CN103741170B - One is prepared rare earth metal and is beaten arc electrolysis all-in-one oven - Google Patents
One is prepared rare earth metal and is beaten arc electrolysis all-in-one oven Download PDFInfo
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- CN103741170B CN103741170B CN201410017684.6A CN201410017684A CN103741170B CN 103741170 B CN103741170 B CN 103741170B CN 201410017684 A CN201410017684 A CN 201410017684A CN 103741170 B CN103741170 B CN 103741170B
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Abstract
The present invention relates to one to prepare rare earth metal and beat arc electrolysis all-in-one oven, comprising: stove seat; Electrolysis body of heater, it is arranged on described stove seat; Elevating and rotating machine, its lifting rotation bar is arranged on and closes on described electrolysis body of heater side; First crossbeam and second cross beam, its one end is enclosed within the turning axle of described lifting rotation bar successively at upper and lower, and forms certain angle in the horizontal direction each other; Cathode bar, its one end is articulated in the other end of described first crossbeam; Play arc rod, its one end is articulated in the other end of described second cross beam; Temperature sensor, it is arranged in described electrolysis body of heater, for sensing the temperature of described electrolysis body of heater; Controller, its with described elevating and rotating machine, temperature sensor, play arc rod and to be electrically connected and electrolysis body of heater is electrically connected, the invention solves current body of heater to need when beating arc, separately to move the problem that dozen arc equipment carries out beating arc time and effort consuming from other places, reach energy-saving and cost-reducing object.
Description
Technical field
The present invention relates to re metal electrolyzing apparatus field, particularly relate to one and prepare rare earth metal and beat arc electrolysis all-in-one oven.
Background technology
Re metal electrolyzing method is used to extract some active metals can not produced in aqueous, as Li, Na, K, Mg, Ti, Ta, Zr etc., because this kind of method has higher ionic conductance, higher spread coefficient, lower viscosity and the advantage such as electrode reaction fast, become one of main production process of current rare earth metal, in current electrolyzer, multiplex arc rod of beating is heated to electrolysis body of heater, when electrolysis body of heater needs to heat time, the another dozen arc equipment that moves from other places carries out beating arc, such working method time and effort consuming, waste energy consumption.
Summary of the invention
In order to solve the problem, the object of this invention is to provide one and preparing rare earth metal and beat arc electrolysis all-in-one oven, comprising:
Stove seat;
Electrolysis body of heater, it is arranged on described stove seat;
Elevating and rotating machine, its lifting rotation bar is arranged on and closes on described electrolysis body of heater side;
First crossbeam and second cross beam, its one end is enclosed within the turning axle of described lifting rotation bar successively at upper and lower, and forms certain angle in the horizontal direction each other;
Cathode bar, its one end is articulated in the other end of described first crossbeam;
Play arc rod, its one end is articulated in the other end of described second cross beam;
Temperature sensor, it is arranged in described electrolysis body of heater, for sensing the temperature of described electrolysis body of heater;
Controller, itself and described elevating and rotating machine, temperature sensor, play arc rod and the electrical connection of electrolysis body of heater, when described elevating and rotating machine starts, control on certain altitude that described cathode bar is placed in described electrolysis body of heater by described lifting rotation bar, when the temperature value of described temperature sensor senses is less than default standard temperature, when then controlling described lifting rotation bar rising certain distance, described cathode bar leaves described electrolysis body of heater, control described lifting rotation bar afterwards and rotate described certain angle, then, control described lifting rotation bar decline certain distance, play arc rod described in making and enter certain altitude in described electrolysis body of heater, then control to play arc rod to start to beat arc, when described temperature sensor senses temperature value reaches described standard temperature, control described lifting rotation bar and perform the operation with said process contrary, then continue to control described electrolysis body of heater electric current, keep normal electrolysis.
Preferred version: described electrolysis body of heater is plumbago crucible material.
Preferred version: described cathode bar is pure iron rod.
Preferred version: described pure iron rod is for be close to by three poles the pole body being welded into, and inserting the degree of depth under negative electrode is 330 ~ 450mm.
The electrolysis production of the present invention electrolysis body of heater beating arc one electrolysis one, form by making arc rod, negative electrode, temperature sensor etc., wherein, electrolysis body of heater is arranged on stove seat, play arc rod, negative electrode be arranged on same lifting rotation bar, be convenient to body of heater situation abnormal time beat arc in time and heat up, then continue electrolysis, solve current body of heater to need when beating arc, separately to move the problem that dozen arc equipment carries out beating arc time and effort consuming from other places, reach energy-saving and cost-reducing object.
Accompanying drawing explanation
Fig. 1 is structural representation of the present invention.
Embodiment
Below in conjunction with embodiment, the present invention is described in further detail:
As shown in Figure 1, the present invention includes: stove seat; Electrolysis body of heater 1, it is arranged on described stove seat, and electrolysis body of heater is plumbago crucible material;
Elevating and rotating machine, its lifting rotation bar 3 is arranged on and closes on described electrolysis body of heater 1 side; First crossbeam 5 and second cross beam 6, its one end is enclosed within the turning axle of described lifting rotation bar 3 successively at upper and lower, and forms certain angle in the horizontal direction each other; Cathode bar 4, its one end is articulated in the other end of described first crossbeam 5, and described cathode bar is pure iron rod, is close to the pole body being welded into by three poles, and inserting the degree of depth under negative electrode is 330 ~ 450mm; Play arc rod 2, its one end is articulated in the other end of described second cross beam 6; Temperature sensor, it is arranged in described electrolysis body of heater 1, for sensing the temperature of described electrolysis body of heater;
Controller, itself and described elevating and rotating machine, temperature sensor, beat arc rod 2 electrical connection and electrolysis body of heater 1 be electrically connected, when described elevating and rotating machine starts, controlling described lifting rotation bar 3 is placed on the certain altitude in described electrolysis body of heater 1 by described cathode bar 4, when the temperature value of described temperature sensor senses is less than default standard temperature, then control described lifting rotation bar 3 rise certain distance time described cathode bar 4 leave described electrolysis body of heater 1, control described lifting rotation bar 3 afterwards and rotate described certain angle, then, control described lifting rotation bar 3 to decline certain distance, play arc rod 2 described in making and enter certain altitude in described electrolysis body of heater 1, then control to play arc rod 2 to start to beat arc, when described temperature sensor senses temperature value reaches described standard temperature, control described lifting rotation bar 3 and perform the operation with said process contrary, then continue to control described electrolysis body of heater 1 electric current, keep normal electrolysis.
Claims (2)
1. prepare rare earth metal and beat an arc electrolysis all-in-one oven, it is characterized in that, comprising:
Stove seat;
Electrolysis body of heater, it is arranged on described stove seat;
Elevating and rotating machine, its lifting rotation bar is arranged on and closes on described electrolysis body of heater side;
First crossbeam and second cross beam, its one end is enclosed within the turning axle of described lifting rotation bar successively at upper and lower, and forms certain angle in the horizontal direction each other;
Cathode bar, its one end is articulated in the other end of described first crossbeam, and described cathode bar is pure iron rod, and described pure iron rod is for be close to by three poles the pole body being welded into, and inserting the degree of depth under negative electrode is 330 ~ 450mm;
Play arc rod, its one end is articulated in the other end of described second cross beam;
Temperature sensor, it is arranged in described electrolysis body of heater, for sensing the temperature of described electrolysis body of heater;
Controller, itself and described elevating and rotating machine, temperature sensor, play the electrical connection of arc rod and the electrical connection of electrolysis body of heater, when described elevating and rotating machine starts, control on certain altitude that described cathode bar is placed in described electrolysis body of heater by described lifting rotation bar, when the temperature value of described temperature sensor senses is less than default standard temperature, when then controlling described lifting rotation bar rising certain distance, described cathode bar leaves described electrolysis body of heater, control described lifting rotation bar afterwards and rotate described certain angle, then, control described lifting rotation bar decline certain distance, play arc rod described in making and enter certain altitude in described electrolysis body of heater, then control to play arc rod to start to beat arc, when described temperature sensor senses temperature value reaches described standard temperature, control described lifting rotation bar and perform the operation with said process contrary, then continue to control described electrolysis body of heater electric current, keep normal electrolysis.
2. rare earth metal of preparing according to claim 1 beats arc electrolysis all-in-one oven, and it is characterized in that, described electrolysis body of heater is plumbago crucible material.
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CN201410017684.6A CN103741170B (en) | 2014-01-15 | 2014-01-15 | One is prepared rare earth metal and is beaten arc electrolysis all-in-one oven |
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CN201410017684.6A CN103741170B (en) | 2014-01-15 | 2014-01-15 | One is prepared rare earth metal and is beaten arc electrolysis all-in-one oven |
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CN103741170A CN103741170A (en) | 2014-04-23 |
CN103741170B true CN103741170B (en) | 2016-02-24 |
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Families Citing this family (3)
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CN106011947A (en) * | 2016-07-20 | 2016-10-12 | 贺州市金利新材料有限公司 | 360-degree rotating device for cathode used for electrolyzing rare earth metal |
CN106835204A (en) * | 2017-04-21 | 2017-06-13 | 包头市鑫业新材料有限责任公司 | A kind of light rare earth electrolytic metal rotary electrolysis stove |
CN110408961B (en) * | 2019-09-05 | 2021-04-23 | 中南大学 | Arc striking starting method of rare earth electrolytic cell |
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CN1936088A (en) * | 2006-09-21 | 2007-03-28 | 上海大学 | Method and apparatus for directly preparing refractory metal and alloy from metal oxide |
CN202415703U (en) * | 2011-12-28 | 2012-09-05 | 赣州科力稀土新材料有限公司 | Electrolytic cell for producing rare earth metals |
CN103290434A (en) * | 2013-04-24 | 2013-09-11 | 包头瑞鑫稀土金属材料股份有限公司 | Fused-salt electrolytic cell for producing rare earth metals and alloys |
CN103484898A (en) * | 2013-10-10 | 2014-01-01 | 宝纳资源控股(集团)有限公司 | Vacuum high-temperature continuous electrolytic furnace system and electrolytic method |
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2014
- 2014-01-15 CN CN201410017684.6A patent/CN103741170B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2002357696A (en) * | 2001-06-04 | 2002-12-13 | Toshiba Corp | Decontamination method and device for solid waste |
CN1936088A (en) * | 2006-09-21 | 2007-03-28 | 上海大学 | Method and apparatus for directly preparing refractory metal and alloy from metal oxide |
CN202415703U (en) * | 2011-12-28 | 2012-09-05 | 赣州科力稀土新材料有限公司 | Electrolytic cell for producing rare earth metals |
CN103290434A (en) * | 2013-04-24 | 2013-09-11 | 包头瑞鑫稀土金属材料股份有限公司 | Fused-salt electrolytic cell for producing rare earth metals and alloys |
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