments, and the like, so the damage to the plant fiber is avoided, the quality of paper products is furthest improved, and the wastes generated in the whole technological process can be completely degraded, thereby realizing the non-toxic, non-harmful and pollution-free effects and meeting the national environment-protection standards; the manufactured ramie paper has the characteristics of classic elegance, high flexibility, softness and attractive appearance, is suitable for the restoration of ancient rare books and the creation of calligraphy and drawing, and can reach the better effect of non-decay for thousands of years; the technical standard is normative, so the method is suitable for factory production, and the good economic benefits and social benefits are realized.
Description
Technical field
The present invention relates to traditional technology for making paper field, be specifically related to a kind of preparation method of ramie paper.
Background technology
China plants and uses the with a long history of ramie, weaves in the < < Book of Songs king wind > of The Spring and Autumn Period (B.C. 770～476 years) > and records: " in mound, have fiber crops." the old wind > of < < Book of Songs > record: " pond at east gate, can retted fibre." according to historical data and relevant expert's textual criticism, papermaking originates from the wadding that floats of spinning cotton and weaving cloth and producing, and has again substantial connection with retted fibre.According to the bright < < of the Southern Dynasties's model book Cai Lun of the Later Han Dynasty, passing > > records: " evidence, compiles with bamboo slip used for writing on during ancient times more from ancient times; It is with fine silk (thin thin,tough silk) silks person, meaning be paper.Expensive and the simple weight of fine silk, and be not easy to people.Human relations are to make meaning, with tree skin, fiber crops head and worn-out cloth, fishing net, think paper." ancient times the ordinary people overwhelming majority wear ramie cloth (being grass cloth) clothes, fishnet is also ramie fabric, therefore, the main raw material of using during Cai Lun papermaking is originally ramie.
The feature of ramie is that fiber is long, and filament length is 60～250mm.Content is high, is 65～75%, and above two indexs are optimum in crudefiber crop; Lignin few (0.8～2%), pectin appropriate (3～6%), is easier to so make paper pulp ratio, pliable and tough prolonged after one-tenth paper, is described as " longevity paper in thousand ".Therefore, ramie paper also just becomes one of main paper using of Chinese ancient books ancient books and records.In addition, have thickness irregular " horizontal joint line " on ramee cell membrane, or implied or is existing, this natural speciality makes ramie paper performance ink and wash effect excellent, thereby the Shen Shou successive dynasties men of literature and writing are liked always.The cursive script < < that calligraphy the earliest handed down from ancient times so far---Palace Museum is hidden writer in Western Jin Dynasty land machine calms down note > >, through expert, repeatedly check, confirm that this note is early stage numb paper; Rice well-known calligraphist in very small < < history of books > > textual criticism ancient times writes copybook paper using, and the Wei Jin Northern and Southern Dynasties overwhelming majority is numb paper (take ramie paper as main); Near the Han dynasty Xuan Quan sugar water well of Dunhuang, Gansu Province puts ruins and finds that after the ancient paper of 460 multi-discs, historical relic magazine the 5th phase in 2000 delivers brief report on the excavation and claims, these ancient paper great majority are ramie paper.Though go through over thousands ofly year, also do not become fragile, variable color; The multiplex numb paper of books during Sui and Tang dynasty and five dynasties (rubbings mounting) (take ramie paper as main), during Song Yuan, because ramie must be made way for weaving dress ornament demand, and paper making raw material increases, not in the highest flight, bright when clear the use of ramie paper more rare.
Ramie paper is made skill by hand and is rarely had literature record from ancient times, even if few places is still being produced so far, but because of reasons such as technical standard are lack of standardization, paper product quality is very different, is absorbed in and is on the verge of lost predicament.
Current, in paper-making process, a large amount of bamboo wood resources that consume, are on the rise to the destruction of ecological environment.China's bamboo wood resource owning amount is few, and the ramie Que China that is commonly called as " China's grass " is widely distributed, and plants with a long history.Ramie is perennial root draft crop, plants fiber crops once, can perennation.And because power of regeneration is strong, within 1 year, can gather in three to the four seasons.Therefore, invention ramie paper preparation method has wide market prospects, and huge social benefit.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of ramie paper, to solve the problem proposing in above-mentioned background technology.
Technical problem solved by the invention realizes by the following technical solutions:
A preparation method for ramie paper, comprises the following steps:
(1) get the raw materials ready: ramie peel is peeled off from straw, removed rascal, outdoor exposing to the sun and rain 2～3 months;
(2) soak fiber crops: the ramie peel after exposing to the sun and rain is put into retted fibre pond, soak 8～10 days, for reaching the object of coming unstuck, before immersion, add Alkaliphilic bacillus preparation, make ramie peel carry out microorganism fermentation, in order to obtain clean ramee, in immersion process, need often to change water;
(3) processing: the ramie peel that will wet cuts sub-wire, makes its width be not more than 0.1cm, the little 1cm of length, while cutting fiber crops, rejects impurity and the rots such as blade of grass, grass joint, wood chip at any time, and the ramie peel after cutting is pounded and is smash into mud paste;
(4) washing: ramie slurry is put into kitchen sink again, repeatedly rinse with clear water, until the foreign material such as the grains of sand, dust are all removed;
(5) ash grinds: ramie slurry is with directly pounding and smash after grey water saturates;
(6) stack retting: the ramie slurry of smashing of pounding soaks 3-4 hour with plant ash in retted fibre pond, banks up subsequently, above covers Polypropylence Sheet, makes it pile fermentation under hyther and comes unstuck;
(7) boiling: the ramee bundle after fermentation is loosely put into steamer boiling, boiling for the first time 6～8 hours, then in the mellow lime liquid that is 5% in concentration, soak, again carry out thermophilic digestion after immersion, method is with for the first time, time is 3～4 hours, boil rear water jaundice, the rotten to the corn one-tenth of fiber crops material is cotton-shaped, through the boiling of alkali lye, the impurity such as the lignin in raw material, natural gum, resin are removed, and through material picking, can become paper stock;
(8) washing: take out well-done ramie paper stock and put into clear water and clean, by the liquid being mingled with in paper pulp and boil and expect that dissolved matter etc. is substantially clean, the ramie paper pulp after washing soaks in water again;
(9) carefully grind: paper stock is pounded and smash in batches, and the stirring while smashing, beats until paper stock becomes screened stock shape, fiber half is separated, expect very soft, till entering water and can scattering completely;
(10) washing: after pounding and smashing, pie ramie paper stock is washed, remove the earth carried secretly, the grains of sand together with other filler;
(11) decolouring: after ramie paper stock is smash, washed through pounding, present greyish white cotton-shapedly to silvery white brocade, finally decolour with the limewash that concentration is 5～10% in pond in decolouring;
(12) slurrying: the ramie slurry after decolouring is poured into and is marked with the dragging in paper groove of clear water, add Sunset Abelmoschus Root mucus (paper medicine), gum rosin (natural plant gum); Alum (precipitating agent), carries out rod and stirs, and fiber is fully disperseed also floating, and the ramee silk silk in liquid stream is connected, and the suspension that these denseness are suitable be paper pulp;
(13) drag for paper: first smooth being placed on of bamboo curtain splint dragged for above paper frame, drag for paper frame extrapolated, need enter pulp suspension (not having water 6～8cm) completely, allow ramee divide equably on bamboo curtain splint, form very thin one deck l Water Paper page, get final product water outlet, during water outlet, shaken 2～3 times, after water outlet, stop 3～5 seconds, then l Water Paper is displaced on l Water Paper frame;
(14) squeezing: cover Kanakin above accumulating l Water Paper page, along periphery, place the plank that a layer thickness is greater than 3cm, utilize capstan winch to exert pressure equably, the water in paper is flowed out lentamente, while by the time not there are flowing out on l Water Paper frame, just capstan winch can be unclamped;
(15) roasting paper: by gluing and be placed on bright and clean baking wall immediately after individual separation of paper after squeezing, make its " cold roasting " air dry;
(16) take off paper: the dried paper of cold roasting lies in to scald on paper machine and plates, and cuts;
(17) coating: talcum powder is fine ground, put into water furnishing suspension, then boil altogether with starch, with spread pen, be coated with and impose on paper;
(18) calendering: by talcum flat wiping 50～60 times repeatedly back and forth from top to bottom gently on paper, make paper calendering, obtain ramie paper.
In step (2), the mass ratio of described ramie peel and Alkaliphilic bacillus preparation is 100:.
In step (12), the mass ratio of described ramie slurry, Sunset Abelmoschus Root mucus, gum rosin, alum is 60:6:3:2.
In step (17), the mass ratio of described water, talcum powder, starch is 10:20:1.
Compared with prior art, beneficial effect of the present invention:
The ramie paper that the inventive method is made has advantages of traditional-handwork paper processed, and applicable standardization, large-scale production, has good economic benefit and social benefit.Technological process, technology standardization have solved that traditional-handwork ramie paper product matter is very different, manufacture skill is on the verge of lost problem; With ramie, to substitute bamboo carpentery workshop be paper making raw material, solved the problem that modern paper expends the forest reserves in a large number; And the discarded object that whole technological process produces can be degradable, reaches nontoxic, harmless, pollution-free, meets national environmental standard, therefore the problem of paper-making industry serious environment pollution is readily solved.
The specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is only the present invention's part embodiment, rather than whole embodiment.Embodiment based in the present invention, those of ordinary skills, not making the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment
A preparation method for ramie paper, comprises the following steps:
(1) get the raw materials ready: ramie peel is peeled off from straw, removed rascal, outdoor exposing to the sun and rain 2～3 months; The ramee that contains moisture is subject to daylight middle-ultraviolet lamp and irradiates the ozone strong oxidizing effect producing, lignin residual in ramie material bleaches slurry through oxidation, owing to not using chlorine bleaches, again to carry out under the reaction condition relaxing simultaneously, cellulose is non-degradable, so the paper of making has advantages of durability and do not have contaminated environment;
(2) soak fiber crops: get 200 kilograms of ramie peels and put into retted fibre pond, soak 8～10 days, before immersion, add 2000g Alkaliphilic bacillus preparation, make ramie peel carry out microorganism fermentation, reach the object of coming unstuck, in order to obtain clean ramee, in immersion process, need often to change water;
(3) processing: the ramie peel that will wet cuts sub-wire, make its width be not more than 0.1cm, the little 1cm of length, while cutting fiber crops, reject at any time impurity and the rots such as blade of grass, grass joint, wood chip, the modes such as manpower, water-powered trip-hammer, stone stone roller for ramie peel after cutting are pounded and are smash into mud paste;
(4) washing: ramie slurry is put into kitchen sink again, repeatedly rinse with clear water, until the foreign material such as the grains of sand, dust are all removed;
(5) ash grinds: ramie slurry is with directly pounding and smash after grey water saturates;
(6) stack retting: ramie slurry soaks 3-4 hour with plant ash in retted fibre pond, banks up subsequently, above covers Polypropylence Sheet, makes it pile fermentation under hyther and comes unstuck, and within 30 days, completes;
(7) boiling: at the cylindrical shape specialty digester (of 1.5～2 meters of diameters Huang bucket), ramee bundle after fermentation is loosely piled to 2/3 of steamer, at pot upper cover Polypropylence Sheet, to keep temperature, boiling for the first time 6～8 hours, in the mellow lime liquid that taking-up is 5% in concentration, soak after 30 minutes, again carry out thermophilic digestion, method is with for the first time, and the time is 3～4 hours, boil rear water jaundice, the rotten to the corn one-tenth of fiber crops material is cotton-shaped.Through the boiling of alkali lye, the impurity such as the lignin in raw material, natural gum, resin are removed, and through material picking, can become paper stock;
(8) washing: take out well-done ramie paper stock and put into clear water, hold and swing back and forth with hook, the liquid being mingled with in paper pulp and to boil material dissolved matter etc. substantially clean, the ramie paper pulp after washing also need soak 24 hours in water;
(9) carefully grind: paper stock is pounded and smash by modes such as artificial, water-powered trip-hammer, stone stone rollers in batches, and the stirring while smashing, pounds at every turn and smash paper stock 1500g, 30 minutes, can obtain pie paper pulp, beat until paper stock becomes screened stock shape at every turn, fiber half is separated, expect very soft, till entering water and can scattering completely;
(10) washing: after pounding and smashing, pie ramie paper stock is put into bottom for pointed bamboo basket, it is erected in pond, with hand, inside stir continuously until evenly, bamboo basket is rocked in rotation simultaneously, every basket of paper stock need wash 10～15 minutes, and the earth of carrying secretly like this, the grains of sand have just been cleaned totally together with other filler, obtain clean ramie slurry after drainage;
(11) decolouring: after ramie paper stock is smash, washed through pounding, present greyish white cotton-shapedly to silvery white brocade, first finally decolour with the limewash that concentration is 5～10% in decolouring pond, the time is 60 minutes;
(12) slurrying: inject the clear water of 3/4 volume in dragging for paper groove, the ramie slurry after about 30 kilograms decolourings is poured into, add 3000g Sunset Abelmoschus Root mucus (paper medicine), 1500g gum rosin (natural plant gum); 1000g alum (precipitating agent), then stir 30 minutes with wooden stick, fiber is fully disperseed also floating, the ramee silk silk in liquid stream is connected, and the suspension that these denseness are suitable be paper pulp;
(13) drag for paper: first smooth being placed on of bamboo curtain splint dragged for above paper frame, drag for paper frame extrapolated, need enter pulp suspension (not having water 6～8cm) completely, allow ramee divide equably on bamboo curtain splint, form very thin one deck l Water Paper page, get final product water outlet, during water outlet, shaken 2～3 times, after water outlet, stopped 3～5 seconds, the bamboo curtain splint that dragged for paper pulp is layered on the other l Water Paper frame of copy paper groove, then carefully promptly mention bamboo curtain splint, l Water Paper has just been displaced on l Water Paper frame;
(14) squeezing: when the l Water Paper page of manufacturing paper with pulp is accumulated to 1000, cover Kanakin in the above, along periphery, place the plank that a layer thickness is greater than 3cm, utilize capstan winch to exert pressure equably, water in paper is flowed out lentamente, the time of draining is 2 hours, while by the time not there are flowing out (moisture is 70%) on l Water Paper frame, just capstan winch can be unclamped;
(15) roasting paper: the edge of l Water Paper is firmly twisted with the fingers, then take gently paper angle off, again entire paper is peeled, the paper of taking off is sticky being placed on bright and clean baking wall immediately, piled up one deck, from the downward 5cm in top of paper, pile up again one deck, the like again pile up after piling up 5～6 layers, make its " cold roasting " air dry.In 2 days seasons of spring and autumn, the time in summer is short, and the time in winter is long;
(16) take off paper: after paper dries, first uncover one jiao, then take off from shining paper wall, lie in to scald on paper machine and plate, cutting;
(17) coating: 500g talcum powder is fine ground, put into 25 kg of water furnishing suspension, then boil altogether with 250g starch, with spread pen, be coated with and impose on paper;
(18) calendering: by talcum flat wiping 50～60 times repeatedly back and forth from top to bottom gently on paper, make paper calendering, obtain ramie paper.
Ramie paper claims " jute paper " after the dyeing of cork tree juice, and the person of being unstained is " hemp paper ".As being coated with yellow wax on " jute paper ", be " firmly yellow ", on " hemp paper ", being coated with Chinese wax is " firmly white ".
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and in the situation that not deviating from spirit of the present invention or essential characteristic, can realize the present invention with other concrete form.Therefore, no matter from which point, all should regard embodiment as exemplary, and be nonrestrictive, scope of the present invention is limited by claims rather than above-mentioned explanation, is therefore intended to include in the present invention dropping on the implication that is equal to important document of claim and all changes in scope.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should make description as a whole, and the technical scheme in each embodiment also can, through appropriately combined, form other embodiments that it will be appreciated by those skilled in the art that.
Claims (4)
1. a preparation method for ramie paper, is characterized in that, comprises the following steps:
(1) get the raw materials ready: ramie peel is peeled off from straw, removed rascal, outdoor exposing to the sun and rain 2～3 months;
(2) soak fiber crops: the ramie peel after exposing to the sun and rain is put into retted fibre pond, soak 8～10 days, for reaching the object of coming unstuck, before immersion, add Alkaliphilic bacillus preparation, make ramie peel carry out microorganism fermentation, in immersion process, need often to change water;
(3) processing: the ramie peel that will wet cuts sub-wire, makes its width be not more than 0.1cm, the little 1cm of length, the ramie peel after cutting is pounded and is smash into mud paste;
(4) washing: ramie slurry is put into kitchen sink again, repeatedly rinse with clear water, until the foreign material such as the grains of sand, dust are all removed;
(5) ash grinds: ramie slurry is with directly pounding and smash after grey water saturates;
(6) stack retting: the ramie slurry of smashing of pounding soaks 3-4 hour with plant ash in retted fibre pond, banks up after immersion finishes, and makes it pile fermentation under hyther and comes unstuck;
(7) boiling: the ramee bundle after fermentation is loosely placed on to boiling on steamer, and boiling for the first time 6～8 hours, soaks in the mellow lime liquid that is then 5% in concentration, again carries out thermophilic digestion after immersion, method is with for the first time, and the time is 3～4 hours;
(8) washing: take out well-done ramie paper stock and put into clear water and clean, by the liquid being mingled with in paper pulp and boil the removal of material dissolved matter, and the ramie paper after washing is put into water and soak;
(9) carefully grind: paper stock is pounded and smash in batches, and the stirring while smashing, beats until paper stock becomes screened stock shape, fiber half is separated, expect very soft, till entering water and can scattering completely;
(10) washing: after pounding and smashing, pie ramie paper stock is washed, remove the earth carried secretly, the grains of sand together with other filler;
(11) decolouring: finally decolour with the limewash that concentration is 5～10% in decolouring pond;
(12) slurrying: the ramie slurry after decolouring is poured into and is marked with the dragging in paper groove of clear water, add Sunset Abelmoschus Root mucus (paper medicine), gum rosin (natural plant gum); Alum (precipitating agent), stirs with wooden stick, ramee is fully disperseed also floating;
(13) drag for paper: first smooth being placed on of bamboo curtain splint dragged for above paper frame, drag for paper frame extrapolated, enter pulp suspension completely, allow ramee divide equably on bamboo curtain splint, form very thin one deck l Water Paper page, get final product water outlet, during water outlet, shaken 2～3 times, after water outlet, stop 3～5 seconds, then l Water Paper is displaced on l Water Paper frame;
(14) squeezing: cover Kanakin above accumulating l Water Paper page, place along periphery the plank that a layer thickness is greater than 3cm, utilize capstan winch to exert pressure equably, the water in paper is flowed out lentamente, while by the time not there are flowing out on l Water Paper frame, just capstan winch can be unclamped;
(15) roasting paper: by gluing and be placed on bright and clean baking wall immediately after individual separation of paper after squeezing, make its " cold roasting " air dry;
(16) take off paper: the dried paper of cold roasting lies in to scald on paper machine and plates, and cuts;
(17) coating: talcum powder is fine ground, put into water furnishing suspension, then boil altogether with starch, with spread pen, be coated with and impose on paper;
(18) calendering: by talcum flat wiping 50～60 times repeatedly back and forth from top to bottom gently on paper, make paper calendering, obtain ramie paper.
2. the preparation method of a kind of ramie paper according to claim 1, is characterized in that, in step (2), the mass ratio of described ramie peel and Alkaliphilic bacillus preparation is 100:1.
3. the preparation method of a kind of ramie paper according to claim 1, is characterized in that, in step (12), the mass ratio of described ramie slurry, Sunset Abelmoschus Root mucus, gum rosin, alum is 60:6:3:2.
4. the preparation method of a kind of ramie paper according to claim 1, is characterized in that, in step (17), the mass ratio of described water, talcum powder, starch is 10:20:1.
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| CN109778579A (en) * | 2018-12-19 | 2019-05-21 | 中国宣纸股份有限公司 | A kind of fibrous raw material of Xuan paper wingceltis skin steps on skin technique |
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| CN105951487A (en) * | 2016-05-20 | 2016-09-21 | 山西朱好古麻笺纸业有限公司 | Preparation method for jute paper by utilizing jute as raw material |
| CN106012632A (en) * | 2016-05-20 | 2016-10-12 | 山西朱好古麻笺纸业有限公司 | Method for making hemp paper from hemp |
| CN105803853A (en) * | 2016-05-25 | 2016-07-27 | 江苏金沃机械有限公司 | Insect-resistant pulp and preparation method and application thereof |
| CN105951500A (en) * | 2016-05-25 | 2016-09-21 | 江苏金沃机械有限公司 | Paper pulp taking amygdalus comnnis husks as raw materials and preparation method of paper pulp |
| CN106012664A (en) * | 2016-05-25 | 2016-10-12 | 江苏金沃机械有限公司 | Paper pulp taking walnut shells as raw materials |
| CN106012651A (en) * | 2016-05-25 | 2016-10-12 | 江苏金沃机械有限公司 | Insect-resistant paper pulp for preparing corrugated boards and preparation method and application thereof |
| CN107254799A (en) * | 2017-07-04 | 2017-10-17 | 吉林化工学院 | A kind of preparation method of environment-friendly type Foreign Trade Logistics waybill label |
| CN107254799B (en) * | 2017-07-04 | 2019-02-22 | 吉林化工学院 | A kind of preparation method of environment-friendly type Foreign Trade Logistics waybill label |
| CN109778579A (en) * | 2018-12-19 | 2019-05-21 | 中国宣纸股份有限公司 | A kind of fibrous raw material of Xuan paper wingceltis skin steps on skin technique |
| CN110130145A (en) * | 2019-04-28 | 2019-08-16 | 郑智源 | The production method of sheep brain writing paper |
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| CN113605120A (en) * | 2021-07-29 | 2021-11-05 | 复旦大学 | Method for making calabash vine paper |
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| CN116791405A (en) * | 2023-07-12 | 2023-09-22 | 中国制浆造纸研究院有限公司 | Writing brush painting paper and manufacturing method thereof |
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