CN103725873B - One freezes off knot ball press technique high magnesium consolidating agent and using method - Google Patents
One freezes off knot ball press technique high magnesium consolidating agent and using method Download PDFInfo
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- CN103725873B CN103725873B CN201310656635.2A CN201310656635A CN103725873B CN 103725873 B CN103725873 B CN 103725873B CN 201310656635 A CN201310656635 A CN 201310656635A CN 103725873 B CN103725873 B CN 103725873B
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- consolidating agent
- magnesium
- high magnesium
- ball press
- press technique
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- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 40
- 238000000034 method Methods 0.000 title claims abstract description 26
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 239000011777 magnesium Substances 0.000 title claims abstract description 21
- 229910052749 magnesium Inorganic materials 0.000 title claims abstract description 21
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 54
- 229910052742 iron Inorganic materials 0.000 claims abstract description 26
- 239000000463 material Substances 0.000 claims abstract description 23
- CSNNHWWHGAXBCP-UHFFFAOYSA-L Magnesium sulfate Chemical compound [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 claims abstract description 16
- 239000000470 constituent Substances 0.000 claims abstract description 11
- PNEYBMLMFCGWSK-UHFFFAOYSA-N Alumina Chemical compound [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000292 calcium oxide Substances 0.000 claims abstract description 10
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000395 magnesium oxide Substances 0.000 claims abstract description 10
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000428 dust Substances 0.000 claims abstract description 8
- 150000002500 ions Chemical class 0.000 claims abstract description 8
- 229910052943 magnesium sulfate Inorganic materials 0.000 claims abstract description 8
- 235000019341 magnesium sulphate Nutrition 0.000 claims abstract description 8
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims abstract description 6
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 claims 5
- 238000007710 freezing Methods 0.000 claims 5
- VDGJOQCBCPGFFD-UHFFFAOYSA-N oxygen(2-) silicon(4+) titanium(4+) Chemical compound [Si+4].[O-2].[O-2].[Ti+4] VDGJOQCBCPGFFD-UHFFFAOYSA-N 0.000 claims 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 17
- 235000012255 calcium oxide Nutrition 0.000 abstract description 8
- 235000012245 magnesium oxide Nutrition 0.000 abstract description 8
- 239000000843 powder Substances 0.000 abstract description 8
- 239000000377 silicon dioxide Substances 0.000 abstract description 8
- 235000012239 silicon dioxide Nutrition 0.000 abstract description 8
- 238000007596 consolidation process Methods 0.000 abstract description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract description 5
- 238000005272 metallurgy Methods 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 4
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract description 2
- 239000011593 sulfur Substances 0.000 abstract description 2
- 229910052717 sulfur Inorganic materials 0.000 abstract description 2
- 239000011499 joint compound Substances 0.000 description 7
- 238000003723 Smelting Methods 0.000 description 5
- 239000011230 binding agent Substances 0.000 description 5
- 229910052681 coesite Inorganic materials 0.000 description 4
- 229910052906 cristobalite Inorganic materials 0.000 description 4
- 238000000227 grinding Methods 0.000 description 4
- 229910052738 indium Inorganic materials 0.000 description 4
- 238000002156 mixing Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000010802 sludge Substances 0.000 description 4
- 229910052682 stishovite Inorganic materials 0.000 description 4
- 229910052905 tridymite Inorganic materials 0.000 description 4
- 229910052593 corundum Inorganic materials 0.000 description 3
- 239000008188 pellet Substances 0.000 description 3
- 229910001845 yogo sapphire Inorganic materials 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000000853 adhesive Substances 0.000 description 2
- 230000001070 adhesive effect Effects 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- AMWRITDGCCNYAT-UHFFFAOYSA-L hydroxy(oxo)manganese;manganese Chemical compound [Mn].O[Mn]=O.O[Mn]=O AMWRITDGCCNYAT-UHFFFAOYSA-L 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- ZGBSOTLWHZQNLH-UHFFFAOYSA-N [Mg].S(O)(O)(=O)=O Chemical compound [Mg].S(O)(O)(=O)=O ZGBSOTLWHZQNLH-UHFFFAOYSA-N 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000440 bentonite Substances 0.000 description 1
- 229910000278 bentonite Inorganic materials 0.000 description 1
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 150000001805 chlorine compounds Chemical group 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003500 flue dust Substances 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- FBAFATDZDUQKNH-UHFFFAOYSA-M iron chloride Chemical compound [Cl-].[Fe] FBAFATDZDUQKNH-UHFFFAOYSA-M 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 229910001629 magnesium chloride Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000012492 regenerant Substances 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000009865 steel metallurgy Methods 0.000 description 1
- 231100000167 toxic agent Toxicity 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
Abstract
The invention provides one and freeze off the knot high magnesium consolidating agent of ball press technique, including magnesium oxide, calcium oxide, magnesium sulfate, silicon dioxide, aluminium oxide and sulfur, in terms of mass parts, each constituent content is as follows: magnesium oxide is 15 45, calcium oxide is 0.5 2, and magnesium sulfate is 15 45, and silicon dioxide is 01, aluminium sesquioxide is 0 0.1, the amount of allocating into is material gross mass the 2 6% of high magnesium consolidating agent.This novel consolidating agent consolidation strength is up to 1000 2000N, is not only suitable for all kinds of ion dust mud contaning material, applies also for iron scale class bulky grain or the metallurgy powder of cohesiveness difference；And can solve the problem that the two English pollution problems that chloride consolidating agent brings, this consolidating agent raw material drawing is the most cheap simultaneously, can be cost-effective.
Description
Technical field
The present invention relates to field of steel metallurgy, particularly one freezes off knot ball press technique with high magnesium consolidating agent and user
Method.
Background technology
Metallurgical industry production process can produce substantial amounts of flue dust, mud, iron scale and other powdery regenerants, these
The iron-holder of powdery regenerant be up to 45% and more than, utilize cold-consolidation pellet process to process these granular materials, have technique letter
List, small investment, instant effect, the saving energy, low cost and other advantages.China's iron and steel annual production 3.5 hundred million tons according to statistics, the iron content of association
Secondary iron-containing resource the most about produces more than ten million ton, and commonly used bentonite, sodium silicate, cement, as binding agent, are mostly deposited
Problem high at green-ball pulverization rate, that rate of drying is slow, intensity is low, ferrous grade reduces.
200510026046.1 disclose a kind of adhesive for fast consolidation of cold solidified pellet, its component includes calcium oxide, two
Silicon oxide, magnesium oxide, aluminium sesquioxide, ferrum oxide and manganese oxide.Its consolidating agent is applied to ion dust mud contaning or ion dust mud contaning contains
Freeze off in knot ball press technique.But, this binding agent is smelted for metallurgy, has certain material limitation, is not suitable for oxidation
The material of the bulky grains such as iron sheet or cohesiveness difference freezes off knot ball press technique.
200610031958.2 disclose a kind of adhesive for fast consolidation of cold solidified pellet, its component includes magnesium chloride, chlorine
Change calcium, iron chloride, sodium chloride, ammonium chloride.Binding agent is the 1.5-2.0% of raw material gross weight with addition of amount.But, this binding agent
Under the metallurgical smelting process condition of high temperature, chloride ion enters flue gas, works the mischief pipeline and fume treatment auxiliary, and uses
This binding agent, chloride ion enters in air with flue gas, also can increase the generation of toxicant two English.
Summary of the invention
It is an object of the present invention to provide a kind of range more extensively, cost is lower and meets the cold consolidation technique of metallurgy powder and makes
By the consolidating agent required and using method, and solve to freeze off the difficult problem that knot pressure ball consolidating agent is chloride.
Realize the object of the invention one freeze off knot ball press technique with high magnesium consolidating agent, including magnesium oxide, calcium oxide, sulphuric acid
Magnesium, silicon dioxide, aluminium sesquioxide and sulfur, in terms of mass parts, each constituent content is as follows:
A kind of high magnesium consolidating agent, in terms of mass parts, each constituent content is as follows:
A kind of high magnesium consolidating agent, in terms of mass parts, each constituent content is as follows:
A kind of high magnesium consolidating agent, in terms of mass parts, each constituent content is as follows:
A kind of high magnesium consolidating agent, in terms of mass parts, each constituent content is as follows:
Magnesium oxide 21.6
Calcium oxide 0.8
Magnesium sulfate 36.9
Silicon dioxide 0.3
The using method of any of the above-described high magnesium consolidating agent, the 2-that the amount of allocating into is material gross mass of described high magnesium consolidating agent
6wt%。
After described material mixes with described high magnesium consolidating agent, control the moisture of mixed material less than 10wt%.
Described material is ion dust mud contaning and iron scale, and wherein said iron scale pulverizing and jevigating to granularity is less than 5mm, contains
Ferrum dirt mud is 1 or more than 1 with the mass ratio of iron scale.
This novel consolidating agent consolidation strength is up to 1000-2000N.It is applicable not only to all kinds of ion dust mud contaning material, the most applicable
In iron scale class bulky grain or the metallurgy powder of cohesiveness difference；And can solve the problem that the two English pollutions that chloride consolidating agent brings are asked
Topic.And this consolidating agent raw material drawing is extensive, cheap, can be with large-scale production and application.
Detailed description of the invention
For better illustrating the present invention, below the technical scheme in the embodiment of the present invention is clearly and completely described.
Embodiment 1
(1) granularity is become to be less than the powder of 5mm iron scale crushing grinding；
(2) preparing novel consolidating agent, meter takes content of MgO 37.9kg, and CaO content 1.4kg, MgSO4 content 20kg, SiO2 contains
Amount 0.4kg, Al2O3 content 0.1kg；
(3), under normal temperature and pressure conditions, consolidating agent joins iron containing sludge and iron scale (proportioning 1:1) by outer dosage 2Wt%
In, material is mixed, it is ensured that mixture moisture is 5-10%；
(4) by belt feeder, mixing material being delivered to ball press feed bin, pressure ball, by under finished ball normal temperature and pressure after balling-up
It is transported to smelting furnace after stacking 12-24h, uses.
Embodiment 2
(1) granularity is become to be less than the powder of 5mm iron scale crushing grinding；
(2) preparing novel consolidating agent, meter takes content of MgO 42.1kg, CaO content 1.6kg, MgSO4 content 44.4kg, SiO2
Content 0.4kg, Al2O3 content 0.1kg；
(3), under normal temperature and pressure conditions, consolidating agent joins iron containing sludge and iron scale (proportioning by outer dosage 2-2.5Wt%
In 1:1), material is mixed, it is ensured that mixture moisture is 6-10%；
(4) by belt feeder, mixing material being delivered to ball press feed bin, pressure ball, by under finished ball normal temperature and pressure after balling-up
It is transported to smelting furnace after stacking 12-24h, uses.
Embodiment 3
(1) granularity is become to be less than the powder of 5mm iron scale crushing grinding；
(2) preparing novel consolidating agent, meter takes content of MgO 37.9kg, CaO content 1.4kg, MgSO4 content 36.9kg, SiO2
Content 0.4kg, Al2O3 content 0.1kg；
(3), under normal temperature and pressure conditions, consolidating agent joins iron containing sludge and iron scale (proportioning 1:1) by outer dosage 6Wt%
In, material is mixed, it is ensured that mixture moisture ＜ 5%；
(4) by belt feeder, mixing material being delivered to ball press feed bin, pressure ball, by under finished ball normal temperature and pressure after balling-up
It is transported to smelting furnace after stacking 12-24h, uses.
Case study on implementation 4
(1) granularity is become to be less than the powder of 5mm iron scale crushing grinding；
(2) preparing novel consolidating agent, meter takes content of MgO 21.6kg, CaO content 0.8kg, MgSO4 content 36.9kg, SiO2
Content 0.3kg；
(3), under normal temperature and pressure conditions, iron containing sludge and iron scale (proportioning 1:1) are joined by outer dosage 3-4Wt%
In, material is mixed, it is ensured that mixture moisture ＜ 5%；
(4) by belt feeder, mixing material being delivered to ball press feed bin, pressure ball, by under finished ball normal temperature and pressure after balling-up
It is transported to smelting furnace after stacking 12-24h, uses.
The beneficial effect that technical solution of the present invention is brought: this novel consolidating agent consolidation strength is up to 1000-2000N.It is suitable for
Scope is wide, is applicable not only to all kinds of ion dust mud contaning material, applies also for iron scale class bulky grain or the metallurgical powder of cohesiveness difference
In material；And can solve the problem that the two English pollution problems that chloride consolidating agent brings, and this consolidating agent raw material drawing is extensive, price
Cheap.
The above, the only present invention preferably detailed description of the invention, but protection scope of the present invention is not limited thereto,
Any those familiar with the art in the technical scope of present disclosure, the change that can readily occur in or replacement,
All should contain within protection scope of the present invention.Therefore, protection scope of the present invention should be with the protection model of claims
Enclose and be as the criterion.
Claims (8)
1. one kind freezes off the knot high magnesium consolidating agent of ball press technique, it is characterised in that by magnesium oxide, calcium oxide, magnesium sulfate, titanium dioxide
Silicon, aluminium sesquioxide form, and in terms of mass parts, each constituent content is as follows:
The most according to claim 1 freezing off ties the high magnesium consolidating agent of ball press technique, it is characterised in that in terms of mass parts, respectively
Constituent content is as follows:
The most according to claim 1 freezing off ties the high magnesium consolidating agent of ball press technique, it is characterised in that in terms of mass parts, respectively
Constituent content is as follows:
The most according to claim 1 freezing off ties the high magnesium consolidating agent of ball press technique, it is characterised in that in terms of mass parts, respectively
Constituent content is as follows:
The most according to claim 1 freezing off ties the high magnesium consolidating agent of ball press technique, it is characterised in that in terms of mass parts, respectively
Constituent content is as follows:
6. the using method freezing off the knot high magnesium consolidating agent of ball press technique described in any one of claim 1-5, it is characterised in that
The 2-6wt% that the amount of allocating into is material gross mass of described high magnesium consolidating agent.
Using method the most according to claim 6, it is characterised in that after described material mixes with described high magnesium consolidating agent,
Control the moisture of mixed material less than 10wt%.
Using method the most according to claim 6, it is characterised in that described material is ion dust mud contaning and iron scale, its
Described in iron scale pulverizing and jevigating to granularity less than 5mm, ion dust mud contaning is 1 or more than 1 with the mass ratio of iron scale.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310656635.2A CN103725873B (en) | 2013-12-06 | 2013-12-06 | One freezes off knot ball press technique high magnesium consolidating agent and using method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310656635.2A CN103725873B (en) | 2013-12-06 | 2013-12-06 | One freezes off knot ball press technique high magnesium consolidating agent and using method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103725873A CN103725873A (en) | 2014-04-16 |
| CN103725873B true CN103725873B (en) | 2016-08-17 |
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|---|---|---|---|
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112126782A (en) * | 2020-10-09 | 2020-12-25 | 河南钰镁新材料科技有限公司 | Binder for alkaline pellet mine and preparation method thereof |
| CN112080633A (en) * | 2020-10-09 | 2020-12-15 | 河南钰镁新材料科技有限公司 | Non-bentonite alkaline pellet and preparation method thereof |
| CN112080634A (en) * | 2020-10-09 | 2020-12-15 | 河南钰镁新材料科技有限公司 | Acidic pellet binder and preparation method thereof |
| CN112176181A (en) * | 2020-10-09 | 2021-01-05 | 河南钰镁新材料科技有限公司 | Bentonite-free acidic pellet and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1737170A (en) * | 2005-09-06 | 2006-02-22 | 季建梅 | Iron concentrate pelletization binder of calcium magnesium reaction type |
| CN101270410A (en) * | 2007-03-20 | 2008-09-24 | 尚国洪 | Cold bonded pellet and method of producing the same |
| CN101525689A (en) * | 2009-03-27 | 2009-09-09 | 莱芜钢铁股份有限公司 | Method for preparing carbonaceous autoreduction cold pressing block and application thereof |
| CN102061359A (en) * | 2004-11-17 | 2011-05-18 | Ism有限公司 | A slag conditioner composition, process for manufacture and method of use in steel production |
| CN102268543A (en) * | 2011-08-30 | 2011-12-07 | 北京科技大学 | Shaping adhesive for chromium powder ore cold-pressed pellets and using method of shaping adhesive |
-
2013
- 2013-12-06 CN CN201310656635.2A patent/CN103725873B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102061359A (en) * | 2004-11-17 | 2011-05-18 | Ism有限公司 | A slag conditioner composition, process for manufacture and method of use in steel production |
| CN1737170A (en) * | 2005-09-06 | 2006-02-22 | 季建梅 | Iron concentrate pelletization binder of calcium magnesium reaction type |
| CN101270410A (en) * | 2007-03-20 | 2008-09-24 | 尚国洪 | Cold bonded pellet and method of producing the same |
| CN101525689A (en) * | 2009-03-27 | 2009-09-09 | 莱芜钢铁股份有限公司 | Method for preparing carbonaceous autoreduction cold pressing block and application thereof |
| CN102268543A (en) * | 2011-08-30 | 2011-12-07 | 北京科技大学 | Shaping adhesive for chromium powder ore cold-pressed pellets and using method of shaping adhesive |
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| CN103725873A (en) | 2014-04-16 |
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